• The Korean Journal of Ceramics
• /
• 제6권1호
• /
• pp.64-67
• /
• 2000

Reactively sputtered $Pb(Zr,Ti)O_3$(PZT) films on $IrO_2$and Ir were evaluated with particular consideration on interface properties. The $IrO_2$and Ir were previously annealed at $650^{\circ}C$ in $O_2$or $N_2$atmosphere, respectively. There was no appreciable roughening in the interface of the $PZT/IrO_2$respective to that of the PZT/Ir; the rms roughness of $IrO_2$and Ir was about 3nm and 10nm, respectively. The ferroelectric properties of the $PZT/IrO_2$were found to be better than that of the PZT/Ir; however, the leakage current of the $PZT/IrO_2$was slightly larger than that of the PZT/Ir. The $PZT/IrO_2$thin films did not exhibit any fatigue up to $10^{11}$ cycles; the $P^*\;_r-P^r$ value decreased only from 16.6 to 14$\mu$C/$\textrm{cm}^2$ until $10^{12}$ polarization reversals. On the other hand, although thin $IrO_2$layer was formed between PZT and Ir, the PZT/Ir thin films began to undergo fatigue after $10^9$ polarization reversals.

• 마이크로전자및패키징학회지
• /
• 제11권1호
• /
• pp.87-96
• /
• 2004

폴리머/세라믹 복합체는 유기기판용 내장형 커패시터의 가장 유망한 재료다. 폴리머/세라믹 복합체의 유효유전상수를 예측하는 것은 복합재료의 설계에 있어 매우 중요하다. 본 논문에서는 크기가 다른 5가지 $BaTiO_3$ 분말을 이용하여 분말함량에 따른 에폭시/$BaTiO_3$ 복합 내장형 커패시터 필름의 유전상수를 측정하였다. 그 측정 결과를 여러 가지 이론식들에 최소 자승법을 이용해 fitting하여 폴리머/세라믹 복합체의 유효유전상수를 예측하는데 가장 유용한 식을 찾고 BaTiO$_3$ 분말의 유전상수를 추정하고자 하였다. Lichtenecker식과 Jayasundere-Smith식이 에폭시/$BaTiO_3$ 복합 내장형 커패시터 필름의 유전상수 예측에 유용한 것으로 나타났다. 피팅을 통해 계산된 $BaTiO_3$ 분말의 유전상수는 분말의 크기에 따라 100 에서 600 사이였는데 이는 다결정 세라믹 $BaTiO_3$의 유전상수보다 작은 값이다.

• The Journal of Advanced Prosthodontics
• /
• 제9권1호
• /
• pp.67-73
• /
• 2017

PURPOSE. The aims of the study were to evaluate the fracture load of zirconia core material after dipping in coloring liquid at different time intervals and to compare the color of dipped blocks with that of prefabricated shaded blocks. MATERIALS AND METHODS. 3-unit bridge frameworks were designed digitally. Sixty frameworks were fabricated using uncolored zirconia blocks by CAD/CAM and divided into 4 groups randomly (n = 15). Group 2 (G2) was subjected to coloring liquids for 2 minutes, Group 4 (G4) for 4 minutes, and Group 6 (G6) for 6 minutes. CFS group was not subjected to any coloring procedure. After coloring, color differences between the test groups and a prefabricated shaded zirconia group (CPZ, n = 15) were evaluated by using a spectrophotometer. Fracture test was conducted immediately after shade evaluation with a Testometric test device at a cross-head speed of 1 mm/sec. Statistical analysis for evaluating color and fracture load was performed by using one way ANOVA followed by Tukey HSD test ($P{\leq}.05$). Weibull analysis was conducted for distribution of fracture load. RESULTS. There was no difference in terms of fracture load and color between CFS (1176.681 N) and G2 (985.638 N) group and between CPZ (81.340) and G2 (81.140) group, respectively. Fracture load values of G4 (779.340 N) and G6 (935.491 N) groups were statistically significantly lower than that of CFS group ($P{\leq}.005$). The color values of G4 (79.340) and G6 (79.673) groups were statistically different than that of CPZ group ($P{\leq}.005$). CONCLUSION. Prolonged immersion of zirconia in coloring liquid not only negatively affected the fracture load of the zirconia being tested in the current study but also deteriorated the desired shade of the restoration.

• 한국전자파학회논문지
• /
• 제19권3호
• /
• pp.343-351
• /
• 2008

본 논문에서는 FPC(Flexible Printed Circuit) 케이블에 적층된 나선형 인덕터를 내장하여 다기능 케이블을 위한 공통 모드 필터를 제안하였다. 공통 모드 필터가 내장된 FPC 케이블은 별도의 SMD(Surface Mounted Device) 필터 없이 연성 케이블과 공통 모드 차단 특성을 가짐으로서, 다기능 케이블이라는 새로운 개념을 제시한다. 내장된 공통 모드 필터는 광대역의 공통 모드 차단 대역을 가지고 손실이 큰 페라이트와 같은 자성 물질을 사용하지 않아 차동 모드 삽입 손실 및 반사 손실이 향상되었다. 3-turn 인덕터를 가진 공통 모드 필터는 공통 모드차단 대역이 $0.4{\sim}3.12GHz$이며, 페라이트를 적용한 상용 LTCC(Low Temperature Co-fire Ceramic) 공통 모드 필터에 비해 3 GHz에서 1.95 dB, 8 GHz에서 6.97 dB의 향상된 차동 모드 삽입 손실을 갖는다.

• 공업화학
• /
• 제31권3호
• /
• pp.338-340
• /
• 2020

견운모는 도자기와 페인트 등의 원료로 쓰이고 있으며 근래에는 흡착제로서 폐수 내 중금속 제거에도 널리 이용되고 있다. 견운모에 함유되어 있는 성분들이 공기 중의 습기와 반응하여 산소를 배출한다는 원리를 이용하여 견운모 분말이 포함된 에어필터를 개발하였다. 새로 개발된 에어필터가 실제로 디젤자동차에 장착되었을 때 연비를 향상시키는지에 대하여 시험하였다. 그 결과 시험에 이용된 디젤자동차가 워밍업이 되었을 때 기존 에어필터를 장착했을 때와 비교하여 연비는 10~17% 증가하는 것으로 나타났다. 하지만 개발된 에어필터가 배출가스(HC, CO, NOx) 배출량에 미치는 영향은 아직 조사되지 않았으며 차후 이에 대한 연구가 필요하다.

• 비파괴검사학회지
• /
• 제28권1호
• /
• pp.40-45
• /
• 2008

고체의 탄성 계수를 구하기 위한 방법으로 초음파의 종파와 횡파 속도를 측정하기 위하여 기존의 접촉식 초음파 시험법 대신 수침 초음파 시험법을 사용하였다. 통상적으로 수침법에서 종파 에코만 고려하는 것과 달리 모드 변환에 의한 횡파 에코를 찾아서 횡파 속도를 측정하였다. 물질의 두께를 알 수 없어 종파와 횡파 속도를 구할 수 없는 경우에도 두 속도의 비를 이용하여 포아송비를 구할 수 있었다. 다양한 재료를 대상으로 이 방법을 적용한 결과, 속도가 빠른 재료이거나, 포아송비가 작을수록 수침법에 의해 측정한 값이 정확하여 이러한 특징을 가진 세라믹이나 고강도 재료가 이 방법을 통한 종파와 횡파 속도 측정에 적당함을 알 수 있었다.

• Journal of Welding and Joining
• /
• 제13권3호
• /
• pp.134-146
• /
• 1995

Aluminium nitride(AlN) is currently under investigation as potential candidate for replacing alumium oxide(Al$_{2}$ $O_{3}$) as a substrate material for for electronic circuit packaging. Brazing of aluminium nitride(AlN) to Cu with Ag base active alloy containing Ti has been investigated in vacuum. Binary Ag$_{98}$ $Ti_{2}$(AT) and ternary At-1wt.%Al(ATA), AT-1wt.%Ni(ATN), AT-1wt.% Mn(ATM) alloys showed good wettability to AlN and led to the development of strong bond between brate alloy and AlN ceramic. The reaction between AlN and the melted brazing alloys resulted in the formation of continuous TiN layers at the AlN side iterface. This reaction layer was found to increase by increase by increasing brazing time and temperature for all filler metals. The bond strength, measured by 4-point bend test, was increased with bonding temperature and showed maximum value and then decreased with temperature. It might be concluded that optimum thickness of the reaction layer was existed for maximum bond strength. The joint brazed at 900.deg.C for 1800sec using binary AT alloy fractured at the maximum load of 35kgf which is the highest value measured in this work. The failure of this joint was initiated at the interface between AlN and TiN layer and then proceeded alternately through the interior of the reaction layer and AlN ceramic itself.

• 한국세라믹학회지
• /
• 제45권12호
• /
• pp.821-826
• /
• 2008

Nanocrystallized glasses with the composition of $(50-x)BaO-xTiO_2-50SiO_2$ (x=10, 15, 16.7 and 20) have been prepared by heat-treatment at $T_x$ (crystallization onset temperature) for 3 h, and their optical properties, photoluminescence (PL), XRD and Raman spectra have been examined. The absorption edges of the glasses were red-shifted and the absorption coefficient increased with an increase of $TiO_2$. The glass subjected to the heat-treatment showed a dense formation of ${Ba_2}{TiSi_2}{O_8}$ crystals. The XRD and Raman results show that the nanocrystallized glasses formed fresnoite phase up to $TiO_2$ concentrations of 15 mol%. Further-more, blue luminescence with a peak at the wavelength of around 470nm was observed in the nanocrystallized glass, demon strating the optical multifunctional nanocrystallized material such as non-linear optics and photo-luminescence. It is thought that the blue luminescence from the ${Ba_2}{TiSi_2}{O_8}$ nanocrystallized glass originated from the presence of $Ti^{4+}$ incorporated into the fresnoite-type structure.

• 대한치과기공학회지
• /
• 제30권2호
• /
• pp.87-92
• /
• 2008

Purpose: In this study, we tried to compare marginal accuracy when produce ceramic crown using all ceramic materials and existent metal-ceramic system. Material and methods: All-ceramic systems were E-max (Ivoclar/Vivadent, Lichtenstein), Lava(3M, U.S.A.) and Wol-ceram(Teamziereis, Germany). Metal-ceramic system(PFG) was composed of Au-Pt alloy (Metalor, Switzerlandand) and overlying ceramic(D-sign, Ivoclar/Vivadent, Lichtenstein). We fabricated metal master die with upper diameter of 7.95mm, bottom diameter of 9.00mm, height of 5.00mm, and taper of $6^{\circ}$. All ceramic system used 0.5mm thickness ceramic coping, while metalceramic system used 0.3 thickness metal coping. By adding dentin and enamel ceramics on each coping, a crown with a proximal thickness of 1.0 mm and occlusal thickness of 2.0mm was fabricated. Pressure of 2kg was applied for 10 seconds on each crown with static load compressor. Before and after cementation, we measured the marginal gap at 4 points of each crown using optical microscope. The data was analyzed using a Student's t test and repeated-measures of analyses of variance(ANOVA) followed by a Bonferroni test. A p value<0.05 was considered significant. Results: As experiment results, marginal accuracy of wol-ceram and Lava is no good when compared with marginal accuracy of PFG. But marginal accuracy of E.max is good when compared with PFG. This result showed not significant. The marginal accuracy of E.max is good when compared with marginal accuracy of wol-ceram and Lava. Conclusion: The marginal accuracy of E.max is very good when compared with marginal accuracy of another group.

• 한국기계가공학회지
• /
• 제16권1호
• /
• pp.118-123
• /
• 2017

It is well known that water jetting is now widely used in the advanced cutting processes of polymers, metals, glass, ceramics, and composite materials because of some advantages, such as heatless and non-contacting cutting different from the laser beam machining. In this paper, we proposed the simulation model of waterjet by lengths and the inner spiral structure of the nozzle. The simulation results show that the outlet velocity of the nozzle is faster than the inlet. Furthermore, we found rapid velocity reduction after passing through the outlet. The nozzle of diameter ${\phi}500$ and length 70mm, shows the optimal fluid width and velocity distribution. Also, the nozzle with inner spiral structure shows a Gaussian distribution of velocity and this model is almost twice as fast as the model without spiral structure, within the effective standoff distance (2.5 mm). In the future, when inserting abrasive material into the waterjet, we plan to analyze the fluid flow and the particle behavior through a simulation model.