• Title/Summary/Keyword: Central X-ray

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The crystal structure of pirprofen$(C_{3},\; H_{14},\; ClNO_2$), a non-steroidal antiinflammmatory agent

  • Kim, Yang-Bae;Park, Il-Yeong
    • Archives of Pharmacal Research
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    • v.19 no.1
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    • pp.71-73
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    • 1996
  • The molecular structure of pirprofen, 3-chloro-4-(2,5-dihydro-1H-pyrrol-1-yl)-.alpha.-methyl-benzeneacetic acid, was determined by single crystal X-ray diffraction analysis. The compound was recrystallized from a mixture of chloroform and toluene in triclinic, space group P over $\bar1,\; with\; a=4.577(1),\; b=11.213(2),\; C=12.485(2){\AA},\alpa.=107.39(1),\;\beta=97.79(1),\;\gamma=92.03(2),\; and Z=2$ The calculated density is $1.384 g/cm^3$. The structure was solved by the direct method and refined by full matrix least-squares procedure to the final R value of 0.034 for 1681 independent reflections. The non-aromatic dihydropyrrol group is found to be coplanar to the central aromatic ring. The molecules are dimerized through the intermolecular hydrogen bonds at the carboxyl group in the crystal.

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A Study on the Accuracy and Convenience of Imaging Method Using Support Device in Knee Joint Lateral Radiography (슬관절의 측면 방사선 촬영에서 보조기구를 이용한 검사방법의 정확성과 편의성에 대한 연구)

  • Uhm, Soyeong;Cho, Yongkeun;Kang, Sungjin
    • Journal of the Korean Society of Radiology
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    • v.11 no.4
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    • pp.253-262
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    • 2017
  • In lateral projection imaging method of knee joint, a method that adjusts the incidence angle of central X-ray toward the head side to $5{\sim}7^{\circ}$ in true lateral position which is existing recommended is called imaging method A, Method of imaging the central X-ray perpendicular to the horizontal plane of the examination table toward the knee is called imaging method B, and a method in which the central X-ray is perpendicularly applied to the joints while the lateral side of the distal tibia is compensated by radiolucent materials is called as method C. After tests each imaging method to classified study subject respectively, the joint space distance and the distance between lateral and medial condyle of femur were measured and compared as the quantitative index from the three imaging methods. In addition, the convenience of each imaging method was confirmed through questionnaires to practician. According to the result of the quantitative index, there is no statistically significant difference in imaging method A and C(p>0.05). However, imaging method B showed a significant difference in both A and C(p<0.05). As a result of evaluating the convenience of the imaging method, imaging method A was relatively assessed lower in all items than imaging methods B and C, and as a small difference, imaging method B is assessed higher than C. In this study suggested new knee joint lateral projection imaging method, by using a simple support device, could describe joint space as not much different as existing recommended method without some complex process, and could increase convenience of the practician in the process of the imaging.

Quantitative X-ray Diffraction Analysis of the Gyeonggi Bay Surface Sediments (경기만 표층퇴적물의 X선 광물정량분석)

  • Moon, Dong-Hyeok;Cho, Hyen-Goo;Kim, Soon-Oh;Yi, Hi-Il;Do, Jin-Young
    • Journal of the Mineralogical Society of Korea
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    • v.22 no.4
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    • pp.279-288
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    • 2009
  • Mineral compositions of the Gyeonggi Bay surface sediments were determined using the high resolution X-ray diffractometer and Siroquant v. 3.0 program. Surface sediments are composed of rock forming minerals (quartz 63.8%, plagioclase 12.9%, alkali feldspar 11.7%, muscovite 4.3%, amphibole 1.2%, biotite 0.5% on average), clay minerals (illite 2.4%, chlorite 1.4%, kaolinite 0.4%) and carbonate minerals (calcite 0.1%, aragonite 0.3%). Coarse sediments are high in the northern, southern and central parts of the study area, whereas fine sediments are high in the northern and southern parts of the central area. Coarse sediments have relatively a high quartz content in the northern part, and relatively high plagioclase and muscovite contents in the southern part of the study area. In the southern part and the northern part of central area, fine sediments have relatively a high illite content, and chlorite and kaolinite contents, respectively.

Biaxial Nematic Phase Derived From Banana-Shaped Molecules Containing Naphthylene Central Unit

  • Seo, Young-Ho;Choi, E-Joon;Park, Sang-Byung;Zin, Wang-Cheol
    • 한국정보디스플레이학회:학술대회논문집
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    • 2008.10a
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    • pp.330-332
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    • 2008
  • Banana-shaped molecules were synthesized introducing ester linking group into mesogenic unit, varying the central unit with 1,6-, 2,3-naphthylenes, and introducing the hexyloxy group as the terminal flexible unit. The properties of the compounds were characterized by FT-IR, NMR spectroscopy, DSC, polarizing optical microscopy, and X-ray diffractometry.

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Research on Microstructure and Properties of TiN, (Ti, Al)N and TiN/(Ti, Al)N Multilayer Coatings

  • Wang, She Quan;Chen, Li;Yin, Fei;Jia, Li
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.658-659
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    • 2006
  • Magnetron sputtered TiN, (Ti, Al)N and TiN/(Ti, Al)N multilayer coatings grown on cemented carbide substrates have been characterized by using electron probe microanalysis (EPMA), X-ray diffraction (XRD), scanning electron spectroscopy (SEM), nanoindentation, scratcher and cutting tests. Results show that TiN coating is bell mouth columnar structures, (Ti, Al)N coating is straight columnar structures and the modulation structure has been formed in the TiN/(Ti, Al)N multilayer coating. TiN/(Ti, Al)N multilayer coating exhibited higher hardness, better adhesion with substrate and excellent cutting performance compared with TiN and (Ti, Al)N coating.

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EFFECT OF FLASH ANNEALING ON MAGNETIC PROPERTIES OF Fe-BASED NANOCRYSTALLINE ALLOYS

  • Yu, Xiaojun;Quan, Baiyun;Sun, Guiqin;Narita, Kenji
    • Journal of the Korean Magnetics Society
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    • v.5 no.5
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    • pp.507-510
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    • 1995
  • A heat-treatment method of pre-annealing and then flash annealing(FA) has been used to improve the soft magnetic properties of nanocrystalline $Fe_{76}CuSi_{13}B_{10}$ and $Fe_{74}CuNb_{3}Si_{12}B_{10}$ alloys. Outstanding magnetic properties of nanocrystalline $Fe_{74}CuNb_{3}Si_{12}B_{10}$ alloy were attained by flash-annealing in air after annealed at $500^{\circ}C$ for 0.5hr below the crystallization temperature. The same results were obtained for $Fe_{74}CuSi_{13}B_{10}$ alloy. The measurment of relief of stress and X-ray diffraction were used to analyze the effect of flashannealing.

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Feasibility Study of Vertical Multileaf Collimator for Determination of Irradiation Size (수직형 다엽 콜리메이터의 방사선 조사면 크기 결정을 통한 유용성 연구)

  • Lee, Chang-Yeol;Son, Ki-Hong;Shin, Sang-Hun;Park, Seung-Woo;Lee, Dong-Han;Jung, Hai-Jo;Choi, Mun-Sik;Oh, Won-Young;Kim, Kum-Bae;Yang, Gwang-Mo;Ji, Young-Hoon
    • Progress in Medical Physics
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    • v.22 no.1
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    • pp.3-11
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    • 2011
  • The purpose of this study was to evaluate feasibility of Vertical Multileaf Collimator for determination of irradiation size using Vertical Multileaf Collimator and lead block to determine 4 different irradiation shape in case of Co-60 gamma-ray and 6 MV X-ray. We chose ion chamber, glass dosimeter and EBT chromic film to compare with Vertical Multileaf Collimator results and lead block results. In case of Co-60 gamma-ray and 6 MV X-ray, the central axis point dose normalized at reference field of lead block with ion chamber results for Vertical Multileaf Collimator were estimated higher than lead block about 5.1%, 4.2%. In case of Co-60 gamma-ray, the central axis point dose normalized at reference field of lead block with glass dosimeter results for Vertical Multileaf Collimator were estimated higher than lead block about 2.2%, 7.8%, 7.2%, 4.0% for reference, circle, triangle, cross field, respectively. In case of 6 MV X-ray, the central axis point dose normalized at reference field of lead block with glass dosimeter results for Vertical Multileaf Collimator were estimated higher than lead block about 6.7%, 6.2%, 3.8%, 6.2% for reference, circle, triangle, cross field, respectively. The results of EBT chromic film, Vertical Multileaf Collimator of penumbra size for all irradiation shape was smaller than lead block of those size that 2.0~3.5 mm for Co-60 gamma-ray, 0.5~1.0 mm for 6 MV X-ray. The results from this study, radiation treatment volume that results in shielding block can be minimized. In addition, during radiation treatment for 2, 3-dimensional radiation therapy using a Vertical Multileaf Collimator of this survey can be used to determine variety of irradiation fields.

A Study on Dobe Distribution outside Co-60 $\gamma$ Ray ana 10MV X Ray Fields ($^{60}Co\;\gamma$선과 10MV X선의 조사면 밖의 선량분포에 관한 연구)

  • Kang, Wee-Saing;Huh, Seung-Jae;Ha, Sung-Whan
    • Radiation Oncology Journal
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    • v.2 no.2
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    • pp.271-280
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    • 1984
  • The peripheral dose, defined as the dose outside therapeutic photon fields, which is responsible for the functional damage of the critical organs, fetus, and radiation. induced carcinogenesis, has been investigated for $^{60}Co\;\gamma$ ray and 10 MV Xray. It was measured by silicon diode controlled by semiautomated water phantom without any shielding or with lead plate of HVL thickness put horizontally or vertically to shield stray radiations. Authors could obtain following results. 1. The peripheral dose was larger than $0.7\%$ of central axis maximum dose even at 20cm distance from field margin. That is clinically significant, so it should be reduced. 2. Even for square fields of 10 MV Xray, radial peripheral dose distribution did not coincide with transverse distribution, because of the position of collimator jaws. 3. Between surface and $d_m$, the peripheral dose distributions show a pattern of the dose distribution of electron beams and the maximum doss was approximately proportional to the length of a side of square field. 4. The peripheral doses depended on radiation quality, field size, distance from field margin and depth in water. Distance from field margin was the most important factor. 5. Except for near surface, the peripheral dose from phantom was approximately equal to that from therapy unit. 6. To reduce the surface dose outside fields, therapist should shield stray radiations from therapy unit by lead plate of at least one HVL for 10 MV X-ray and by bolus equivalent to tissue of 0.5cm thickness for $^{60}Co$. 7. To reduce the dose at depth deeper than $d_m$, it is desirable to shield stray radiations from therapy unit by lead.

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Influence of water content on dynamic mechanical properties of coal

  • Gu, Helong;Tao, Ming;Wang, Jingxiao;Jiang, Haibo;Li, Qiyue;Wang, Wen
    • Geomechanics and Engineering
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    • v.16 no.1
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    • pp.85-95
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    • 2018
  • Water affects the mechanical properties of coal and stress wave propagation. To comprehensively investigate the effect of water content on the properties of coal, laboratory tests including X-Ray Diffraction (XRD) analysis, P-wave test, S-wave test, static and dynamic compression test with different water contents were conducted. The compressive strength, elastic modulus and failure strain and their mechanism of coal specimen under coupled static-dynamic load with the increased water content were observed. Meanwhile, energy transmission and dissipation characteristics of a stress wave in coal specimens with different water contents under dynamic load and its relation with the failure features, such as fragmentation and fractal dimension, of coal was analyzed. Furthermore, the dynamic interpretation of water infusion to prevent coal burst based on water infusion model of coal seam roadway was provided.

Pictorial Review of Diffuse Central Airway Diseases: Focus on CT Findings

  • Ahn, Hye-Shin;Hwang, Jung-Hwa;Chang, Yun-Woo;Kim, Hyun-Joo;Kwon, Kui-Hyang;Choi, Deuk-Lin
    • Tuberculosis and Respiratory Diseases
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    • v.70 no.1
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    • pp.10-20
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    • 2011
  • Various diseases can diffusely involve central airways, including the trachea and main stem bronchi. Central airway abnormalities are frequently not apparent or are overlooked on chest radiographs, even though the patient may have significant symptoms. Recent advances in spiral and multi-detector computed tomography (CT) with multi-planar reconstruction and three-dimensional demonstration, including virtual bronchoscopy, allow for excellent display of central airway anatomy and abnormalities with visualization of accurate locations of lesions. Early detection and proper diagnosis of airway diseases based on various radiographic findings will help determine appropriate treatment, including surgical planning and evaluation of treatment response. Herein we describe and illustrate the imaging findings of a wide spectra of diffuse central airway diseases.