• 제목/요약/키워드: Carbon Content Analysis

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Microstructural, mechanical, and electrochemical analysis of carbon doped AISI carbon steels

  • Muhammad Ishtiaq;Aqil Inam;Saurabh Tiwari;Jae Bok Seol
    • Applied Microscopy
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    • 제52권
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    • pp.10.1-10.15
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    • 2022
  • The effect of carbon doping contents on the microstructure, hardness, and corrosion properties of heat-treated AISI steel grades of plain carbon steel was investigated in this study. Various microstructures including coarse ferrite-pearlite, fine ferrite-pearlite, martensite, and bainite were developed by different heat treatments i.e. annealing, normalizing, quenching, and austempering, respectively. The developed microstructures, micro-hardness, and corrosion properties were investigated by a light optical microscope, scanning electron microscope, electromechanical (Vickers Hardness tester), and electrochemical (Gamry Potentiostat) equipment, respectively. The highest corrosion rates were observed in bainitic microstructures (2.68-12.12 mpy), whereas the lowest were found in the fine ferritic-pearlitic microstructures (1.57-6.36 mpy). A direct correlation has been observed between carbon concentration and corrosion rate, i.e. carbon content resulted in an increase in corrosion rate (2.37 mpy for AISI 1020 to 9.67 mpy for AISI 1050 in annealed condition).

시멘트 재료의 광물탄산화를 위한 이산화탄소 마이크로버블 배합수 활용성 평가 (Evaluation of the Utilization of Carbon Dioxide Microbubble Mixing Water for Mineral Carbonation of Cement Materials)

  • 남민석;박동천
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2023년도 가을학술발표대회논문집
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    • pp.205-206
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    • 2023
  • In this study, the characteristics of cement were analyzed using carbon dioxide microbubble water as a mixed water for mineral carbonation of cement materials. Carbon dioxide reacts with the calcium compound of cement to produce calcium carbonate and affects the initial strength improvement. Therefore, in this study, temperature, air content, thermal analysis, and compressive strength tests were conducted to confirm the reaction between cement materials and carbon dioxide. As a result of the measurement, the reaction between cement and carbon dioxide was confirmed in a specimen using carbon dioxide microbubble water as a mixed water, which affected the initial strength improvement.

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HSLA 강의 미세조직과 저온 샤르피 충격 특성에 미치는 탄소와 니켈의 영향 (Effect of Carbon and Nickel on Microstructure and Low Temperature Charpy Impact Properties of HSLA Steels)

  • 엄해원;조성규;조영욱;신건철;권용재;이정구;신상용
    • 한국재료학회지
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    • 제30권4호
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    • pp.184-196
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    • 2020
  • In this study, effects of carbon and nickel on microstructure and low temperature Charpy impact properties of HSLA (high strength low alloy) steels are investigated. To understand the complex phase transformation behavior of HSLA steels with high strength and toughness before and after welding processes, three kinds of HSLA steels are fabricated by varying the carbon and nickel content. Microstructure analysis, low temperature Charpy impact test, and Vickers hardness test are performed for the base metals and CGHAZ (coarse-grain heat affected zone) specimens. The specimens with the lowest carbon and nickel content have the highest volume fraction of AF, the lowest volume fraction of GB, and the smallest GB packet size. So, the low temperature Charpy absorbed energy of the CGHAZ specimen is the highest. The specimens with increased carbon and nickel content have the lowest volume fraction of AF, the highest volume fraction of GB, and the largest GB packet size. So, the low temperature Charpy absorbed energy of the CGHAZ specimen is the lowest.

전투기 J85-GE-21 터보제트 엔진 후기 연소기 연료펌프의 내부 피스톤 패킹 연료 누출 원인 (Cause of Fuel Leakage from the Inner Piston Packing of Afterburner Fuel Pump in an Aircraft J85-GE-21 Turbojet Engine)

  • 김익식;황영하;손경숙;이중훈;김성욱
    • Elastomers and Composites
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    • 제49권4호
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    • pp.305-312
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    • 2014
  • 대부분 군사용 초음속 전투기는 후기 연소기를 사용한다. 후기 연소기는 초음속 비행, 이륙, 전투 상황에 대해 비상 임무 수행을 가능하게 하는 중요한 역할을 한다. 최근 전투기 J85-GE-21 터보제트 엔진 후기 연소기 연료펌프의 내부 피스톤 패킹고무에서 반복적인 연료 누출 결함이 발생하였다. 이러한 결함은 두 제조사 중 한 제조사의 부품에서만 발생하였다. 따라서, 결함발생 원인을 제조사가 상이한 정상품 및 결함품에 대하여 다양한 비교 분석방법을 통하여 조사하였다. 결함분석에는 팽윤 또는 팽윤도, 총 황함량, 폴리머 확인, 카본블랙 함량 및 표면적, 경도와 같은 분석방법이 적용되었다. 결론적으로, 반복적인 연료 누출 결함의 주요 원인은 보강제 카본블랙의 함량 미달로 확인되었으며, 더불어 표면적이 작은 카본블랙과 함량이 낮은 황 적용이 결함원인에 부가적인 영향을 준 것으로 확인되었다.

텅스텐-15% 카파 사출성형체의 잔류 탄소량 분석에 대한 측정 불확도 (Measurement Uncertainty for Analysis of Residual Carbon in a Tungsten-15% Copper MIM part)

  • 이정근
    • 한국분말재료학회지
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    • 제14권6호
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    • pp.410-414
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    • 2007
  • Carbon contamination from the binder resin is an inherent problem with the metal powder injection molding process. Residual carbon in the W-Cu compacts has a strong impact on the thermal and electric properties. In this study, uncertainty was quantified to evaluate determination of carbon in a W-15%Cu MIM body by the combustition method. For a valid generalization about this evaluation, uncertainty scheme applied even to the repeatability as well as the uncertainty sources of each analyse step and quality appraisal sources. As a result, the concentration of carbon in the W-Cu part were measured as 0.062% with expanded uncertainty of 0.003% at 95% level. This evaluation example may be useful to uncertainty evaluation for other MIM products.

중탄소 고망간강의 합금원소와 열처리 조건이 미세조직과 기계적 특성에 미치는 영향 (Effect of Alloying Elements and Heat Treatment on the Microstructures and Mechanical Properties of Medium Carbon High Manganese Steels)

  • 이동수;박현균
    • 열처리공학회지
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    • 제23권6호
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    • pp.338-343
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    • 2010
  • Mechanical properties and microstructures of medium carbon high manganese steels were investigated in terms of alloying elements such as Mn, C contents, and heat treatment condition. Austenite volume fraction was increased with increasing Mn content, leading to hardness decrease in the range of Mn content of above 10% after quenching and tempering. Such results are also supported by microstructural analysis and X-ray diffraction in that the increase in mangaese content results in the increase in austenite fraction. Studies on tempering condition indicated that not only hardness and tensile strength but also charpy impact values were reduced as tempering temperature were raised in the range of $250^{\circ}C$ to $600^{\circ}C$. It was also observed that fracture mode was changed from dimple to intergranular fracture. Such results are thought to be due to very fine carbide precipitation or impurity segreagation at grain boundaries as tempering temperature goes up. Heat treatment of Fe-5Mn-2Si-1Al-0.4C can be optimized by austenitizing at $850^{\circ}C$, air cooling and tempering at $250^{\circ}C$, resulting in 1950 MPa in Tensile strength, 17% in elongation and 23.3 $J/cm^2$ in charpy impact energy with high work hardening characteristics.

신선 가공에 의한 시멘타이트 재분해가 기계적 특성에 미치는 영향 (Effects of Cementite Dissolution on the Mechanical Properties of the Heavily Drawn Hyper-Eutectoid Steel Wires used for Steel Cords)

  • 양요셉;배종구;박찬경
    • 대한금속재료학회지
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    • 제46권3호
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    • pp.111-117
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    • 2008
  • The effects of the dissolved cementite on the mechanical properties have been experimentally investigated. The steel wires were fabricated depending on the carbon content of 0.82 and 1.02 wt.% and drawing strain from 4.12 to 4.32. The bending fatigue resistance and torsion ductility were measured by a hunter fatigue tester and torsion tester specially designed for thin-sized wires. The results showed that as the drawing strain and carbon content increased, the fatigue resistance and the torsional ductility of the steel wires decreased, while the tensile strength increased. In order to elucidate this behavior, the microstructure in terms of lamellar spacing (${\lambda}_p$), cementite thickness ($t_c$) and morphology of cementite was observed by advanced analysis techniques such as transmission electron microscope (TEM) and 3 dimensional atom probes (3-D AP).

Fabrication and Evaluation of a Total Organic Carbon Analyzer Using Photocatalysis

  • Do Yeon Lee;Jeong Hee Shin;Jong-Hoo Paik
    • 센서학회지
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    • 제32권3호
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    • pp.140-146
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    • 2023
  • Water quality is crucial for human health and the environment. Accurate measurement of the quantity of organic carbon in water is essential for water quality evaluation, identification of water pollution sources, and appropriate implementation of water treatment measures. Total organic carbon (TOC) analysis is an important tool for this purpose. Although other methods, such as chemical oxygen demand (COD) and biochemical oxygen demand (BOD) are also used to measure organic carbon in water, they have limitations that make TOC analysis a more favorable option in certain situations. For example, COD requires the use of toxic chemicals, and BOD is time-consuming and can produce inconsistent and unreliable results. In contrast, TOC analysis is rapid and reliable, providing accurate measurements of organic carbon content in water. However, common methods for TOC analysis can be complex and energy-intensive because of the use of high-temperature heaters for liquid-to-gas phase transitions and the use of acid, which present safety risks. This study focuses on a TOC analysis method using TiO2 photocatalysis, which has several advantages over conventional TOC analysis methods, including its low cost and easy maintenance. For TiO2, rutile and anatase powders are mixed with an inorganic binder and spray-coated onto a glass fiber substrate. The TiO2 powder and inorganic binder solutions are adjusted to optimize the photocatalytic reaction performance. The TiO2 photocatalysis method is a simple and low-power approach to TOC analysis, making it a promising alternative to commonly used TOC analysis methods. This study aims to contribute to the development of more efficient and cost-effective approaches for water quality analysis and management by exploring the effectiveness and reliability of the developed equipment.

연결성 분석을 활용한 산림의 주연부와 내부의 탄소저장량 비교 (Comparison of Carbon Stock Between Forest Edge and Core by Using Connectivity Analysis)

  • 성선용;이동근;모용원
    • 농촌계획
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    • 제21권4호
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    • pp.27-33
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    • 2015
  • Forest ecosystem is considered as an important stepping stone to minimize the impact of climate change. However, the rapid urbanization has caused fragmentation of forest ecosystem. The fragmentation of forest patch results in edge effect which brings about adverse impacts on forest function and structure. Degradation of forest ecosystem decreases carbon sequestration because edge effect reduces productivity. Therefore, we analyzed the impact of forest edge effect on forest ecosystem carbon stock change in Seongnam-si, Gyeonggi-do. We used connectivity analysis to determine forest edge and core area. The field study sites were selected with considering forest age, density, class and soil type. Secondly, forest carbon stock was calculated with allometric equation. The soil carbon stock was derived from Walkely-Black method. Lastly, Mann-Whitney test was conducted to validate differences between carbon stock in edge and core area. As a result of study, the connectivity analysis was effective to determine forest edge and core. The core and edge of forest patch showed different composition of tree species and soil properties. Carbon stock per tree in the edge area was lower than that in the core area. However, the difference of soil organic carbon content between the edge and core were relatively small. This assessment can be applied for the conservation of forest patch as well as quantitative assessment on the forest carbon stock change caused by fragmentation.