• Title/Summary/Keyword: Capsule free het isostatic pressing

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Capsule Free Hot Isostatic Pressing of Ceria-Doped Tetragonal Zirconia Powder Crystallized in Supercritical Methanol

  • Shu Yin;Satoshi Uehida;Yoshinobu Fujishiro;Mamoru Ohmori;Tsugio Sato
    • The Korean Journal of Ceramics
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    • v.5 no.1
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    • pp.73-77
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    • 1999
  • Capsule free hot isostatic pressing (HIPing) of 12 mol% $CeO_2-88 mo% ZrO_2 (12CeO_2-88ZrO_2)$ powder was conducted at 1100~$1200^{\circ}C$ using the powder crystallized in supercritical methanol followed by supercritical drying. Porous $12CeO_2-88ZrO_2$ ceramics with ~35% open porosity, micropore diameter of ~23 nm and a narrow pore size distribution were fabricated by capsule free hot isostatic pressing at $1100^{\circ}C$. The porosity increased with decrease in HIPing temperature and was accompanied by a steady decrease in fracture strength.

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