• 제목/요약/키워드: Calibration Equation

검색결과 311건 처리시간 0.031초

근적외 분광분석법에 의한 밥의 노화도측정 (Determination of Degree of Retrogradation of Cooked Rice by Near-Infrared Reflectance Spectroscopy)

  • 조승용;최성길;이철
    • 한국식품과학회지
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    • 제26권5호
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    • pp.579-584
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    • 1994
  • 기존의 노화도 측정법은 분석시간이 오래 걸리고 노동력이 많이 드는 단점이 있어 이를 개선하기 위해 신속 간편하고 비파괴적인 근적외선 분광분석법(NIR)을 노화도측정에 적용하였다. 밥을 $4^{\circ}C$에서 저장하면서 6시간 간격으로 시료를 채취한 후 동결 건조하여 분말화 한 것을 시료로 하여, 각기 다른 노화($0.0%{\sim}47.1%$)를 나타내는 시료들의 노화도를 NIR을 이용하여 추정하였다. 표준분석법으로는 기존의 분석방법인 glucoamylase를 이용한 효소적 방법에 의해 호화도를 측정하여 이로부터 노화도를 산출하였다. 일정 수분함량인 각 시료의 2차 미분 스펙트럼으로 부터 노화에 의한 흡수(吸收)띠의 변이는 1360, 1434, 1528, 1700, 1780, 1928. 2100, 2284, 2320 nm 영역에서 관찰되었다. 수분함량 5% 이하의 분말시료 32개를 사용하여 이의 2차 미분 스펙트럼으로 부터 노화도를 추정하기 위한 검량식을 구하였으며, 이때 상관계수는 0.9753, SEC는 3.64% 및 SEP는 3.91%를 나타내어 노화도측정을 위한 NIR의 적용 가능성을 보여주었다. 각기 다른 수분함량을 갖는 시료의 노화도 측정에 이 검량식을 적용할 경우 측정시료의 수분함량이 7.0%, 11.4%로 증가함에 따라 SEP와 bias가 증가하고 상관계수가 낮아져 NIR에 의한 노화도의 측정시에는 검량식의 작성에 사용된 5% 이하의 수분함량의 시료를 사용하여야 할 것으로 사료된다.

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전북산 브랜드 쌀의 근적외선 분광스펙트럼과 기계적 식미치간의 상호관계 (Relationship between Near Infrared Reflectance Spectra and Mechanical Sensory Score of Commercial Brand Rice Produced in Jeonbuk)

  • 송영주;송영은;오남기;최영근;조규채
    • 한국작물학회지
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    • 제51권spc1호
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    • pp.42-46
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    • 2006
  • 쌀의 기계적 식미치 측정용으로 최근 많이 사용되고 있는 도요 미도메타의 미도치를 근적외선 분광분석 기를 이용 신속 간편하게 측정할 수 있는지를 검토하고자 실험 하였던바 그 결과는 다음과 같다. 1. 수집된 브랜드 쌀의 도요 미도치는 최저 62.9, 최고 84.2까지의 비교적 넓은 범위를 보였으며, 샘플의 분포 양상도 정규분포에 가까웠다. 2. MPLS(Modified Partial Least Square) 방식에 의한 검량식 작성시 도요 미도치와 근적외선 스펙트럼 간 결정계수 $(R^2)$는 0.94, 표준오차(SEC)는 0.95정도로 비교적 높은 상관성을 보였다. 3. 검량식 검증 표준오차는 1.64, 검증시 상관정도는 0.81로서 근적외선 분광분석기로 도요 미도치를 비 파괴적으로 손쉽게 측정할 수 있는 가능성을 제시 할 수 있었다.

측정 불확도 표현 지침서(GUM)와 Monte-Carlo Simulation에 의한 불확도 전파 결과의 비교 연구 (A Study on Comparison between the Propagation of Uncertainty by GUM and Monte-Carlo Simulation)

  • 서정기;민형식;박민수;우진춘;김종상
    • 대한화학회지
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    • 제47권1호
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    • pp.31-37
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    • 2003
  • 측정 및 화학분석에 많이 이용되는 한 점 교정식에 대하여 측정 불확도 표기 지침서(GUM)의 근사법과 Monte-Carlo Simulation에 의해 계산된 각각의 확장불확도를 비교하였다. 이 비교를 위하여 임의의 자료들을 여러 농도 수준에서 정규 분포 또는 t-분포로 가정하여 계산하였다. 나눗셈에 의한 한 점 교정식의 비선형성과 t-분포 형식을 함에 따른 입력량의 과도한 퍼짐으로 인하여, 경우에 따라서, GUM의 근사법으로 계산된 불확도가 Monte-Carlo Simulation에 의해 계산된 것보다 약 50% 이상의 오류가 있다는 것이 확인되었다. 그러나, 검출 하한을 계산하기 위하여 한 점 교정식을 이용하는 경우, 반응량의 표준불확도가 상대적으로 매우 크고 비선형성에 희한 계산 오류가 상대적으로 무시되므로 근사식에 따른 계산 오류가 발생하지 않았다.

해상도 3차원 상호상관 Volume PIV 시스템 개발 및 적용 (Development and Application of High-resolution 3-D Volume PIV System by Cross-Correlation)

  • 김미영;최장운;이현;이영호
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2002년도 학술대회지
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    • pp.507-510
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    • 2002
  • An algorithm of 3-D particle image velocimetry(3D-PIV) was developed for the measurement of 3-D velocity Held of complex flows. The measurement system consists of two or three CCD camera and one RGB image grabber. Flows size is $1500{\times}100{\times}180(mm)$, particle is Nylon12(1mm) and illuminator is Hollogen type lamp(100w). The stereo photogrammetry is adopted for the three dimensional geometrical mesurement of tracer particle. For the stereo-pair matching, the camera parameters should be decide in advance by a camera calibration. Camera parameter calculation equation is collinearity equation. In order to calculate the particle 3-D position based on the stereo photograrnrnetry, the eleven parameters of each camera should be obtained by the calibration of the camera. Epipolar line is used for stereo pair matching. The 3-D position of particle is calculated from the three camera parameters, centers of projection of the three cameras, and photographic coordinates of a particle, which is based on the collinear condition. To find velocity vector used 3-D position data of the first frame and the second frame. To extract error vector applied continuity equation. This study developed of various 3D-PIV animation technique.

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3차원 Volume PIV의 개발 (Development of 3-D Volume PIV)

  • 최장운;남구만;이영호;김미영
    • 대한기계학회논문집B
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    • 제27권6호
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    • pp.726-735
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    • 2003
  • A Process of 3-D Particle image velocimetry, called here, as '3-D volume PIV' was developed for the full-field measurement of 3-D complex flows. The present method includes the coordinate transformation from image to camera, calibration of camera by a calibrator based on the collinear equation, stereo matching of particles by the approximation of the epipolar lines, accurate calculation of 3-D particle positions, identification of velocity vectors by 3-D cross-correlation equation, removal of error vectors by a statistical method followed by a continuity equation criterior, and finally 3-D animation as the post processing. In principle, as two frame images only are necessary for the single instantaneous analysis 3-D flow field, more effective vectors are obtainable contrary to the previous multi-frame vector algorithm. An Experimental system was also used for the application of the proposed method. Three analog CCD camera and a Halogen lamp illumination were adopted to capture the wake flow behind a bluff obstacle. Among 200 effective particle s in two consecutive frames, 170 vectors were obtained averagely in the present study.

철도교 상시계측시스템의 센서교정방안 연구 (A Study on Calibrations of health monitoring system installed in Railway bridge)

  • 이현석;이준석;최일윤;임명재
    • 한국철도학회:학술대회논문집
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    • 한국철도학회 2003년도 추계학술대회 논문집(II)
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    • pp.483-488
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    • 2003
  • Calibration and gauge factor readjustment process made for the health monitoring system installed in the railway bridges is reviewed and some findings are explained in this study: specifically, the calibrators made for this purpose are illustrated and the regression processes of the calibration on long-term displacement using water level sensor, longitudinal displacement using LVDT sensor, instantaneous displacement using LVDT sensors and accelerometer are described in details. Based on the regression results, new gauge factors are obtained from regression equation and another verification is made by performing another calibration again with new factors. From the second calibration, it was found that the suggested regression curves and their factors are appropriate and much better results are expected. Future work will be concentrated on the long-term analysis of the measurement data and on the database structures so that the assessment of the structure such as damage detection and remaining life estimation is possible.

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물체의 운동패턴을 이용한 로보트 팔의 자기보정 (Self-Calibration of a Robot Manipulator by Using the Moving Pattern of an Object)

  • Young Chul Kay
    • 전자공학회논문지B
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    • 제32B권5호
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    • pp.777-787
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    • 1995
  • This paper presents a new method for automatically calibrating robot link (Kinematic) parameters during the process of estimating motion parameters of a moving object. The motion estimation is performed based on stereo cameras mounted on the end-effector of a robot manipulator. This approach significantly differs from other calibration approaches in that the calibration is achieved by simply observing the motion of the moving object (without resorting to any other external calibrating tools) at numerous and widely varying joint-angle configurations. A differential error model, which expresses the measurement errors of a robot in terms of robot link parameter errors and motion parameters, is developed. And then a measurement equation representing the true measurement values is derived. By estimating the above two kinds of parameters minimizing the difference between the measurement equations and the true moving pattern, the calibration of the robot link parameters and the estimation of the motion parameters are accomplished at the same time.

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레이저 슬릿을 사용하는 능동거리 센서의 정확한 3D 데이터 추출 알고리즘 (An Exact 3D Data Extraction Algorithm For Active Range Sensor using Laser Slit)

  • 차영엽;권대갑
    • 한국정밀공학회지
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    • 제12권8호
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    • pp.73-85
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    • 1995
  • The sensor system to measure the distance precisely from the center of the sensor system to the obstacle is needed to recognize the surrounding environments, and the sensor system is to be calibrated thoroughly to get the range information exactly. This study covers the calibration of the active range sensor which consists of camera and laser slit emitting device, and provides the equations to get the 3D range data. This can be possible by obtaining the extrinsic parameters of laser slit emitting device through image processing the slits measured during the constant distance intervals and the intrinsic parameters from the calibration of camera. The 3D range data equation derived from the simple geometric assumptions is proved to be applicable to the general cases using the calibration parameters. Also the exact 3D range data were obtained to the object from the real experiment.

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SELECTION OF WAELENGTH REGION FOR PLS BRIX CALIBRATION OF MANGO BY MLR METHOD

  • Sarawong, Sirinnapa;Sornsrivichai, Jinda;Kawano, Sumio
    • 한국근적외분광분석학회:학술대회논문집
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    • 한국근적외분광분석학회 2001년도 NIR-2001
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    • pp.1625-1625
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    • 2001
  • The calibration equations for Brix value determination of intact mango were developed using the NIR spectra in a short wavelength region from 700 to 1100 nm. Multiple linear regression (MLR) and partial least square regression (PLS) was used for the calibration. It was found that the best wavelength region for PLS calibration from 900 to 1000 nm was similar to the wavelength region selected by MLR from 906 nm to 996 nm. Both MLR and selected region PLS provided sufficiently accurate prediction equations for Brix determination of intact mango. For MLR, the prediction results were SEP = 0.45 Brix and Bias = -0.04 Brix while PLS prediction results were SEP : 0.46 Brix and Bias = -0.2 Brix. It was concluded that MLR and PLS would have similar abilities in making calibration equation for Brix determination of intact mango if the appropriate wavelengths or wavelength region were selected. The appropriate wavelength region for PLS regression could be assumed by using the wavelength region selected by MLR in place of random selection, The relationship between calibration results of MLR and PLS regression is discussed.

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근외적 분광분석법을 이용한 담배 중 전휘발성염기 분석 (Determination of Total Volatile Bases of Tobacco Using Near Infrared Spectroscopy)

  • 김용옥;장기철;이철희;정한주
    • 한국연초학회지
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    • 제27권2호
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    • pp.207-211
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    • 2005
  • This study was carried out to develop calibration equation of total volatile bases of tobacco leaf using near infrared spectroscopy(NIRS). Burley, imported flue-cured and oriental leaf tobacco samples were collected in 2005 crop year. Calibration equation was developed by modified partial least square method. The standard error of calibration and $R^2$ between traditional analytical method and NIRS analytical method were $0.038\%$, 0.983 for burley and $0.027\%$, 0.986 for imported flue-cured and oriental leaf, respectively. The standard error of performance and $R^2$ between traditional analytical method and NIRS analytical method were $0.048\%$, 0.940 for burley and $0.024\%$, 0.986 for imported flue-cured and oriental leaf, respectively. From these results, the NIRS analytical method seems to be applicable in analyzing total volatile bases of tobacco.