• Title/Summary/Keyword: Bulk samples

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Magnetic Properties of $GdBa_2Cu_3O_{7-y}$ Bulk Superconductors Fabricated by a Top-seeded Melt Growth Process (종자 결정 성장법으로 제조된 $GdBa_2Cu_3O_{7-y}$ 벌크 초전도체의 자기적 특성)

  • Kim, K.M.;Park, S.D.;Jun, B.H.;Ko, T.K.;Kim, C.J.
    • Progress in Superconductivity
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    • v.14 no.1
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    • pp.39-44
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    • 2012
  • The fabrications condition and superconducting properties of top-seeded melt growth (TSMG) processed $GdBa_2Cu_3O_{7-y}$ (Gd123) bulk superconductors were studied. Processing parameters (a maximum temperature ($T_{max}$), a temperature for crystal growth ($T_G$) and a cooling rate ($R_G$) through a peritectic temperature ($T_P$) for the fabrication of single grain Gd123 superconductors were optimized. The magnetic levitation forces, trapped magnetic fields, superconducting transition temperature ($T_c$) and critical current density ($J_c$) of the Gd123 bulks superconductors were estimated. Single grain Gd123 bulk superconductors were successfully fabricated at the optimized processing condition. The $T_c$ of a TSMG processed Gd123 sample was 92.5 K and the $J_c$ at 77 K and 0 T was approximately $50kA/cm^2$. The trapped magnetic field contour and magnetic levitation forces were dependent on the top surface morphology of TSMG processed Gd123 samples. The single grain Gd123 samples, field-cooled at 77 K using a Nd-B-Fe permanent magnet with 5.27 kG and 30 mm dia., showed the trapped magnetic field contour of a single grain with a maximum of 4 kG at the sample center. The maximum magnetic levitation forces of the single grain Gd123 sample, field-cooled or zero field-cooled, were 40 N and 107 N, respectively.

Introduction to European Standard Methods for Physical and Chemical Analysis of Horticultural Substrates (원예용 배지의 물리·화학성 분석을 위한 유럽의 표준방법)

  • Kim, Kye-Hoon;Kang, Ji-Young
    • Horticultural Science & Technology
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    • v.19 no.2
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    • pp.179-185
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    • 2001
  • Throughout the world, physical and chemical analyses of horticultural substrates are carried out in many different ways at the different laboratories. In Europe, standardization in properties and analytical methods of horticultural substrates has been a topic over the last decades. As a result, the CEN methods as European standard methods for the physical and chemical analyses were introduced and the final draft was reported in 1999 by CEN(Committee for European Standardization). Dry matter and moisture content are analyzed after drying samples at $103^{\circ}C$. Laboratory compacted bulk density is analyzed by determining the weight of sample compacted in the test cylinder with constant volume. Dry bulk density, particle density, total pore space, water volume, air volume and volume shrinkage are determined by saturating, draining and drying the sample using double rings and a sand suction table. pH and EC are analyzed by 1:5(sample:distilled water) extraction method on the basis of volume. Organic matter and ash content are determined after drying and combusting the samples. Now, CEN methods are being regarded almost as European standard methods. Further study needs to be carried out for universal applicability of the CEN methods to all the substrates.

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Effect of Bulk Shape on Mechanical Properties of Ti-6Al-4V Alloy Manufactured by Laser Powder Bed Fusion (Laser Powder Bed Fusion 공정으로 제조된 Ti-6Al-4V 합금의 형상 차이에 따른 기계적 특성 변화)

  • Haeum Park;Yeon Woo Kim;Seungyeon Lee;Kyung Tae Kim;Ji-Hun Yu;Jung Gi Kim;Jeong Min Park
    • Journal of Powder Materials
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    • v.30 no.2
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    • pp.140-145
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    • 2023
  • Although the Ti-6Al-4V alloy has been used in the aircraft industry owing to its excellent mechanical properties and low density, the low formability of the alloy hinders broadening its applications. Recently, laser-powder bed fusion (L-PBF) has become a novel process for overcoming the limitations of the alloy (i.e., low formability), owing to the high degree of design freedom for the geometry of products having outstanding performance used in high-tech applications. In this study, to investigate the effect of bulk shape on the microstructure and mechanical properties of L-PBFed Ti-6Al-4V alloys, two types of samples are fabricated using L-PBF: thick and thin samples. The thick sample exhibits lower strength and higher ductility than the thin sample owing to the larger grain size and lower residual dislocation density of the thick sample because of the heat input during the L-PBF process.

Manufacturing and Evaluation of the Properties of Hybrid Bulk Material by Shock-compaction of Nanocrystalline Cu-Ni Mixed Powder (나노 구리-니켈 혼합분말의 충격압축법을 통한 복합벌크재의 제조 및 특성평가)

  • Kim, Wooyeol;Ahn, Dong-Hyun;Park, Lee Ju;Kim, Hyoung Seop
    • Journal of Powder Materials
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    • v.21 no.3
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    • pp.196-201
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    • 2014
  • In this study, nanocrystalline Cu-Ni bulk materials with various compositions were cold compacted by a shock compaction method using a single-stage gas gun system. Since the oxide layers on powder surface disturbs bonding between powder particles during the shock compaction process, each nanopowder was hydrogen-reduced to remove the oxide layers. X-ray peak analysis shows that hydrogen reduction successfully removed the oxide layers from the nano powders. For the shock compaction process, mixed powder samples with various compositions were prepared using a roller mixer. After the shock compaction process, the density of specimens increased up to 95% of the relative density. Longitudinal cross-sections of the shock compacted specimen demonstrates that a boundary between two powders are clearly distinguished and agglomerated powder particles remained in the compacted bulk. Internal crack tended to decrease with an increase in volumetric ratio of nano Cu powders in compacted bulk, showing that nano Cu powders has a higher coherency than nano Ni powders. On the other hand, hardness results are dominated by volume fraction of the nano Ni powder. The crystalline size of the shock compacted bulk materials was greatly reduced from the initial powder crystalline size since the shock wave severely deformed the powders.

Phoneme Segmentation based on Volatility and Bulk Indicators in Korean Speech Recognition (한국어 음성 인식에서 변동성과 벌크 지표에 기반한 음소 경계 검출)

  • Lee, Jae Won
    • KIISE Transactions on Computing Practices
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    • v.21 no.10
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    • pp.631-638
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    • 2015
  • Today, the demand for speech recognition systems in mobile environments is increasing rapidly. This paper proposes a novel method for Korean phoneme segmentation that is applicable to a phoneme based Korean speech recognition system. First, the input signal constitutes blocks of the same size. The proposed method is based on a volatility indicator calculated for each block of the input speech signal, and the bulk indicators calculated for each bulk in blocks, where a bulk is a set of adjacent samples that have the same sign as that of the primitive indicators for phoneme segmentation. The input signal vowels, voiced consonants, and voiceless consonants are sequentially recognized and the boundaries among phonemes are found using three devoted recognition algorithms that combine the two types of primitive indicators. The experimental results show that the proposed method can markedly reduce the error rate of the existing phoneme segmentation method.

Hydrogen Absorption by Crystalline Semiconductors: Si(100), (110) and (111)

  • Jeong, Min-Bok;Jo, Sam-Geun
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.383-383
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    • 2010
  • Gas-phase hydrogen atoms create a variety of chemical and physical phenomena on Si surfaces: adsorption, abstraction of pre-adsorbed H, Si etching, Si amorphization, and penetration into the bulk lattice. Thermal desorption/evolution analyses exhibited three distinct peaks, including one from the crystalline bulk. It was previously found that thermal-energy gaseous H(g) atoms penetrate into the Si(100) crystalline bulk within a narrow substrate temperature window(centered at ~460K) and remain trapped in the bulk lattice before evolving out at a temperature as high as ~900K. Developing and sustaining atomic-scale surface roughness, by H-induced silicon etching, is a prerequisite for H absorption and determines the $T_s$ windows. Issues on the H(g) absorption to be further clarified are: (1) the role of the detailed atomic surface structure, together with other experimental conditions, (2) the particular physical lattice sites occupied by, and (3) the chemical nature of, absorbed H(g) atoms. This work has investigated and compared the thermal H(g) atom absorptivity of Si(100), Si(111) and Si(110) samples in detail by using the temperature programmed desorption mass spectrometry (TPD-MS). Due to the differences in the atomic structures of, and in the facility of creating atom-scale etch pits on, Si(100), (100) and (110) surfaces, the H-absorption efficiency was found to be larger in the order of Si(100) > Si(111) > Si(110) with a relative ratio of 1 : 0.22 : 0.045. This intriguing result was interpreted in terms of the atomic-scale surface roughening and kinetic competition among H(g) adsorption, H(a)-by-H(g) abstraction, $SiH_3(a)$-by-H(g) etching, and H(g) penetraion into the crystalline silicon bulk.

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Iodine Concentrations in Commercial Milks and Bulk Tank Milks of Dairy Farms Performed Different Teat Dipping Methods (젖소 목장의 유두침지소독 방법에 따른 집합유와 시판 우유 내 요오드 농도)

  • Jeong, Jihyeok;Kim, Danil;Kim, Doo
    • Journal of Veterinary Clinics
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    • v.33 no.5
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    • pp.274-277
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    • 2016
  • To determine the concentrations of commercial milks and the effect of different teat dipping methods on iodine concentrations of bulk tank milk, iodine concentration was analyzed by inductively coupled plasma mass spectrometry (ICP-MS). The 59 bulk tank milk samples were collected. The 8 brands of commercial whole milk and 5 brands of commercial organic milk were purchased. The iodine concentrations of bulk tank milks of 59 dairy farms were in the range from 42.7 to $562.5{\mu}g/L$. The iodine levels of 4 different teat dipping methods with pre-dipping, post-dipping, pre & post-dipping, and non-dipping were $138.9{\pm}41.1$, $200.6{\pm}106.9$, $205.1{\pm}93.2$, and $110.9{\pm}70.4{\mu}g/L$, respectively. No significant difference (P > 0.05) was observed among 4 different teat dipping methods. Iodine concentrations of commercial whole milks were in the range from 149.1 to $210.4(178.8{\pm}22.0){\mu}g/L$, and iodine concentrations of commercial organic milks were in the range from 85.0 to $356.9(214.2{\pm}123.3){\mu}g/L$. Iodine concentrations of commercial milk in Korea are relatively low comparing with those of other countries.

In vitro Study on the Functionality in Digestive Tract of Chitin and Chitosan from Crab Shell (게껍질 Chitin 및 Chitosan의 소화관내 기능성에 관한 in vitro 연구)

  • Chang, Hyun-Joo;Jeon, Dong-Won;Lee, Su-Rae
    • Korean Journal of Food Science and Technology
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    • v.26 no.4
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    • pp.348-354
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    • 1994
  • Chitin and chitosan samples prepared from crab's shells under different conditions were compared for their physicochemical properties; and functionality in gastrointestinal tract by in vitro test. Their bulk density was in the range of $127{\sim}208\;mg/ml$, and their viscosity was $80{\sim}581\;cP$ in 0.1 chitin and $80{\sim}3,670\;cP$ in 0.5% chitosan solution, showing a wide variation. The degree of deacetylation in chitosan samples as determined by IR spectral analysis was relatively high, showing $81{\sim}93%$. At the same alkali concentration and reaction temperature, a longer reaction period gave an increased degree of deacetylation and lower viscosity. The water holding capacity of chitic substance became greater at higher soaking temperature; chitosan D at $37^{\circ}C$ showed the greatest value. Chitic substance with lower bulk density showed the higher water holding capacity. The retardation effect toward glucose absorption was higher in critic substances of lower density and higher water holding capacity; chitosan D showed the highest value of 38%. The retardation index toward bile acid absorption after 1 hour dialysis was $15{\sim}34%$ in chitic substances, 39% in pectin and 9% in cellulose. The retarding effect showed the highest value of 34% in chitosan D at 3% concentration.

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Sintering and Dielectric of $YMnO_3$ Ceramics with the Effect of Y/Mn Ratio (Y/Mn의 혼합비에 따른 $YMnO_3$세라믹의 소결 및 유전특성)

  • 김재윤;김부근;김강언;정수태;조상희
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.13 no.2
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    • pp.137-142
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    • 2000
  • The sintering and electrical properties of YMnO3 bulk ceramics were investigated with Y/Mn ratios(Mn rich ;0.80/1.20, 0.90/1.10, 0.95/1.05, and Y rich ; 1.00/1.00, 1.05/0.95, 1.10/0.90). The crystal structure of samples showed a hexagonal structure, and the sample of Y/Mn = 0.95/1.05 indicated higher c-axis oriented peak than other samples. In the case of Mn rich samples, the grain sizes were about 7.8${\mu}{\textrm}{m}$ and they showed 95% of theoretical density. Whereas, in the case of Y rich samples, the grain sizes were about 2.3${\mu}{\textrm}{m}$ and they showed 86%. The dielectric constant and dissipation factor of the Mn rich samples were smaller than those of the Y rich samples. The samples of Y/Mn = 0.90/1.10 showed the lowest a dissipation factor, and their dielectric constant, dissipation factor and Curie temperature were 36, 0.0136 and 68$0^{\circ}C$, respectively.

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Prevalence of bovine viral diarrhea virus from dairy cattle farms in Gyeongnam southern area, Korea (경남 남부지역 젖소 사육 농가의 소바이러스성설사병(BVD) 감염실태 조사)

  • Park, Jong-Sik;Park, Jong-Kyu;Cho, Eun-Jung;Kim, Eun-Gyeong;Lee, Jong-Min;Kim, Do-Kyung;Son, Seong-Ki
    • Korean Journal of Veterinary Service
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    • v.36 no.1
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    • pp.7-13
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    • 2013
  • Bovine viral diarrhea virus (BVDV) is one of the most important disease viruses in cattle that can cause severe economical losses due to decreased fertility, abortion, diarrhea, and respiratory symptoms. Therefore, this study was aimed to investigate prevalence of BVDV infection (Transiently infection, Persistently infection) in dairy cattle in Gyeongnam southern area, Korea and use this data as the basis for establishing an eradication program and policy. A total of 44 bulk-tank milk samples (farms) collected in milk collecting center were tested for BVDV antibody using an ELISA. As the result, out of a total of 44 bulk-tank milk samples (farms), 38 (86.4%) samples were BVDV antibody positive. Blood samples (17 farms, n=543) were collected from BVDV antibody positive farms in bulk-tank milk, tested for BVDV antigen with ELISA and PCR. BVDV infected farms were 47% (8/17) and BVDV infected head were 2.2% (12/543). Persistently infected cattle (PI) were detected at 6 (35.3%) farms out of 17 farms and a total of 6 (1.1%) out of 543 head of cattle were identified as PI. The seropositive of BVDV antibody at farms and head were 100% (17/17) and 49.45% (91/184), respectively. The seroprevalence of BVDV antibody in PI infected farms (67.35%) much higher than that of BVDV antibody in transiently infected cattle (TI) infected farms (45%) and uninfected farms (34.48%). For eradication of BVDV infection in cattle populations, First of all, we should remove PI and need vaccination.