• Restorative Dentistry and Endodontics
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• 제40권2호
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• pp.136-142
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• 2015

Objectives: The aim of this study was to evaluate the effects of tri-antibiotic paste (TAP) on microtensile bond strengths (MTBS) of dental adhesives to dentin. Materials and Methods: Sixty extracted molars had their occlusal surfaces flattened to expose dentin. They were divided into two groups, i.e., control group with no dentin treatment and experimental group with dentin treatment with TAP. After 10 days, specimens were bonded using self-etch (Filtek P90 adhesive) or etch-and-rinse (Adper Single Bond Plus) adhesives and restored with composite resin. Teeth were sectioned into beams, and the specimens were subjected to MTBS test. Data were analyzed using two-way ANOVA and post hoc Tukey tests. Results: There was a statistically significant interaction between dentin treatment and adhesive on MTBS to coronal dentin (p = 0.003). Despite a trend towards worse MTBS being noticed in the experimental groups, TAP application showed no significant effect on MTBS (p = 0.064). Conclusions: The etch-and-rinse adhesive Adper Single Bond Plus presented higher mean bond strengths than the self-etch adhesive Filtek P90, irrespective of the group. The superior bond performance for Adper Single Bond when compared to Filtek P90 adhesive was confirmed by a fewer number of adhesive failures. The influence of TAP in bond strength is insignificant.

• 구강회복응용과학지
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• 제21권2호
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• pp.95-103
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• 2005

Purpose: Recently, various metal primers have been developed, and these are known to increase the bond strength between metal and relining resin. In this study, the change in bond strength according to amount of thermocycling was evaluated. Materials and Methods: In this study, 216 specimens were fabricated. Tokuyama Rebase $II^{(R)}$(Tokuyama Corp., Japan) and $Kooliner^{(R)}$(GC America Inc., Japan) as relining material, and MR. $Bond^{(R)}$(Tokuyama Corp., Japan) and Alloy $Primer^{(R)}$(Kuraray Medical Inc., Japan) as a metal primers were used. Using Ni-Cr and various metal surface treatment methods, resin was bonded and the change in bond strength during thermocycling was measured. The data was analyzed by one-way ANOVA, t-test(p<.05 level of significance). Results: When comparing the groups with only sandblasting, rapid decrease in shear bond strength could be seen. In the groups using Tokuyama Rebase $II^{(R)}$, with the exception of the 1000 and 2000 cycle groups, each group showed statistically significant decrease in shear bond strength(p<0.05). In comparison according to relining materials, $Kooliner^{(R)}$ showed higher shear bond strength than Tokuyama Rebase $II^{(R)}$ in all groups. In groups using MR $bond^{(R)}$, $Kooliner^{(R)}$ had higher shear bond strength than Tokuyama Rebase $II^{(R)}$ but, there was no statistical significance(p<0.05). In the other groups, $Kooliner^{(R)}$ showed significantly higher shear bond strength(p<0.05). There was significant difference between groups with sandblasting and metal primer treatments(p<0.05). In comparison according to metal primer materials, Alloy $Primer^{(R)}$ showed the highest shear bond strength but there was no statistical significance(p>0.05). According to the number of thermocycling cycles, when using Tokuyama Rebase $II^{(R)}$, there were no significant differences between the 0, 1000 and 2000 cycle groups regardless of the type of metal primer. There were no differences between the 2000 and 3000 cycle groups. When using $Kooliner^{(R)}$, regardless of the type of metal primer, there were no significant differences between the 0, 1000, 2000 and 3000 cycle groups(p>0.05). Conclusion: The use of metal primers showed increase in bond strength, and the stability after to thermocycling has been authenticated. Thus, the use of metal primers in relining and rebasing of metal frameworks is essential. But when selecting the material various physical properties should be considered.

• Restorative Dentistry and Endodontics
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• 제32권4호
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• pp.377-384
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• 2007

작금의 치질 접착시스템은 도말층 처리 방법에 따라 전부식형과 자가부식형 접착시스템으로 대별된다. 이러한 두 가지 접착시스템의 효용성을 비교, 평가하고 열순환 횟수에 따른 미세누출도 변화를 측정하기 위해 각각의 접착시스템으로 수복된 우치 5급 수복물에, 수복 초기의 효용성를 의미하는 500회의 열순환 자극과 상대적으로 긴 내구성을 의미하는 5,000회의 열순환 자극을 부여한 다음, 전기화학적 방법으로 측정하였다. 건전한 40개의 단근관을 가진 우치를 이용하여 백악법랑 경계부를 중심으로 5급 와동을 형성하였으며, 치아를 각각 10개씩 4개의 실험군 (열순환 횟수 2종 $\times$ 복합레진 수복 2개 군)으로 분류하였다. 20개의 치아에는 전부식형 접착시스템인 Single bond와 Z250 (shade A4)을, 나머지 20개의 치아에는 자가부식형 접착시스템인 AQ bond와 Metafil (shade A4)로 각각 충전하고 광중합기 (XL2500, 3M ESPE, St. Paul, MN, USA)를 이용하여 $600\;mW/cm^2$의 광도로 40초간 광중합하였다. 모든 시편을 실온에서 24 시간동안 증류수에 보관한 다음, 연마하고 각 수복물의 반은 섭씨 5도와 55도의 수조에 30초씩 담궜으며 이동 시간 10초의 열순환 (thermocycling)을 500회 시행하였고, 나머지 반은 5,000회 실시하였다. 미세 전류 측정을 위해 직류 공급원인 TOE 8841 (TOELLNER electronic instrument GMBH, Germany)을 이용하여 10 V의 전압을 부여하였으며 6514 system Electrometer (Keithley Co., Cleveland, Ohio, USA)로 미세전류 (${\mu}A$)를 측정하였다. 전류를 흐르게 한 다음 5-10분까지 20초 간격으로 측정 한 15개 측정치의 평균값을 시편의 미세전류 측정치로 인정하였다. 각 군간의 미세전류 측정치에 대한 유의성은 수복방법 및 열순환 횟수의 변수에 대한 Two-way ANOVA test로 95% 유의 수준에서 검증하여 다음과 같은 결과를 얻었다. 수복방법과 열순환 횟수 사이의 상호작용은 없었으며 (p = 0.485), 열순환 횟수에 따른 미세누출의 차이도 없었다(p = 0.814). 그러나 자가부식형 접착시스템인 AQ Bond와 Metafil로 수복된 실험군이 전부식형 접착시스템인 Single Bond와 Z250으로 수복된 군에 비해 적은 미세누출도를 보였다 (p = 0.005).

• Restorative Dentistry and Endodontics
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• 제23권1호
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• pp.183-196
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• 1998

The purpose of this study was to determine the effect of bleaching technique on the shear bond strength of esthetic restorative materials to bovine enamel. The bleaching agent was used 35% $H_2O_2$(Hi-Lite, Shofu, U.S.A.). Experimental groups were divided into two divisions as group A and B. Experimental A groups for the effect of number of bleaching were as follows ; Group Al : no bleaching Group A2 : bleaching 1 time ( for 5 minutes ) Group A3 : bleaching 3 times ( each for 5 minutes ) Group A4 : bleaching 6 times ( each for 5 minutes ) Group A5 : bleaching 9 times ( each for 5 minutes ) Experimental B groups for the effect of storage period in artificial saliva were as follows ; Group B1 : not stored in artificial saliva after bleaching Group B2 : stored in artificial saliva for 1 day after bleaching Group B3 : stored in artificial saliva for 1 week after bleaching Group B4 : stored in artificial saliva for 2 weeks after bleaching Group B5 : stored in artificial saliva for 4 weeks after bleaching Composite resin and glass ionomer cement were bonded to all specimens, and the shear bond strength between enamel and r~storative material were measured in Instron Universal Testing Machine(Instron, 4467, U.S.A,), Additionally, the bleached enamel specimens were examed after etching with 37.4% $H_3PO_4$ for 1 min under SEM(S-2300, Hitachi Co., Japan) to observe the effect of bleaching procedure on enamel surface morphology. The result were as follows ; 1. In SEM findings, bleached bovine enamel was found to be superficially rough. 2. In bleached bovine enamel, the effect of acid etching was reduced with the increase of number of bleaching. 3. The mean shear bond strength of composite resin and glass ionomer cement to bleached enamel surface tended to be lower than those to non-bleached enamel surface. 4. With the increase of number of bleaching, the shear bond strength of composite resin and glass ionomer cement to bleached enamel were progressively decreased. 5. Increasing the, storage period in artificial saliva after bleaching, the shear bond strength of composite resin and glass ionomer cement to bleached enamel were progressively increased. 6. The mean shear bond strength of glass ionomer cement to bleached bovine enamel tended to be clearly lower than that of composite resin.

• Advances in materials Research
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• 제8권1호
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• pp.25-36
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• 2019

The utilization of fibre in concrete production not only solves the problem of disposing this solid waste but helps conserve natural resources. This study investigated the effect of waste aluminum shavings on bond strength of laterized concrete. Laterized concrete spliced beams of $150{\times}250{\times}2150mm$ and $175{\times}275{\times}2300mm$ were prepared. Fifteen specimens with 16 mm and 20 mm were cast with the addition of aluminium shavings at varying percentages of 1vol%, 1.5vol% and 2vol%; another ten specimens with 16 mm and 20 mm diameter bars at 0% of aluminium shavings were cast as control. Concrete cubes of number were prepared, three taken for each set of various percentages of aluminium shavings were used to determine the concrete strength. It was observed from the analysis that the compressive strength decreased as the percentage of aluminium shavings increased, while the aluminium shavings increased the bond between concrete and steel. However, for normal concrete there was an increase in bond resistance with increase in aluminium shavings. The bond resistance of 16 mm was found to be higher than that of 20 mm in all the specimens tested.

• 한국세라믹학회지
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• 제44권3호
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• pp.175-181
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• 2007

Molecular dynamics simulation (MD) of $(62-x)CaO{\cdot}38Al_{2}O_{3}{\cdot}xBaO$ glasses has been carried out using empirical potentials with the covalent term. The simulations closely reproduce the total neutron correlation functions of glass with 5 mol% BaO and physical properties of these glasses such as elastic constants. For these glasses, aluminum is tetrahedrally coordinated by oxygen, but there is a part of five-fold and six-fold coordination of aluminum. There are no major changes to the mid-range structure of glass, as barium is substituted for calcium. To predict the barium coordination number, we have used the bond valence (BV) theory and also compared the results of simulation with Bond valence. The coordination number for oxygen around barium atoms is close to 8 and the average distance of barium and oxygen is nearly 2.80 A. The viscosity of these glasses increases with the content of barium oxide substituted for calcium oxide.

• Bulletin of the Korean Chemical Society
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• 제15권10호
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• pp.868-873
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• 1994

We have re-examined the linear solvation energy relationships in reversed phase liquid chromatography by considering various solutes including quite a number of compounds of strong hydrogen bond capability. We observed that solutes of strong hydrogen bond ability should be excluded in order to obtain resonable correlations between In k' and solute polarity parameters and that inclusion of one or two such solutes causes severe distortions of correlation results. This anomaly may be due to existence of residual silanol groups in the stationary phase, that is, their specific interactions with solutes.

• Restorative Dentistry and Endodontics
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• 제17권2호
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• pp.383-397
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• 1992

The purpose of this study was to evaluate the influence of artificial saliva contamination on bonding of several dentin adhesives to dentin. Sixty - three human molar teeth extracted within a month were used. Each tooth was sectioned longitudinally in a buccolingual direction to obtain 126 specimens. These specimens were randomly divided into three groups and were treated by Scotchbond 2, Gluma and All bond. Each group was subdivided into three subgroups; normal group not contaminated with artificial saliva, contaminated with artificial saliva and dried group, and contaminated with artificial saliva and washed and dried group. Enamel/dentin bonding agent(Dental Adhesive of Scotchbond 2) was applied and light cured on the treated dentin surfaces. Thereafter P - 50 were cured on them, and specimens were stored in $37^{\circ}C$ artificial saliva for 24 hours before measuring shear bond strength. Shear bond strengths were determined using an universal testing machine with cross head speed 1mm/min and SEM examinations were conducted to evaluate the resin - dentin interface and degree of penetrating resin string into the dentinal tubules. The following results were obtained. 1. Normal groups not contaminated with artificial saliva showed greater shear bond strength than any other group contaminated with artificial saliva(P<0.01). 2. The shear bond strengths showed no significant difference between washed groups with distilled water and not washed groups after contamination with artificial saliva(P>0.05). 3. In normal groups, the shear bond strength of A group was significantly greater than in any other group(P<0.01). 4. In Sand G groups, fractures after shear bond strength tests occured adhesively on resintooth interface in all specimens. But in A groups, fracture of the normal group occured cohesively in dentin and fracture of the contaminated groups occured adhesively and cohesively. 5. On SEM examination, the number of resin strings penetrated into dentinal tubules were the greatest in normal groups, followed by, in descending order, washed groups and not washed groups after contamination with artificial saliva.

• 대한소아치과학회지
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• 제25권1호
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• pp.76-92
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• 1998

The purpose of this study was to evaluate the possible efficacy of Nd-YAG laser as a dentin conditioner by observing the laser irradiation dentin surface under scanning electron micrograph and measuring shear bond strength of restored light-cured glass ionomer mold. Fifty intact premolars were prepared for shear bond strength tests. The teeth were randomly divided into five groups as follows; Group I. no treatment Group II. 10% poly acrylic acid, 20 sec Group III. laser treatment 2 w, 20 Hz, 2 sec Group IV. laser treatment 2 w, 20 Hz, 5 sec Group V. laser treatment 2 w, 20 Hz, 10 sec Samples of each group were restored with light-cured glass ionomer cement after dentin conditioning and then measuring the shear bond strength of each specimen were measured using universal testing machine. Additional ten premolars were prepared for SEM analysis The result from the this study can be summarized as follows. 1. Shear bond strength of polyacrylic acid-treated group (II) was significantly higher than other groups (p<0.05). 2. No statistically significant difference could be found between three laser-treated groups (III, IV, V) in shear bond strength(p>0.05) 3. According to the result of observation under SEM, Polyacrylic acid was shown to have removed the smear layer effectively and opened the dentinal tubules, whereas the laser has produced the irregular surface mainly composed of melted and fused structure. The microcracks found in laser-treated groups increased in number with irradiation time and formed the regular mesh-type in 10 sec-irradiation group. 4. The ultrastructural change of dentin surface created by laser irradiation was found to the improper for bonding of the glass ionomer restorative materials. And the lower shear bond strength of laser irradiated group might have been due to the failure to form the suit able dentin surface for the glass ionomer to penetrated into and form the proper micromechanical retention.

• Journal of Welding and Joining
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• 제14권2호
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• pp.71-78
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• 1996

In order to rpovide proper SMT design criteria in a systematic way, a mathematical formulation has been developed to predict the configuration of the solder fillet formed between the gullwing type lead and rectangular pad. Effects of SMT design parameters such as the solder volume and pad dimension on the solder profile are investigated using the FEM that calculates the 3D configuration by minimizing the energy due to surface tension and gravity in the equilibrium state. Design criteria of QFP and SOP are illustrated by plotting the acceptable range of the solder volume with respect to the length and width ratios of the pad and lead. The results show that the acceptable design range increases with increase in the pad length and width. The pad length has more significant effects on design criteria compared with the pad width, and Bond number can be utilized to predict the joint quality.