• Title/Summary/Keyword: Boiling absorption

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Hydride Generation-Atomic Absorption Spectrophotometric Determination of Total Selenium in Atmospheric Particulate (환원기화 원자 흡광광도법에 의한 대기분진중의 총 셀렌의 정량)

  • 이용근;최건형;이동수;황규자
    • Journal of Korean Society for Atmospheric Environment
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    • v.6 no.2
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    • pp.147-154
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    • 1990
  • A sensitive method for the determination of total selenium in aerosol particles is described. The method involves dissolution of aerosol particles by $HNO_3-HClO_4$ mixed acids, pre-reduction of Se (VI) to Se (IV) by boiling hydrochloric acid, and hydride generation followed by atomic absorption detection. Dissolved Se (IV) in 4M hydrochloric acid is reacted with $NaBH_4$ to form $H_2Se$, which is subsequently collected in an U-tube cooled in liquid nitrogen. Upon the completion of $H_2Se$ generation, the collected $H_2Se$ is rapidly vaporized into a quartz cuvette burner by removing the U-tube from liquid nitrogen, atomized, and then detected by an atomic absorption spectrophotometer. The absolute sensitivity of the method is 0.49 ng/0.0044 Abs. The accuracy of the method evaluated by analyzing standard reference materials for urban aerosol is better than 10%. Analytical results for urban and rural aerosol particles are reported.

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A Study on Remodeling for Solar driven $NH_3/H_2O$ absorption chiller (태양열 구동 $NH_3/H_2O$ 흡수식 냉동기 리모델링 연구)

  • Shin, You-Soo;Maeng, Ju-Sung;Kwak, Hee-Youl
    • Journal of the Korean Solar Energy Society
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    • v.23 no.4
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    • pp.37-43
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    • 2003
  • The aim of this research is to study the feasibility of the solar(hot fluid) driven $NH_3/H_2O$ absorption chiller, made by re-manufacturing of Gas fired $NH_3/H_2O$ absorption chiller. This experimental study is performed with the temperature of the inlet hot fluid of generator. In order to determine the inlet temperature of the generator, which gives maximum COP, the experimental data are obtained with various hot fluid supply temperature in range of $130\sim170^{\circ}C$. Remodeled chiller is operated with periodical cooling effect, which due to mixture subcooled pool boiling, then the COP is evaluated in average. The maximum COP$(\sim0.36)$ is at $160^{\circ}C$. The temperature is stable operation temperature range of typical vacuum collector. It offers a feasibility of solar driven $NH_3/H_2O$ absorption chiller.

A Power-Generation System using Cavitation jet flow (케비테이션 제트 유동을 이용한 발전 시스템)

  • Na, Jeoungsu;Lee, Kangju;Lee, Bongyeol;Joo, Namsik
    • 한국신재생에너지학회:학술대회논문집
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    • 2010.06a
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    • pp.162.1-162.1
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    • 2010
  • Cavitation phenomenon has long been a difficult problem that regarded as negative event to fluid machines or industrial facilities. In the latest, however, some engineers became to understand the power of cavitation and use it to cleaning wall after developing cavitation nozzle. In this paper, we introduce new concept for power-generation system using cavitation jet flow maid by nozzle and impulse turbine in vacuum condition. The vacuum needed to make cavitation is generated naturally by Torricelli's vacuum, 10.23m effective head drop without additional power. We analyzed water's boiling and the steam's mean free path according to vacuum purity levels for nozzles and turbine blades. The nozzles make water accelerate in the neck and boil in expansion section of the nozzles. The shape of the impulse turbine is designed for absorption of the molecule's kinetic energy of the steam.

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Palatability Evaluation and Physical Characteristics of Cooked Rice (쌀의 물리적 특성과 식미와의 상관)

  • Kim Young Doo;Ha Un Gu;Song You Chun;Cho Jun Hyeon;Yang Eun In;Lee Jae Kil
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.50 no.spc1
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    • pp.24-28
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    • 2005
  • Many parameters such as textural, cooking and pasting properties and chemical components aye the main reasons of tardy progress in evaluation of cooked rice. To increase the evaluation effect of cooked rice, physical properties and palatability of cooked rice were studied with five varieties. The highest palatability was observed in Kosihikari while Hoan showed the lowest value. The cooked rice of Kosihikari showed a high values of waxiness (0.12) and boiling time (21.1 min.) while the porosity and expansibility were as low as 19.0 and $28.6\%$, respectively. The water absorption time of Kosihikari and Sindongin was a little bit slow compare to the other varieties. A negative correlations were observed between palatability and expansibility (-0.390), porosity (-0.874**) and water absorption time (-0.960**) while a positive correlations were observed between palatability and boiling time (0.861**), waxiness (0.920**) and hardness (0.478). The path coefficient of water absorption time, porosity, boiling time and waxiness contributed to the palatability were 35.9, 22.7, 17.0 and $8.2\%$, respectively, Thus, the results obtained in this study suggested that the physical characteristics of vice grains could be effectively utilized in high quality of cooked rice breeding programs.

인공심장판막의 현황

  • 김형묵
    • Journal of Biomedical Engineering Research
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    • v.10 no.2
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    • pp.94-96
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    • 1989
  • Explosive evaporative removal process of biological tissue by absorption of a CW laser has been simulated by using gelatin and a multimode Nd:YAG laser. Because the point of maximun temperature of laser-irradiated gelatin exists below the surface due to surface cooling, evaporation at the boiling temperature is made explosively from below the surface. The important parameters of this process are the conduction loss to laser power absorption (defined as the conduction-to-laser power parameter, Nk), the convection heat transfer at the surface to conduction loss (defined as Bi), dimensionless extinction coefficient (defined as Br.), and dimensionless irradiation time (defined as Fo). Dependence of Fo on Nk and Bi has been observed by experiment, and the results have been compared with the numerical results obtained by solving a 2-dimensional conduction equation. Fo and explosion depth (from the surface to the point of maximun temperature) are increased when Nk and Bi are increased.To find out the minimum laser power for explosive evaporative removal process, steady state analysis has been also made. The limit of Nk to induce evaporative removal, which is proportional to the inverse of the laser power, has been obtained.

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A Study on the Improvement for the Lifetime of Epoxy Composites (에폭시복합체의 수명개선에 관한 연구)

  • Kim, T.Y.;Lee, D.J.;Shin, J.Y.;Shin, S.K.;Hong, J.W.;Kim, J.H.
    • Proceedings of the KIEE Conference
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    • 2000.11c
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    • pp.485-487
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    • 2000
  • Dielectric strength of insulators made of epoxy composites rapidly decreases due to ageing to interfaces between the matrix resin and filler particles. The adhesion variation of interfaces caused by moisture absorption also alters electrical properties that are the basic characteristics of insulators, particularly, in out door use. In this paper, electrical properties of epoxy/$SiO_2$ composites were investigated at boiling absorption condition to observe that influence of moisture. The breakdown time of samples were measured under AC 6[kV] applied voltage, and the variation of lifetime was varified by using Weibull distribution function.

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Thermal stabilityof fluorine doped silicon oxide films

  • Lee, Seog-Heong;Yoo, Jae-Yoon;Park, Jong-Wan
    • Journal of Korean Vacuum Science & Technology
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    • v.2 no.1
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    • pp.25-31
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    • 1998
  • The reliability of fluorine doped silicon oxide (SiOF) films for intermetal dielectrics in multilevel interconnections of ultra-large scale integrated circuits (ULSIs) is investigated. SiOF films were deposited by electron cyclotron resonance plasma-enhanced chemical vapor deposition (ECRPECVD) using H-free source gases, i.e., SiF4 and O2. The effect of post plasma treatment on the moisture absorption and dielectric properties of SiOF films was carried out I terms of air exposure time, The reliability test of Cu/TiN/SiOF/Fi specimen was carried out in terms of temperature by rapid thermal annealing (RTA) in N2 ambient. After O2 plasma treatment,, no appreciable peak directly related to moisture absorption was detected. The capacitance-voltage (C-V) characteristics of the O2 plasma treated SiOF film showed that the film remained to hold the sound dielectric properties even after boiling treatment. The Cu/TiN/SiOF/Si system was found to be reliable up to $600^{\circ}C$.

Effect of Parameters in Evaporative Removal Process by Absorption of a CW Laser (연속 레이저 흡수에 의한 증발제거 과정의 관련 인자 영향 고찰)

  • 김진윤;송태호
    • Journal of Biomedical Engineering Research
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    • v.16 no.1
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    • pp.67-76
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    • 1995
  • Explosive evaporative removal process of biological tissue by absorption of a CW laser has been simulated by using gelatin and a multimode Nd: YAG laser. Because the point of maximun temperature of laser-irradiated gelatin exists below the surface due to surface cooling, evaporation at the boiling temperature is made explosively from below the surface. The important parameters of this process are the conduction loss to laser power absorption (defined as the conduction-to-laser power parameter, Nk), the convection heat transfer at the surface to conduction loss (defined as Bi), dimensionless extinction coefficient (defined as BrJ, and dimensionless irradiation time (defined as Fo). Dependence of Fo on Nk and Bi has been observed by experiment, and the results have been compared with the numerical results obtained by solving a 2-dimensional conduction equation. Fo and explosion depth (from the surface to the point of maximun temperature) are increased when Nk and Bi are increased. To find out the minimum laser power for explosive evaporative removal process, steady state analysis has been also made. The limit of Nk to induce evaporative removal, which is proportional to the inverse of the laser power, has been obtained.

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Varietal Difference in Water Absorption Characteristics of Milled Rice, and Its Relation to the Other Grain Quality Components

  • Hae Chune, Choi;Jeong Hyun, Chi;Soo Yeon, Cho
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.44 no.3
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    • pp.288-295
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    • 1999
  • Nineteen japonica and Tongil-type rices were selected from seventy nine Korean and Japanese rice cultivars grown in 1989 based on the water uptake behavior of milled rice under the room temperature and boiling conditions. The selected rice cultivars were investigated for water absorbability and some physicochemical characteristics of milled rice, proper water amount for cooking and sensory evaluation of cooked rice. The relationships among the tested grain properties were also examined. The highest varietal variation of water uptake rate was observed at twenty minutes after soaking in water. The maximum water uptake of milled rices at room temperature occurred mostly at about eighty minutes after soaking in water. Newly harvested rices showed a significantly lower water uptake rate of milled rice at 20 minutes after soaking, a relatively higher maximum water absorption ratio under the room temperature, and the less water uptake and volume expansion of boiled rice compared with the one-year old rice samples. The water uptake rate and the maximum water absorption ratio showed significantly negative correlations with the K/Mg ratio and alkali digestion value(ADV) of milled rice. The rice materials showing the higher amount of hot water absorption exhibited the larger volume expansion of cooked rice. The harder rices with lower moisture content revealed the higher rate of water uptake at twenty minutes after soaking and the higher ratio of maximum water uptake under the room temperature condition. These water uptake characteristics were not associated with the protein and amylose contents of milled rice ansd the palatability of cooked rice. The water/rice ratio(in w/w basis) for optimum cooking was averaged to 1.52 in dry milled rices (12% wet basis) with varietal range from 1.45 to 1.61 and the expansion ratio of milled rice after proper boiling was averaged to 2.63(in v/v basis). The water amount needed for optimum cooking was the lowest in Cheongcheongbyeo (Tongil-type rice) and the highest in Jinbubyeo, and the amount could be estimated with about 70% fittness by the multiple regression formula based on some water uptake characteristics, ADV and amylose content of milled rice as the independent variables. Nineteen rice cultivars were classified into seven groups based on scatter diagram projected by principal component analysis using eight properties related to water uptake and gelatinization of milled rice.

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Optical Limiting Properties of Multi-Walled Carbon Nanotube Suspensions (다중벽 탄소 나노튜브 현탁액의 광 리미팅 특성)

  • Yu Hyojung;Kim Sok Won
    • Korean Journal of Optics and Photonics
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    • v.15 no.5
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    • pp.449-454
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    • 2004
  • The optical limiter is an optical component which reduces laser beam intensity for the protection of eyes and light sensors. Carbon nanotube is now known as a highly efficient optical limiting material. Optical limiting effect of the multi-walled carbon nanotube suspensions, in several kinds of solvents such as distilled water, chloroform, ethanol and ethylene glycol, were measured in the range from room temperature to near to the boiling points of the solvents. The pulsed Nd:YAG laser whose wavelength is 1064 nm and pulse duration is 6 ns was used as a light source. The experimental result shows that the limiting efficiency was reduced as the temperature increased, and the suspension which has lower boiling point, viscosity and surface tension has highest efficiency.