• Title/Summary/Keyword: Bench-scale reactor

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Dynamic Behavior of an Internal Loop Reactor during Scale-up (내부순환반응기의 Scale-up에 따른 동력학적 특성의 변화)

  • 최윤찬;박영식
    • Journal of Environmental Science International
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    • v.6 no.1
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    • pp.25-31
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    • 1997
  • The variations of gas hold-up, overall volumetric oxygen mass transfer coefficients and liquid circulation velocity in an internal loop reactor were investigated to manifest scale-up effect. The relationship between superficial gas velocity and gas hold-up were found as Ugr = 0.045 $\varepsilon$r in the pilot-scale and Ugr = 0.056 $\varepsilon$r in the bench-scale reactor. The overall volumetric oxygen mass tractsfer coefficient, KLa was slightly increased in the pilot-scale than in the bench-scale reactor. Flow regime was changed from the bubble flow to the churn-turbulent flow when the superficial gas velocity reached to 3.5 - 4 cm/sec in the pilot-scale.

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KIER Liquefaction R & D's status (KIER 액화 기술 개발 현황)

  • Yang, Jung-Il;Yang, Jung Hoon;Lee, Ho-Tae;Chun, Dong Hyun;Kim, Hak-Joo;Jung, Heon
    • 한국신재생에너지학회:학술대회논문집
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    • 2010.06a
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    • pp.110.1-110.1
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    • 2010
  • A bench scale slurry bubble column reactor (SBCR) with active-Fe based catalyst was developed for the Fischer-Tropsch synthesis (FTS) reaction. Considering the highly exothermic reaction heat generated in the bench scale SBCR, an effective cooling system was devised consisting of a U-type dip tube submerged in the reactor. Also, the physical and chemical properties of the catalyst were controlled so as to achieve high activity for the CO conversion and liquid oil ($C_{5+}$) production. Firstly, the FTS performance of the FeCuK/$SiO_2$ catalyst in the SBCR under reaction conditions of $265^{\circ}C$, 2.5 MPa, and $H_2/CO=1$ was investigated. The CO conversion and liquid oil ($C_{5+}$) productivity in the reaction were 88.6% and 0.226 $g/g_{cat}-h$, respectively, corresponding to a liquid oil ($C_{5+}$) production rate of 0.03 bbl/day. To investigate the FTS reaction behavior in the bench scale SBCR, the effects of the space velocity and superficial velocity of the synthesis gas and reaction temperature were also studied. The liquid oil production rate increased upto 0.057 bbl/day with increasing space velocity from 2.61 to 3.92 $SL/h-g_{Fe}$ and it was confirmed that the SBCR bench system developed in this research precisely simulated the FTS reaction behavior reported in the small scale slurry reactor.

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Effect of Temperature on Treatment of Nitrogen and Phosphorus of Pig Wastewater in Bench Scale Reactor (실험실 수준의 반응조 온도가 양돈폐수중 질소, 인의 처리에 미치는 영향)

  • 박석환
    • Journal of Environmental Health Sciences
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    • v.21 no.1
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    • pp.86-92
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    • 1995
  • This study was performed to evaluate the effect of temperature on operating parameters for reactor in pig wastewater treatment using sequencing batch reactor method which is one of the biological treatment methods. Study was accomplished by experimental apparatus of bench scale, and the degradation rate coefficient and temperature correction factor were derived. The followings are the conclusions that were derived from this study. 1. In the characteristics of pig wastewater, concentrations of TKN and T-P were very high as 590 mg/l and 40 mg/l, respectively. 2. Removal efficiency of BOD and $COD_{Mn}$ as organic compound indicators were the highest mark as 97% at 25$\circ$C. 3. When temperature was incresed from 10$\circ$C to 25$\circ$C, removal efficiencies of TKN and T-P were proportionally increased. Especially, the former was greatly effected by temperature of reactor. 4. In experiment of bench scale, the degradation rate coefficients were increased as temperature increased, but decreased at the temperature range of 25~35$\circ$C. Temperature adjustment coefficients for $COD_{Mn}$, BOD, TKN and T-P were 1.1460, 1.1356, 1.1140 and 1.0565, respectively.

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A Study on Microorganism Dominant Species in Bench-scale Shipboard STP Using Combined SBR and MBR Process (SBR 및 MBR 복합공정을 적용한 Bench-scale Shipboard STP에서의 미생물 우점종에 관한 연구)

  • Choi, Young-Ik;Shin, Dae-Yeol;mansoor, Sana;Kwon, Min-Ji;Jung, Jin-Hee;Jung, Byung-Gil
    • Journal of the Korean Society for Environmental Technology
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    • v.19 no.6
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    • pp.550-555
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    • 2018
  • International Maritime Organization (IMO) is one of the most effective organizations in evolving international law for the protection and conservation of the marine environment. The IMO, MARPOL(Marine Pollution) 73/78 contains six Annexes that provide an overarching framework for the objectives of the international marine pollution. Annex IV was regulated by 64 th resolution in 2012 to control sea pollution from sewage. In 2014 large-scale wastewater treatment and nutrient removal device was developed with a grant from the Ministry of Oceans and Fisheries. A combined new process of Sequence Batch Reactor (SBR) and Membrane Bioreactor(MBR) was developed to overcome the pollution caused by shipboard sewage. In the present study, shipboard sewage wastewater was treated by mixing and aeration cycle in the newly developed SBR process. Furthermore, during analysis by NGS technique(Macrogen Co., Ltd.), dominant species of bacteria were found in the aeration tank of the Bench-scale wastewater treatment facility. Bacteroidetes and Gammaproteobacteria accounted for 27.1 % of the aerobicbacteria and 16.8 % of the anaerobicbacteria, respectively. Microorganisms play a vital role in shipboard wastewater treatment. A further detailed study is required to understand the precise role of the microorganisms in the wastewater treatment.

Study on $SF_6$ hydrate Formation and Dissociation Behavior inside of Bench-scale High Pressure Reactor (Bench-scale 고압반응기 내의 미세액적분사에 따른 $SF_6$ 하이드레이트 형성 거동 연구)

  • Moon, Dong-hyun;Lee, Jae-jeong;Shin, Hyung-Joon;Lee, Ju-Dong;Lee, Gang-Woo
    • 한국신재생에너지학회:학술대회논문집
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    • 2009.06a
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    • pp.687-690
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    • 2009
  • 본 연구에서는 가스 하이드레이트 형성과정에서 발생할 수 있는 유도지체시간을 줄이고 전체 가스 저장량과 반응 속도의 향상을 위하여 이류체 분사 방식을 이용하여 물분자의 액적을 최소화하는 실험을 통하여, 미세액적 분사에 따른 하이드레이트 형성 시간을 확인하였으며, 반응기 내부의 온도 변화를 확인하여 반응기 내부의 하이드레이트 형성 거동을 확인하고 이를 통하여 상용화를 위한 반응기 설계의 기초 자료로 활용하고자 하였다.

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Biological Phosphorus Removal using the Sequencing Batch Reactor Process (연속회분식반응조를 이용한 생물학적인 인 제거 연구)

  • Yang, Hyung-Jae;Shin, Eung-Bai;Chung, Yun-Chul;Choi, Hun-Geun
    • Journal of Korean Society on Water Environment
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    • v.16 no.4
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    • pp.533-539
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    • 2000
  • A bench-scale reactor using SBR process was experimented with an synthetic wastewater. The main purpose of this investigation was to evaluate applicability in the field and process removal efficiencies in terms of BOD and T-P and its corresponding kinetic parameters. Removal rate of phosphorus was 77% in terms of total phosphorus. Effluent concentrations were $9.8mg/{\ell}$ BOD and $1.1mg/{\ell}$ T-P. Effluent quality was maintained consistently stable by controlling decant volume and operating cycles. The efficiency for phosphorus removal was increased due to decrease in BOD-SS loading value in the range of $0.25{\leq}$aeration time ratio${\leq}0.52$.

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Bench-scale Test of Sulfuric Acid Decomposition Process in SI Thermochemical Cycle at Ambient Pressure (SI 열화학싸이클 황산분해공정의 Bench-scale 상압 실험)

  • Jeon, Dong-Keun;Lee, Ki-Yong;Kim, Hong-Gon;Kim, Chang-Soo
    • Transactions of the Korean hydrogen and new energy society
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    • v.22 no.2
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    • pp.139-151
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    • 2011
  • The sulfur-iodine (SI) thermochemical water splitting cycle is one of promising hydrogen production methods from water using high-temperature heat generated from a high temperature gas-cooled nuclear reactor (HTGR). The SI cycle consists of three main units, such as Bunsen reaction, HI decomposition, and $H_2SO_4$ decomposition. The feasibility of continuous operation of a series of subunits for $H_2SO_4$ decomposition was investigated with a bench-scale facility working at ambient pressure. It showed stable and reproducible $H_2SO_4$ decomposition by steadily producing $SO_2$ and $O_2$ corresponding to a capacity of 1 mol/h $H_2$ for 24 hrs.

A Study on a Process for Conversion of Carbon Dioxide through Saline Water Electrolysis (염수 전기분해와 연계한 이산화탄소의 전환 공정 연구)

  • Lee, Dong Woog;Lee, Ji Hyun;Lee, Junghyun;Kwak, No-Sang;Lee, Sujin;Shim, Jae-Goo
    • Korean Chemical Engineering Research
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    • v.55 no.1
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    • pp.86-92
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    • 2017
  • A process, which converts carbon dioxide contained in the flue gas of coal-fired power plants to sodium bicarbonate, was studied experimentally and numerically. In this process, the carbon dioxide reacts with sodium hydroxide which is produced through saline water electrolysis. A bench scale reactor system was prepared for experiments of this process and numerical process modeling was performed for the bench scale reactor system. Comparing the process modeling results with the experimental data, responsibility of the process modeling was confirmed. Using this model, commercial scale process was simulated. Mass and energy balance of this process were calculated. Temperature profile in the reactor and carbon dioxide removal rate were obtained.

Control of a batch reactor using iterative learning (반복학습을 이용한 회분식 반응기의 제어)

  • 조문기;방성호;조진원;이광순
    • 제어로봇시스템학회:학술대회논문집
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    • 1991.10a
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    • pp.81-86
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    • 1991
  • The iterative learning operation has been utilized in the temperature Control of a batch reactor. A generic form of feedback-assisted first-order learning control scheme was constructed and then various design and operation modes were derived through convergence and robustness analysis in the frequency domain. The proposed learning control scheme was then implemented on a bench scale batch reactor with the heat of reaction simulated by an electric heater. The results show a great improvement in the performance of control as the number of batch operations progressed.

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Control of a batch reactor by learning operation

  • Lee, Kwang-Soon;Cho, Moon-Khi;Cho, Jin-Won
    • 제어로봇시스템학회:학술대회논문집
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    • 1990.10b
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    • pp.1277-1283
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    • 1990
  • The iterative learning control synthesized in the frequency domain has been utilized for temperature control of a batch reactor. For this purpose, a feedback-assisted generalized learning control scheme was constructed first, and the convergence and robustness analyses were conducted in the frequency domain. The feedback-assisted learning operation was then implemented in a bench scale batch reactor where reaction heat is simulated using an electric heater. As a result, progressive reduction of temperature control error could be obviously observed as batch operation is repeated.

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