• Smart Structures and Systems
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• v.5 no.4
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• pp.329-344
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• 2009

Ultrasonic chaotic excitations combined with sensor prediction algorithms have shown the ability to identify incipient damage (loss of preload) in a bolted joint. In this study we examine a physical experiment on a single-bolt aluminum lap joint as well as a three-dimensional physics-based simulation designed to model the behavior of guided ultrasonic waves through a similarly configured joint. A multiple bolt frame structure is also experimentally examined. In the physical experiment each signal is imparted to the structure through a macro-fiber composite (MFC) patch on one side of the lap joint and sensed using an equivalent MFC patch on the opposite side of the joint. The model applies the waveform via direct nodal displacement and 'senses' the resulting displacement using an average of the nodal strain over an area equivalent to the MFC patch. A novel statistical classification feature is developed from information theory concepts of cross-prediction and interdependence. This damage detection algorithm is used to evaluate multiple damage levels and locations.

• Archives of Pharmacal Research
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• v.24 no.2
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• pp.100-104
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• 2001

Differential pulse polarographic(DPP) analytical procedure for the rifampicin antibiotic, which can be applied to monitor its synthetic process from the starting antibiotic of rifamycin B or rifamycin SV has been developed based on the electrochemical reduction of an azomethine group. Rifampicin exhibited a cathodic peak due to the azomethine group in the side chain of 3-[(4-methyl-1-piperazinyl)imino]methyl moiety and another cathodic peak due to the carbonyl group in rifamycin SV by DPP. The experimental peak potential shift of an azomethine reduction was -73 mV/pH in the pH range between 3.0 and 7.5, agreeing with involvement of 4 e-and 5 $H^5$ in its reduction. By the cyclic voltammetric(CV) studies, the azomethine and the carbonyl reductions in rifampicin were processed irreversibly on the mercury electrode. The plot of peak currents vs. concentrations of rifampicin ranging $1.0{\times}10^{-7} M~$1.0{\times}10^{-5} M yielded a straight line with a correlation coefficient of 0.9996. The detection limit was $1.0{\times}10^{-8} M with a modulation amplitude of 50 mV DPP has been successfully applied for the determination of rifampicin in the pharmaceutical preparations.

• Bulletin of the Korean Chemical Society
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• v.35 no.2
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• pp.489-493
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• 2014

A phenylbenzimidazole derivatized sensor (L) that behaves as a ratiometric fluorescent receptor for $Zn^{2+}$ in water has been described. In HEPES buffer at pH 7.4, sensor L displays a weak fluorescence emission band at 367 nm. Upon addition of $Zn^{2+}$, the emission intensity at 367 nm is decreased, concomitantly, a new emission band centered at 426 nm is developed, thus facilitates a ratiometric $Zn^{2+}$ sensing behavior. Sensor L binds $Zn^{2+}$ through a 1:1 binding stoichiometry with high selectivity over other metal cations. Sensor L displays a linear response to $Zn^{2+}$ concentration from 0 to $6.0{\times}10^{-5}M$, sensor L also exhibits high sensitivity to $Zn^{2+}$ with a detection limit of $3.31{\times}10^{-7}M$.

• Bulletin of the Korean Chemical Society
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• v.32 no.3
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• pp.809-814
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• 2011

A method based on the TMS derivatives and acidic hydrolysis was developed for the simultaneous determination of free and conjugated steroidal hormones in surface water. A silylation of five natural and two synthetic steroidal hormones was achieved with N-methyl-N-(trimethylsilyl) trifluoroacetamide/$NH_4I$ (1000:3) under catalysis of dithioerythritol for 60 min at $80^{\circ}C$. TMS derivatives of the steroid hormones containing multifunctional groups offer a single derivative product under this condition. The accuracy of the analytes was in the range of 87 to 110% at a concentration of 20 and 50 ng/L with relative standard deviations of less than 10%. The method detection limit was in the range of 0.01 to 0.02 ng/L for surface water. Natural steroidal hormones were detected in a concentration range of 0 to 1.03 ng/L in free form and 0 to 14.6 ng/L in conjugated form, respectively. We found that most of the natural hormonal steroids exist in conjugate forms (43 to 100%) in river water.

• Bulletin of the Korean Chemical Society
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• v.30 no.6
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• pp.1252-1256
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• 2009

A simple, selective and sensitive fluorescence quenching method was developed to the determination Cr(VI). The method is based on the oxidation of $I^-\;to\;{{I_3}^-}$ by Cr(VI) in sulfuric acid solution followed by immediate formation of ion association compound between I3 − and rhodamine 6G in Tween-80 micellar media at room temperature. The influence of several surfactants on rhodamine 6G fluorescence signal was studied; particular attention was paid in the aggregation behavior of rhodamine 6G–Tween-80 system. The experimental parameters (e.g., type of surfactant, reagent concentration) were studied and the optimal conditions were established. The linear calibration graph was obtained in the range 2.0 - 100.0 ng m$L^{-1}$ Cr(VI). The detection limit of the method was 0.37 ng m$L^{-1}$. The relative standard deviation (R.S.D.) is less than 5% (n = 5). The efficiency of the method for the determination of Cr(VI) in the presence of Cr(III) in the sample was investigated. The method was applied successfully to the determination of Cr(VI) and total Cr in water, and liver tissue samples.

• Proceedings of the KIEE Conference
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• 2000.07d
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• pp.3233-3235
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• 2000

A new method for HRV(heart rate variability} detection from the R-wave signal, based on the IPFM (integral pulse frequency modulation) model and its similarity to pulse position modulation, is presented. The proposed method exert lowpass filtering with a Kaiser window. In this paper, The proposed method presents a powerful, but simple, tool for investigation of HRV. It also guarantees real-time behavior, simplicity in design, and phase linearity. Even without the basic assumption of IPFM model, the new algorithm can still be used on-line and with higher performance. It is thoroughly proved that lowpass filtering is an ideal method for PSD (Power Spectrum Density) analysis of HRV.

• Computers and Concrete
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• v.3 no.2_3
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• pp.123-144
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• 2006

Reinforced concrete corbels are structural elements widely used in practical engineering. The complex response of these elements is described in design codes in a simplified manner. These formulations are not sufficient to show the real behavior, which, however, is an essential prerequisite for the manufacturing of numerous elements. Therefore, a deterministic and probabilistic study has been performed, which is described in this contribution. Real complex structures have been modeled by means of the finite element method supported primarily by experimental works. The main objective of this study was the detection of uncertainties effects and safety margins not captured by traditional codes. This aim could be fulfilled by statistical considerations applied to the investigated structures. The probabilistic study is based on advanced Monte Carlo simulation techniques and sophisticated nonlinear finite element formulations.

• Journal of the Korean Society of Marine Environment & Safety
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• v.3 no.2
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• pp.23-31
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• 1997

The results of high speed photography, acoustic emission detection and plasma UV radiation intensity measurement during CO2 laser welding of stainless steel 304 are presented. Video images with high spatial and temporal resolution allowed to observe the melt dynamics and keyhole evolution. The existence of a high speed melt flow which originated from the part of weld pool and flowed along the sides wall of keyhole was confirmed by the slag motion on the weld pool. the characteristic frequencies of flow instability and keyhole fluctuations at different welding speed were measured and compared with the results of Fourier analyses of temporal acoustic emission (AE) and light emission (LE) spectra. The experimental results were compared with the newly developed numerical model of keyhole dynamics. (The model is based on the assumption that the propagation of front part of keyhole into material is due to the melt ejection driven by laser induced surface evaporation.) The calculations predict that a high speed melt flow is induced at the front part of keyhole when the sample travel speed exceeds several 10mm/s. The numerical analysis also shows the hump formation on the front keyhole wall surface. Experimentally observed melt behavior and transformation of the AE and LE spectra with variation of welding speed are qualitatively in good agreement with the model predictions.

• Convergence Security Journal
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• v.17 no.2
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• pp.69-80
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• 2017

Due to the advanced IT environment, the role of Security Monitoring & Control becomes more important as the cyber-crime is becoming intelligent, diversified, and advanced. In contrast to the way it relied solely on security devices such as Firewall and IDS in the past, Security Monitoring & Control tasks responding to cyber attacks through real-time monitoring have become wide spread and their role is also important. In response to current cyber threats, since security equipment alone can not be guaranteed a stable defense, the task of Security Monitoring & Control became essential to operate and monitor security equipment and to respond in real time. In this study, we will discuss how to configure network security system effectively and how to improve the real-time Security Monitor & Control.

• Journal of Information Technology Applications and Management
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• v.12 no.2
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• pp.1-13
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• 2005

This paper proposes a software-reliability growth model incoporating the amount of testing effort expended during the software testing phase after developing it. The time-dependent behavior of testing effort expenditures is described by a Logistic curve. Assuming that the error detection rate to the amount of testing effort spent during the testing phase is proportional to the current error content, a software-reliability growth model is formulated by a nonhomogeneous Poisson process. Using this model the method of data analysis for software reliability measurement is developed. After defining a software reliability, This paper discusses the relations between testing time and reliability and between duration following failure fixing and reliability are studied. SRGM in several literatures has used the exponential curve, Railleigh curve or Weibull curve as an amount of testing effort during software testing phase. However, it might not be appropriate to represent the consumption curve for testing effort by one of already proposed curves in some software development environments. Therefore, this paper shows that a logistic testing-effort function can be adequately expressed as a software development/testing effort curve and that it gives a good predictive capability based on real failure data.