• Journal of the Korean Ceramic Society
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• v.48 no.2
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• pp.168-172
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• 2011

Alumina powder was added in a general porcelain (Backja) with clay, feldspar and quartz contents to promote the mullite ($3Al_2O_3{\cdot}2SiO_2$) generation in the porcelain. Low melting materials ($B_2O_3(450^{\circ}C)$, $MnO_3(940^{\circ}C)$, CuO($1080^{\circ}C$)) were doped at ~3 wt% to modify the sinterability of porcelain with a high alumina contents and promote the mullite generation. Green body was made by slip casting method with blended slurry and then, they were fired at $1280^{\circ}C$ for 1hr by a $2^{\circ}C/min$. Densifications of samples with high alumina contents (20~30 wt%) were impeded. As the doping contents of low melting materilas increased, the sinterability of samples was improved. The shrinkage rate and bulk density of samples were improved by doping with low melting materials. Mullite phase increased with increasing the low melting contents in the phase analyses. This means lots of alumina and quartz were transformed into mullite phase by low melting contents doping. In the results, high bending strength of samples with high alumina contents was accomplished by improving the densification and mullite generation in the porcelain.

• Transactions of the Korean Society of Mechanical Engineers
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• v.10 no.5
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• pp.713-723
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• 1986

The purpose of this research was to study the heat transfer characteristics of heat pipe which used non-metallic(SiO$_{2}$), circumferential wick and meshed slab wick as ADI method and experimental results. Compared wick experimental data and results by ADI method showed the good agreement and ADI method was utilized in pridicting the performance of heat pipe. Also, ADI method was applied to predict heat pipe performance according to the various volume ratios of metallic bond. The heat transfer characteristics of heat pipe could be predicted by heat flux and superheat term below the maximum heat flux limit. According to the addition ratio of metallic bond, heat transfer ratio could be improved as 2-3 times and when heat conductivity ratio(K$_{b}$/K$_{a}$) was increased at 4-12 ratio, heat transfer was in creased as 1.7-2.4 times, and the prediction of heat transfer could be show as exponential type. In producting non-metallic wick used to low heat pipe, metallic bond which is the conductivity of good quality and enduring for high temperature will be improved as in important problem.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.21 no.9
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• pp.1105-1114
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• 1997

The heat transfer characteristics of free surface water jet impinging normally against a flat uniform heat flux surface were investigated. This deals with the effect of three nozzle configurations (Cone type, Reverse cone type, Vertical circular type) on the local and the average heat transfer. Heat transfer measurements were made for water jet issuing from a nozzle of which exit diameter 8 mm. The experimental conditions investigated are Reynolds number range of 27000 ~ 70000( $V_{O}$=3 ~ 8 m/s), nozzle-to-target plate distances H/D=2 ~ 10, and radial distance from the stagnation point r/D ~ = 0 ~ 7.42. For all jet velocities of H/D=2, the local Nusselt number decreased monotonically with increasing radial distance. However, for H/D from 4 to 10, and for the jet velocity $V_{O}$.geq.7 m/s for Cone type nozzle and $V_{O}$.geq.6 m/s for the other type nozzles, the Nusselt number distributions exhibited secondary peaks at r/D=3 ~ 3.5. For Reverse cone type nozzle and Vertical circular nozzle, the maximum stagnation point heat transfer and the maximum average heat transfer occurs at H/D=8. But for the Cone type nozzle, the maximum stagnation and average heat transfer occurs at H/D=10, 4, respectively. From the optimum nozzle-to-target plate distance, the stagnation and the average heat transfer reveal the following ranking: Reverse cone type nozzle, Vertical circular type nozzle, Cone type nozzle.ozzle.

• Progress in Superconductivity
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• v.3 no.1
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• pp.78-82
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• 2001

The spatial resolution of $high-T_{c}$ scanning SQUID microscope is limited by the washer size of SQUID and the gap distance between SQUID sensor and the sample. In this work, we tried to improve the spatial resolution of scanning SQUID microscope by reducing the size of SQUID sensor fabricated with $YBa_2$$Cu_3$$O_{7}$ thin film. Outer dimensions of the SQUiDs we tested are 24 $\mu\textrm{m}$ $\times$ $ 28\mu\textrm{m}$, $12 \mu\textrm{m}$ $\times$ $16\mu\textrm{m}$, $12\mu\textrm{m}$ x $12\mu\textrm{m}$, $10 \mu\textrm{m}$ $\times$ $10 \mu\textrm{m}$ each. To operate them in the flux-locked loop scheme, we used a direct-coupled electronics instead of using conventional electronics involving a modulation scheme. Since the direct-coupled feedback scheme does not require modulation current adjustment that poses as a practical difficulty in the SQUID operation in modulation-scheme, the direct feedback operation is rather simpler than the conventional modulation method. The resulting noise features were dominated by the noise of preamp in FLL electronics except that of the largest SQUID. The noise levels of SQUIDs are expected below 1$\times$$10^{-5}$ $\Phi_{0}$H $z^{1}$2/ (at 300 Hz), that is a typical noise level for SQUID made of $YBa_2$C $u_3$$O_{7}$ thin film. The data acquisition and motion-controlling parts were also improved, resulting in faster data acquisition rate and less vibration of the system.m.

• Korean Journal of Crystallography
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• v.5 no.2
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• pp.93-99
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• 1994

Growth form and surface morphology of NYAB single crystal grown by TSSG technique using a K2O/3MoOS/0.5B203 flux was investigated. In the crystal grown from <100> or <120> seed, prismatic and (101) faces were well developed with different size each other. (001) face was also developed in the crystal grown from <001> seed. While growth hillocks were observed on the prismatic face of the crystal grown from <100> seed, surface striations parallel to neighbor (101) faces were formed on that face of the crystal grown from <001> seed. The (101) faces were grown by two dimensional nucleation growth. (001) face which was developed at slow growth velocity of [001] direction was grown by screw dislocation Anisotropy of growth velocity as to seed orientation affected on crystal morphology and surface morphology.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.12 no.6
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• pp.288-291
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• 2002

We developed a new RF indirect-heating LPE furnace. The thermal gradient of our newly developed furnace is less than that of direct heating, and is as gentle as that of the resistance-heating LPE furnace. With this new furnace, the heating and/or cooling is faster than that of the resistance-heating furnace. Impurity-doped YIG film was grown from a $PbO-B_{2}O_{3}$, based flux on a (111) GGG substrate. To study the effect of the impurities on the MSSW threshold power and the saturation response time, we used two microstrip lines to excite and propagate the MSSW at 1.9 GHz. The MSSW threshold power and saturation response time was found to be related to the $\Delta$H.

• Journal of Advanced Marine Engineering and Technology
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• v.23 no.2
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• pp.140-149
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• 1999

This study is on the development of the computer program that calculates a 3-D hull temperadistribution and analyzes BOR(Boil off rate) to be important to the heat design of a membrane type LNG carrier. The quarter of a tank is taken as an calculation model. And the thermal conductivity of insulation is assumed to be the function of a temperature. In the present steady state calculation, the temperature of LNG in a cargo tank is assumed to be -$162^{\circ}C$ and the air temperature of a cofferdam, to be +$5^{\circ}C$. The lowest air temperature in compartments is calculated as $21.39^{\circ}C$ under the USCG condition ($T_{air}=-18^{\circ}C,\;T_{sw}=O^{\circ}C)$ and B.O.R value is O.0977%/day under the maximum boil-off condition, IMO IGC ($T_{air}=45^{\circ}C,\;T_{sw}=32^{\circ}C$), which satisfies the requirement by KOGAS. The calculated temperature distribution over tank panels at each condition is maximum 3% less than GTT's results. From the results of this study, it can be concluded that the present design of LNG cargo tank satisfies the requirement by KOGAS.

• Journal of the Korean Ceramic Society
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• v.26 no.4
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• pp.459-470
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• 1989

Single crystals of rare-earth iron garnets were grown from solutions of molten lead oxide, lead fluoride, baric oxide, iron oxide, and the oxides of yttrium, samarium orgadolinium. The crystals were grown by slow cooling technique. A convenient composition was 41.8mol% PbO, 20.59mol% PbF2, 8.23mol% B2O3, 20.00mol% Fe2O3 and 10.00mol% R2O3 where R is Y, Sm or Gd. For this experiment, platinum crucibles of size 20, 30cc and a vertical siliconit tube furnace were used. The precipitation temperature of YIG was observed in the range of 115$0^{\circ}C$-112$0^{\circ}C$ and the optimum growth conditions in this experiment were determined. The nucleation rate was controlled by the holding time after the fast colling, the growth rate by the slow cooling conditiions. The form of the grown YIG crystals showed a combination of {110} and {211}, and the size of the crystals grown in this experiment was up to about 9mm under the conditions of holding time 16hour, cooling rate 2$^{\circ}C$/hr. and temperature range 115$0^{\circ}C$-90$0^{\circ}C$. The precipitatin temperature of SmIG was observed in the range of 105$0^{\circ}C$-98$0^{\circ}C$ and the size of the crystals grown in this experiment was up to about 5mm under the conditiions of holding time 16hours, cooling rate 2$^{\circ}C$/hr. and temperature range 100$0^{\circ}C$-80$0^{\circ}C$.

• Progress in Superconductivity
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• v.10 no.2
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• pp.87-91
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• 2009

Fluorine-doped $SmFeAsO_{1-x}F_x$ single crystals with the nominal value of x=0.2 were grown at $1350-1450^{\circ}C$ under the pressure of 3.3 GPa by using the self-flux method. Plate-shaped single crystals in the range of a few-150 ${\mu}m$ in their lateral size were obtained. The detailed crystal structure was analyzed by using the x-ray diffractometry. Superconducting transition temperature, determined by the resistive transition, of a single crystal was about 49 K with a narrow resistive transition width of ${\sim}1$ K. A relatively sharp transition, a low residual resistivity, and a large residual resistivity ratio compared with those reported for $REFeAsO_{1-x}F_x$(RE=Sm, Nd) single crystals indicate the high quality of our single crystals.

• Korean Journal of Materials Research
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• v.25 no.12
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• pp.694-702
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• 2015

Nd-Fe-B permanent magnets have been used in a wide variety of applications because of their high magnetic flux density. So, demand for neodymium has been increasing in worldwide. In this study, an electrowinning process was performed in $LiF-NdF_3-Nd_2O_3$ high temperature molten salts. However, a corrosion resistant material for use in the molten salt must be found for stable operation because of the harsh corrosion environment of the electrowinning process. Therefore, for this paper, boron nitride(BN), aluminum nitride(AlN), and silicon nitride($Si_3N_4$) were selected as protective and structural materials in the high temperature electrolyte. To investigate the characteristics of BN, AlN, and $Si_3N_4$, in molten salts, materials were immersed in the molten salts for 24, 72, 120, and 192 hours. Also, surface condition and stability were investigated by SEM and EDS and corrosion products were calculated by HSC chemistry. As a result, among BN, AlN, and $Si_3N_4$, AlN was found to show the best protective material properties.