• Journal of the Korean Society for Heat Treatment
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• v.20 no.6
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• pp.311-317
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• 2007

This study examined the phase changes, nitride precipitation and variation in mechanical properties of STS 304, STS 321 and STS 316L austenitic stainless steels after high temperature gas nitriding (HTGN) at temperature ranges from $1050^{\circ}C\;to\;1150^{\circ}C$. Fine round type of $Cr_2N$ nitrides were observed in the surface layers of 304 and 316L steels, even more in STS 321. Additionally, square type of TiN was found in STS 321 austenitic matrix too. As a result of many precipitates in the surface layer of the STS 321, it was seen $370{\sim}470Hv$ hardness variation depending on the HTGN treatment conditions, and interior region of austenite represented 150Hv. The surface hardness value of STS 304 and STS 316L showed $255{\sim}320Hv$, respectively. The nitrogen content was shown 0.27, 1.7 and 0.4% respectively at the surface layers of the STS 304, STS 321 and STS 316L. After the HTGN it was shown the improvement of corrosion resistance of the STS 321 and STS 316L compared with solution annealed steels in the solution of 1N $H_2SO_4$ whereas the STS 304 was not.

• Journal of Welding and Joining
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• v.15 no.5
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• pp.46-55
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• 1997

This study has evaluated the liquation cracking behavior in the heat affected zone of several Ni base superalloys (Incoloy 825, Inconel 718 and Inconel 600). 304 and 310S austenitic stainless steels were also included for comparison. In addition, the mechanism of liquation cracking in the HAZ was postulated based on the extensive microstructural examinations with SEM, EDAX and TEM. The liquation cracking resistance of Ni base alloys was found to be far inferior to that of austenitic stainless steels. The liquation cracking of Incoloy 825 and Inconel 718 was believed to be closely related with the Laves-austenite(Ti rich in 825 and Nb rich in 718) and MC-austenitic eutectic phases formed along the grain boundaries by constitutional liquation and incipient melting under rapid welding thermal contraction. Further, liquation cracking resistance of the HAZ was dependent not only upon the type and amount of low melting phases but also on the grain size.

• Transactions of the Korean Society of Pressure Vessels and Piping
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• v.20 no.1
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• pp.56-65
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• 2024

Cast austenitic stainless steels (CASS) and austenitic stainless steel weldments with a ferrite-austenite duplex structure are widely used in nuclear power plants, incorporating ferrite phase to enhance strength, stress relief, and corrosion resistance. Thermal aging at 290-325℃ can induce embrittlement, primarily due to spinodal decomposition and G-phase precipitation in the ferrite phase. This study evaluates the effects of thermal aging by collecting and analyzing various mechanical properties, such as Charpy impact energy, ferrite microhardness, and tensile strength, from various literature sources. Different model expressions, including hyperbolic tangent and phase transformation equations, are applied to calculate activation energy (Q) of room-temperature impact energies, and the results are compared. Additionally, predictive models for Q based on material composition are evaluated, and the potential of machine learning techniques for improving prediction accuracy is explored. The study also examines the use of ferrite microhardness and tensile strength in calculating Q and assessing thermal embrittlement. The findings provide insights for developing advanced prediction models for the thermal embrittlement behavior of CASS and the weldments of austenitic steels, contributing to the safety and reliability of nuclear power plant components.

• Journal of Powder Materials
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• v.16 no.2
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• pp.122-130
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• 2009

Austenitic oxide-dispersion-strengthened (ODS) stainless steel was fabricated using a wet mixing process without a mechanical milling in order to reduce contaminations of impurities during their fabrication process. Solution of yttrium nitrate was dried after a wet mixing with 316L stainless steel powder. Carbon and oxygen contents were effectively reduced by this wet processing. Microstructural analysis showed that coarse yttrium silicates of about 150 nm were formed in austenitic ODS steels with a silicon content of about 0.8 wt%. Wet-processed austenitic ODS steel without silicon showed higher yield strength by the presence of finer oxide of about 20 nm.

• Proceedings of the KWS Conference
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• 2002.10a
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• pp.211-216
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• 2002

To investigate transition region in welded overlay relating to disbonding crack, the effect of vanadium addition on disbonding of Cr-Mo steels overlay welded with austenitic stainless steel was studied. V modified Cr-Mo steels have a higher resistance to disbonding than V free Cr-Mo steel. One reason is due to the fact that fine vanadium carbide precipated in base metal traps hydrogen and thus decreases the susceptibility to the disbonding. The second is related to the higher stability of the vanadium and stable carbides formed during PWHT, in which the carbon diffusion to the interface is lower than for V free Cr-Mo steel. Decreasing the carbon content at the interface of the weld overlay shows good resistance to the disbonding. Hence, it is important to control the carbon content at the interface of the weld overlay.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2001.10a
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• pp.293-296
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• 2001

The dynamic softening mechanisms of AISI 316, AISI 304 and AISI 430 stainless steels were studied with torsion test in the temperature range of $900 - 1200^{\circ}C$ and the strain rate range of $5.0x10^{-2}-5.0x10^0/sec$. The austenitic stainless steels, such as AISI 316 and AISI 304 were softened by dynamic recrystallization (DRX) during hot deformation. Also, the evolutions of flow stress and microstructure of AISI 430 ferritic stainless steel show the characteristics of continuous dynamic recrystallization (CDRX). To establish the quantitative equations for DRX of AISI 316 stainless steel, the evolution of flow stress curve with strain was analyzed. The critical strain (${\varepsilon}_c$) and strain for maximum softening rate (${\varepsilon}^{*}$) could be confirmed by the analysis of work hardening rate ($d{\sigma}/d{\varepsilon}={\theta}$). The volume fraction of dynamic recrystallization ($X_{DRX}$) as a function of processing variables, such as strain rate ( $\varepsilon$ ), temperature (T), and strain ( $\varepsilon$ ) were established using the ${\epsilon}_c$ and ${\varepsilon}^{*}$. For the exact prediction the ${\varepsilon}_c,\;{\varepsilon}^{*}$ and Avrami' exponent (m') were quantitatively expressed by dimensionless parameter, Z/A, respectively. It was found that the calculated results were agreed with the experimental data for the steels at my deformation conditions. Also, we can reasonably conclude that the DRX, CDRX and grain refinement of stainless steels can be achieved by large strain deformation at high Z parameter condition.

• Korean Journal of Materials Research
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• v.19 no.7
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• pp.369-375
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• 2009

The spot weldability of dissimilar metal joints between stainless steels (AISI316) and interstitial free (IF) steels were investigated. This study was aimed to determine the spot welding parameters for a dissimilar metal joint and to evaluate the dissimilar metal joint's weldability, including its welding nugget shape, tensileshear strength, hardness, and microstructure. The fracture surface was investigated by using a Scanning Electron Microscopy (SEM). The experimental results showed that the shape of nugget was asymmetric, in which the fusion zone of the STS316 sheet was larger due to the higher bulk-resistance. The microstructure of the fusion zone was fully martensite. In order to evaluate the microstructure further, dilution of stainless steels were calculated and imposed onto the Schaeffler diagram. The predicted microstructure from the Schaeffler diagram was martensite. In order to confirm the predicted microstructure, XRD measurements were carried out. The results showed that that initial weld nugget was composed of austenite and martensite.

• Journal of Korean Society of Steel Construction
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• v.28 no.5
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• pp.303-312
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• 2016

Many researches on the application of stainless steels as structural steels have been performed thanks to their material properties such as superior ductility and corrosion resistance. Ferritic stainless steels(STS430) with little or no nickel have been used increasingly in building structure because it is inexpensive compared to austenitic stainless steels(STS304) with nickel, but provide performances similar to the austenitic stainless steel. This paper deals with block shear fracture behavior of base metal in stainless steel welded connection. Although the block shear fracture behavior for welded connection due to stress triaxiality is different from that of bolted connection, the block shear strength of welded connection in current design specifications has been predicted based on that of bolted connection. The main parameters are weld length and welding process(Arc and TIG welds). The ultimate strengths of TIG welded specimens were higher than those of arc welded specimens and current design predictions by AISC, EC3 etc. were compared with test strengths.

• 한국전기화학회:학술대회논문집
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• 2000.04a
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• pp.23-23
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• 2000

• 한국전기화학회:학술대회논문집
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• 2001.10a
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• pp.20-20
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• 2001