• Title/Summary/Keyword: Attrition milling

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Evaluation of Operational Conditions and Power Consumption of a Bioattritor for Enzymatic Saccharification of Uncooked Starch (무증자 전분당화용 분쇄마찰매체 함유 효소반응기의 조작조건과 동력소모의 검토)

  • 이용현;박진서
    • Microbiology and Biotechnology Letters
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    • v.17 no.4
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    • pp.349-357
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    • 1989
  • Uncooked starch can be effectively saccharified in an enzyme reaction system containing attrition-milling media. To develope the high efficiency bioattritor, an agitated bead type bioreactor was constructed, and its effectiveness was evaluated. The optimal operation condition of bioattritor was found to be 300 g glass bead/L, 200 rpm, standard type impeller for 220 g/L of uncooked corn starch. The torque under the various operational conditions were also measured. The interrelation-ship between energy consumption for agitation of attrition-milling media and enhanced extent of saccharification of uncooked starch was evaluated, Power consumption was measured to be around 1.53 watt/L under the optimal operation condition. The attrition coupled enzyme reaction system is identified to tie a very excellent energy saying process for saccharification of uncooked starch, and seems to have a bright prospect of industrial application.

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Enhancing mechanism of the saccharification of uncooked starch in an agitated bead reaction system (무증자전분의 분쇄마찰매체에 의한 효소당화촉진 Mechanism의 규명)

  • 조구형;이용현
    • Microbiology and Biotechnology Letters
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    • v.14 no.5
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    • pp.407-413
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    • 1986
  • In an agitated bead reaction system, the enzymatic saccharification of uncooked starch was substantially enhanced. The enhancement mechanism was investigated front the view of the structural aspect of starch. The mechanical impact caused by the movement of the attrition-milling media resulted neither the destruction of microcrystalline structure nor the fragmentation of starch granule. instead, the most distinct phenomenon was the swelling of starch granule up to about 2.5 times, and the swelling mechanism was not similar with that caused by cooking. However, in the case of the enzyme addition in the attrition coupled reaction system, the swollen starch was easily fragmented into the large number of small particles by the synergistic action of the enzyme and milling-media. The exposed surface area of the fragmented particles plays the major role in enhancing the saccharification. The saccharification rate was quite different depending on the source of starch, the reason was discussed in terms of the granular structure of uncooked starches.

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Synthesis of Nano Size $BaCeO_3$ as an Effective Flux Pining Center for YBCO Superconductor (YBCO 초전도체의 효과적인 플럭스 피닝 센터로서의 나노 크기 $BaCeO_3$ 합성)

  • Youn, J.S.;No, K.S.;Kim, Y.H.;Jun, B.H.;Lee, J.P.;Jung, S.Y.;Kim, C.J.
    • Progress in Superconductivity
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    • v.10 no.1
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    • pp.12-16
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    • 2008
  • In this work, nano size $BaCeO_3$, which is a possible flux pinning medium of melt processed $YBa_{2}Cu_{3}O_x$ superconductor, was synthesized by the conventional solid state reaction method using powders. $BaCeO_3$ and $CeO_2$ were mixed thoroughly using a ball milling for 24 hours and calcined at $1200^{\circ}C$ for 5 hours for the formation $BaCeO_3$ powder. The obtained $BaCeO_3$ powder was attrition milled at various milling times of 60 min, 120 min and 240 min. The $BaCeO_3$ powders of various milling times were mixed with $YBa_{2}Cu_{3}O_x$ powder. Seed melt processed $YBa_{2}Cu_{3}O_x$-$BaCeO_3$ (15wt.%) superconductors were prepared and the superconducting properties were investigated. It was found that $T_c$ of $Y_{1.5}Ba_{2}Cu_{3}O_x$ samples was not significantly affected by $BaCeO_3$ addition, but $J_c$ of samples was increased by $BaCeO_3$ addition. The $J_c$ improvement by fine $BaCeO_3$ powder (120 min attrition-milled) was effective at low magnetic fields less than 2 T.

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Formation Behaviour Al-Ti Intermetallic Compounds by Ball milling methods (볼 밀링에 의한 Al-Ti 계 금속간화합물 생성 거동)

  • 안인섭
    • Journal of Powder Materials
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    • v.6 no.1
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    • pp.42-48
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    • 1999
  • Three mixtures of elemental powders of Al-25at.%Ti, 48at.%Ti and 70at.%Ti were offered to ball milling process for the formation of intermetallic compounds of $Al_3Ti$, AlTi and $Ti_3Al$. Ballmilling or attrition process were carried out at the condition of rotaing speed of 110 or 350 rpm at $10^{-3}$ torr vacuum or argon atmospheres. $Al_3Ti$phases were fully obtained by heat treatment for 1 hors at $600^{\circ}C$ with Al-25at.%Ti composition mixtures milled by 100 hours. The amorphous phase was completely formed at the composition of Al-48at.%Ti mixed powders by milling 100hours at the 50 to 1 weight ratio of ball to powder, and AlTi compounds were obtained by heat treament. In the case of Al-70at%Ti mixed powders milled for 100 hours, $Ti_3Al$ and $Al_3Ti$intermetallic compounds were formed by heat treatment for 1 hour at $600^{\circ}C$. By attrition milling of 350rpm for 10 hours, $Ti_3Al$ phase was formed completley after heat treatment for 1 hour at $600^{\circ}C$.

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Analysis of Attrition Rate of Y2O3 Stabilized Zirconia Beads with Different Microstructure and Mechanical Properties (고에너지 분쇄 매체 지르코니아 Beads의 미세구조 및 기계적 특성에 따른 마모율 분석)

  • Kim, Jung-Hwan;Yoon, Sae-Jung;Hahn, Byung-Dong;Ahn, Cheol-Woo;Yoon, Woon-Ha;Choi, Jong-Jin
    • Korean Journal of Materials Research
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    • v.28 no.6
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    • pp.349-354
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    • 2018
  • Particle size reduction is an important step in many technological operations. The process itself is defined as the mechanical breakdown of solids into smaller particles to increase the surface area and induce defects in solids, which are needed for subsequent operations such as chemical reactions. To fabricate nano-sized particles, several tens to hundreds of micron size ceramic beads, formed through high energy milling process, are required. To minimize the contamination effects during high-energy milling, the mechanical properties of zirconia beads are very important. Generally, the mechanical properties of $Y_2O_3$ stabilized tetragonal zirconia beads are closely related to the mechanism of phase change from tetragonal to monoclinic phase via external mechanical forces. Therefore, $Y_2O_3$ distribution in the sintered zirconia beads must also be closely related with the mechanical properties of the beads. In this work, commercially available $100{\mu}m-size$ beads are analyzed from the point of view of microstructure, composition homogeneity (especially for $Y_2O_3$), mechanical properties, and attrition rate.

Microwave Absorbing Properties of Fe-Si-Al Alloy Flaky Powder-Rubber Composites (Fe-Si-Al 합금 분말 · 고무 복합 자성체의 전파 흡수 특성)

  • Lee Kyung-Sub;Yoon Yeo-Choon;Choi Gwang-Bo;Kim Sung-Soo;Lee Jun-Young
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.16 no.2 s.93
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    • pp.228-234
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    • 2005
  • A magnetic composite as noise absorber of quasi-microwave band was developed. The Fe-Si-Al alloy powder were forged by attrition mill to get flaky shape. The magnetic composite sheet was fabricated in which powders are dispersed in polymer and aligned in the direction perpendicular to electromagnetic wave propagation. The permittivity of magnetic composite is increased as forging time increasing, while the permeability is decreased slightly. The maximum attenuation peak of reflection loss is shifted to lower fiequency range as milling time increasing, and the value of maximum attenuation peak is to get smaller gradually. From these result, we could designed a noise absorber sheet (t=1.0 mm) for quasi-microwave band, which is impedance matched at 1.4 GHz with respect to -8.2 dB reflection 1055.