• 제목/요약/키워드: Atomized powder

검색결과 142건 처리시간 0.033초

Spark Plasma Sintering에 의한 가스분무 Mg-Zn-Y 합금분말의 성형특성 (Consolidation Behavior of Gas Atomized Mg-Zn-Y Alloy Powders by Spark Plasma Sintering)

  • 이진규;김택수;배정찬
    • 한국분말재료학회지
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    • 제14권2호
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    • pp.140-144
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    • 2007
  • Using Spark Plasma Sintering process (SPS), consolidation behavior of gas atomized $Mg_{97}Zn_1Y_2$ alloys were investigated via examining the microstructure and evaluating the mechanical properties. In the atomized ahoy powders, fine $Mg_{12}YZn$ particles were homogeneously distributed in the ${\alpha}-Mg$ matrix. The phase distribution was maintained even after SPS at 723 K, although $Mg_{24}Y_5$ particles were newly precipitated by consolidating at 748 K. The density of the consolidated bulk Mg-Zn-Y alloy was $1.86g/cm^3$. The ultimate tensile strength (UTS) and elongation were varied with the consolidation temperature.

Phase Stability Studies of Unirradiated Al-U-10wt.%Mo Fuel at Elevated Temperature

  • Kim, Ki-Hwan;Jang, Se-Jung;Hyun suk Ahn;Park, Jong-Man;Kim, Chang-Kyu;Sohn, Dong-Seong
    • 한국원자력학회:학술대회논문집
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    • 한국원자력학회 1998년도 춘계학술발표회논문집(2)
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    • pp.273-278
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    • 1998
  • The phase stability of atomized U-10wt. %Mo powder and the thermal compatibility of dispersed fuel meats at 40$0^{\circ}C$ and 50$0^{\circ}C$ have been characterized. Atomized U-10Mo powder has a good \ulcorner-U phase stability, and excellent thermal compatibility with aluminum matrix in a dispersion fuel. It is thought that the good phase stability is related to th large supersaturation of Mo atoms in the atomized particles. The reasons for the excellent thermal compatibility have been considered to be as follows. Before thermal decomposition of ${\gamma}$-U in particle, supersaturated Mo atoms at ${\gamma}$-U grain boundaries inhibit the diffusion of Al atoms. After thermal decomposition of ${\gamma}$-U into ${\gamma}$-U and U$_2$Mo, the intermetallic compound of U$_2$Mo seems to retard the penetration of Al atoms. The penetration mechanisms of aluminum atoms in the atomized particles are assumed be classified as (a) diffusion through the reacted layer between fuel particles and Al matrix leaving a kernel-like unreacted island and (b) diffusion along grain boundaries showing several unreacted islands and more reacted regions.

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가스분무 Mg-Zn-Y 합금분말 및 압출재의 특성 (Materials Properties of Gas Atomized and Extruded Mg-Zn-Y Alloys)

  • 채홍준;이진규;배정찬;김택수
    • 한국분말재료학회지
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    • 제13권6호
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    • pp.427-431
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    • 2006
  • Mg-4.3Zn-0.7Y (at%) alloy powders were prepared using an industrial scale gas atomizer, followed by warm extrusion. The powders were almost spherical in shape. The microstructure of atomized powders and those extruded bars was examined using Scanning Electron Microscopy (SEM), Energy Dispersive X-ray Spectroscope (EDS) and X-ray Diffractometer (XRD). The grain size of the powders was coarsen as the initial powder size increased. After the extrusion, the grain size became fine due to the severe plastic deformation during the extrusion with the ratio of 10:1. Both the ultimate strength and elongation were enhanced with the decrease of initial particle size.

수분무 STS 316L 분말사출성형체의 탈지 및 소결공정에 따른 인장 특성 (Effect of Debinding and Sintering Conditions on the Tensile Properties of Water-atomized STS 316 L Parts by Powder Injection Molding)

  • 윤태식;성환진;안상호;이종수
    • 한국분말재료학회지
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    • 제9권4호
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    • pp.218-226
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    • 2002
  • The purpose of the present study is to investigate the influence of thermal debinding and sintering conditions on the sintering behavior and mechanical properties of PIMed 316L stainless steel. The water atomized powders were mixed with multi-component wax-base binder system, injection molded into flat tensile specimens. Binder was removed by solvent immersion method followed by thermal debinding, which was carried out in air and hydrogen atmospheres. Sintering was done in hydrogen for 1 hour at temperatures ranging from 1000℃ to 1350℃ The weight loss, residual carbon and oxygen contents were monitored at each stage of debinding and sintering processes. Tensile properties of the sintered specimen varied depending on the densification and the characteristics of the grain boundaries, which includes the pore morphology and residual oxides at the boundaries. The sinter density, tensile strength (UTS), and elongation to fracture of the optimized specimen were 95%, 540 MPa, and 53%, respectively.

방전플라즈마 소결법으로 제작된 순 마그네슘 분말 소결체의 특성평가 (Characteristics of Pure Mg Powder Compacts Prepared by Spark Plasma Sintering Process)

  • 홍지민;손현택;장세훈;이재설;차용훈;오익현
    • 한국재료학회지
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    • 제17권6호
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    • pp.331-336
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    • 2007
  • The pure Mg powder compacts were successfully fabricated using SPS process. The machined chip powder showed flake shaped morphology with coarse surfaces, while gas atomized powders were spherical in morphology with smooth surfaces. In this study, SPS process was used to consolidate the pure Mg powder because this process allows high density consolidation in a short time. The results showed that increased sintering temperature from $350^{\circ}C$ to $500^{\circ}C$ with pressure of 30MPa, the maximum values of the density was increased from 98.1% to 99.8% of theoretical density, respectively. However, density of the sintered chip powders was higher than that of gas-atomized powder due to larger contact areas between particles.

A Comparative Study of Mechanical Property in Al-8Fe-2Mo-2V-1Zr Bulk Alloys Fabricated from an Atomized Powder and a Melt Spun Ribbon

  • Jung, T.K.;Sung, T.J.;Kim, M.S.;Kim, W.Y.
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.1023-1024
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    • 2006
  • Al-8Fe-2Mo-2V-1Zr alloys were prepared by the gas atomization/hot extrusion and the melt spinning/hot extrusion. For the gas atomized and extruded alloy, equiaxed grains with the average size of 400 nm and finely distributed dispersoids with their particle sizes ranging from 50nm to 200nm were observed. For the melt spun and hot extrusion processed alloy, refined microstructural feature consisting of equiaxed grains with the average size of 200nm and fine dispersoids with their particle sizes under 50nm appeared to exhibit a difference in microstructure. Strength of the latter alloy was higher than that for the former alloy up to elevated temperatures.

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DEVELOPMENT OF HIGH-DENSITY U/AL DISPERSION PLATES FOR MO-99 PRODUCTION USING ATOMIZED URANIUM POWDER

  • Ryu, Ho Jin;Kim, Chang Kyu;Sim, Moonsoo;Park, Jong Man;Lee, Jong Hyun
    • Nuclear Engineering and Technology
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    • 제45권7호
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    • pp.979-986
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    • 2013
  • Uranium metal particle dispersion plates have been proposed as targets for Molybdenum-99 (Mo-99) production to improve the radioisotope production efficiency of conventional low enriched uranium targets. In this study, uranium powder was produced by centrifugal atomization, and miniature target plates containing uranium particles in an aluminum matrix with uranium densities up to 9 $g-U/cm^3$ were fabricated. Additional heat treatment was applied to convert the uranium particles into UAlx compounds by a chemical reaction of the uranium particles and aluminum matrix. Thus, these target plates can be treated with the same alkaline dissolution process that is used for conventional $UAl_x$ dispersion targets, while increasing the uranium density in the target plates.