• 보존과학연구
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• s.27
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• pp.203-214
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• 2006

The work focuses on the chemical analysis of organic residues in archaeological soils. Particularly, the detection of manuring in archaeological soils can provide important information concerning early human behavior, diet, parasites, ecological adeptation. In this study, archaeological soils excavated at bunto-ri, Haenam and kumjang-ri, Kyungju were used to assess the possibility as indicators of ancient human activity in archaeological areas. The sampled soils were analyzed soil color, pH for their physical and chemical properties and GC/MSD to detect and quantify specific compound. The results showed that the sampled soils were normal pH(6.8~7.2) and soil color of light brown to yellowish brown. Also, the result from the GC/MS analysis indicated that their compounds were hexadecanoic acid, octadecanoic acid, nonadecane, docosanoic acid, methyl ester, teracosanoic acidand methyl este from bunto-ri site and 1-heptadecene, cyclotetracosane, tetracosane, cyclotetracosane,1-docosene, n-nonadecane, tetracosanoic acid methyl ester, cyclooctacosane, 1-nonadecene, eicosane, cyclotriacontane from kumjang-ri site. These compounds are not only normal soil materials but also animal lipid compounds. And the more scientific analysis of the soils will solve a curiosity for artificially incoming.

• Parasites, Hosts and Diseases
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• v.51 no.4
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• pp.489-492
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• 2013

A paleoparasitological survey to detect helminth eggs was performed in archaeological sites of Jeolla-do and Jeju-do, the Republic of Korea. Total 593 soil samples were collected in 12 sites of Jeolla-do and 5 sites of Jeju-do from April to November 2011, and examined by the methods of Pike and coworkers. A total of 4 helminth eggs, 2 eggs each for Trichuris trichiura and Ascaris sp., were found in soil samples from 1 site, in Hyangyang-ri, Jangheung-eup, Jangheung-gun, Jeollanam-do. The egg-recovery layer was presumed to represent a 19th century farm, which fact suggested the use of human manures. This is the third archaeological discovery of parasite eggs in Jeolla-do. Additionally, no helminth eggs in archaeological sites of Jeju-do is an interesting problem to be solved in the further investigations.

• The Journal of the Korea Contents Association
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• v.8 no.12
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• pp.214-221
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• 2008

Terrestrial magnetism has left traces through residues such as fossils of the terrestrial magnetism as time went by. An analysis of archaeological terrestrial magnetism is an estimation of dates of archaeological remains where baked earth is exposed by measuring the change of the past terrestrial magnetism through thermo-remnant magnetization of baked earth. This paper attempts to apply an analysis of the archaeological terrestrial magnetism to archaeological remains using fourteen soil samples extracted from a charcoal kiln with side window located at the Area Ⅰ of Maegokdong. The date of A.D.440${\pm}$15 the analysis of archaeological terrestrial magnetism came up with gives solid evidence, while an archeological chronicle used arrangements of surrounding artifacts because of the absence of remains and assumed uncertainly that a charcoal kiln with side window was from the three kingdom periods. This analysis of archaeological terrestrial magnetism has come to anchor as a main natural scientific analysis because it relatively easily removes pollutants and comes up with highly reliable results owing to its considerably narrow error tolerance of assumed dates.

• Korean Journal of Heritage: History & Science
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• v.40
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• pp.413-430
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• 2007

This study analyzed the foreign substances in waterlogged archaeological woods and compounds in soil where waterlogged archaeological wood was buried, in order to examine the relationship between burial environment and foreign substances in waterlogged archaeological wood. The XRF(X-ray Fluorescence Spectroscopy) and EDX(Energy Dispersive X-ray) analysis were conducted to examine the effect of iron(Fe) to blacken the waterlogged wood. The XRF results showed that investigated soil contained Si, Al, and Fe. Wood ash contained more sulfur and Fe than any other elements in the EDX analysis. Cellulose and hemicellulose were significantly reduced at the surface of wood, which is the blackened part of waterlogged wood. Foreign substances changed the surface color. These problems could be solved by removal of foreign substances in waterlogged archaeological wood using EDTA(Ethylene Diamine Tetra Acetic acid). The optimum condition to remove Fe from waterlogged wood by EDTA was investigated. To do this, the concentration of Fe removed was measured with various concentration of EDTA-2Na. The optimum pH of EDTA-2Na was figured to be 4.1 to 4.3. As the concentration of EDTA increased, the extracted concentration of Fe also increased. In the case of 0.4 wt% of EDTA-2Na, about 60ppm of Fe was eliminated and was stabilized after 48 hours. In the case of EDTA-3Na, the optimum pH was 7 to 8, and about 10 ppm of Fe was eliminated at 0.4 wt% of EDTA-3Na. In the case of EDTA-4Na, the optimum pH was 10 to 11, and about 20 ppm of Fe was eliminated at 0.4 wt% of EDTA-4Na. In conclusion, the iron(Fe) in waterlogged archaeological wood was removed by EDTA treatment and it increased the whiteness of the surface.

• Journal of Conservation Science
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• v.27 no.3
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• pp.291-300
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• 2011

Archaeomagnetic dating method is used to assign a date to the archaeological remains in which burnt soil is found by measuring the changes in terrestrial magnetism with the thermal remanent magnetization retained in burnt soil. This method, in particular, is quite useful to determine an age of the archaeological remains in which no properties are found, which makes it difficult to assigning a date. Hemp kiln and lime kiln fall under remains of these features, and 21 and 5 archaeomagnetic data from both kilns respectively were obtained by measuring the- remanent magnetization in burnt soil samples that are extracted in hemp kilns and lime kilns in the country. The results of archaeomagnetic dating with these data show the age range of the hemp kilns is between the late 10th century A.D. and the middle of the 19th century, and that of the lime kilns is between the early 16th century A.D. and the middle of the 18th century. The factor that the number of data collected from the hemp kilns was comparatively more than those from the lime kilns might affect the result, however corresponding to the fact that hemp had been used for a long period of time, the period of hemp kiln are widely spread over the chronological table. And the archaeomagnetic dating of lime kiln, in view of archaeological periods, is not only in accord with the late Joseon period when the tombs with lime-soil mixture barrier in trend; this is also telling that its width of archaeological period is comparatively narrow.

• 보존과학연구
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• s.26
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• pp.103-126
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• 2005

Coprostanol is a metabolic product of cholesterol, formed by microbial action in the mammalian gut. This chemical compound is the major sterol in human and has been routinely studied as a biomarker of sewage pollution in marine and lacustrinesediments. This has led to the search for coprostanol as a biomarker in archaeologicalsoils, in order to detect the presence of fecal material. In this study, five samples of archaeological soils excavated at Wanggung ri, Iksancity, were used to assess the possibility of using coprostanol as indicators of ancient human activity in archaeological areas. The sampled soils were analyzed MXRD,EDXRF for their physical and chemical properties. And coprostanol was analysed byGC/MSD, using SIM method to detect and quantify specific compound. The results showed the soils were composed of quartz and feldspars, inorganicelement such as $SiO_2$, $Al_2O_3$, $Fe_2O_3$ etc. Moreover, the result from the analysis wasindicated that the specific compound is coprostanol. The coprostanol was determined at $0.16~1.01\mug$/g in the range of concentrations. This finding indicate that clear promise exists for the exploitation of coprostanol as biomarker of ancient human activity inarchaeological survey. Therefore such studies can serve to increase the confidence we place on biomarker-based methodologies for assessing fecal pollution. The application of this methodology has proved a simple and effective way of searching for that pattern in successively more aged deposits either known or suspected to contain fecal material. And the more scientific analysis of the soils will be showed to utility of the area ancient dietary life style, ancient environment.

• Journal of Conservation Science
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• v.33 no.3
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• pp.181-188
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• 2017

A total of 16 precious archaeomagnetic dating data were obtained from various historic sites including fired soils from eight archaeological sites on Jeju Island. We researched the measurement results of 12 pieces of data from before the Common Era (BCE), and four pieces of data from after the Common Era. First, the BCE data could be divided into three groups (A, B, and C) based on the difference in the archaeomagnetic data. By comparing the data accumulated in other parts of Korea and referring to the archaeological years, the order of the groups was as follows: A group (Bronze Age~Early Iron Age) ${\rightarrow}$ B group (Early Iron Age when the circular rim eomtodae pottery was excavated) ${\rightarrow}$ C group (Early Iron Age when triangulated rim jeomtodae pottery was excavated), with A group being the earliest data group and C group being the latest data group. In addition, the data after the Common Era could be used to determine the archaeomagnetic dating of the archaeological sites. Through the archaeomagnetic dating of Jeju's archaeological sites for the BCE period, the relative order of the relics was determined, and for the period after the Common Era, the absolute age of the historic sites was obtained. They are expected to be used diversely in the chronological study of Jeju.

• The Korean Journal of Quaternary Research
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• v.25 no.1
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• pp.31-39
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• 2011

Phytolith of soil in earthenware buried in the wooden chamber tombs at the archaeological site in Hwangseong-dong, Gyeongju along Hyeongsan River are analyzed. The study area has adjoined the seat of government during approximately thousand years in Shilla Dynasty and can be regarded as being closely related to the agricultural activities using the floodplains of Hyeongsan River. By the analytical results, Phragmites, Paniceae and Andropogoneae as well as Oryza sativa are found in the lower horizons, indicating the agricultural activities in the nearby areas. It is suggested for understanding the use of earthenware that the comparisons of buried soils in the site and soils in the earthenware and analysis on the macro plant fossils of soil in the earthenware are needed.

• Journal of Conservation Science
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• v.19
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• pp.19-30
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• 2006

Alteration of physical and chemical characteristics and the effect of removal of mineral substances in waterlogged archaeological woods by different cleaning processes were examined using oak wood(Quercus spp.) that was excavated from wetland near Gwangju, Korea. Cleaning methods employed in the present work were (1) tools, (2) deaeration, (3) EDTA and (4) ultrasonic cleaning, which are being currently applied in the field of preservation treatment. Cleaning process were performed independently or continuously. Composition of mineral substances in the waterlogged archaeological wood was almost same as the that of soil in which waterlogged archaeological woods were buried. In case of independent cleaning, tools cleaning efficiently removed the mineral substances on surface. Surface color become brighter after cleaning with EDTA. In contrast, deaeration and ultrasonic cleaning did not show any significant removal of mineral substances. In continuous cleaning process, tool cleaning as the first step treatment showed the same effect as shown in independent cleaning. Although deaeration as the second step cleaning did not remove the mineral substances, it could be assumed to contribute the infiltration of dimensional agents by homogenization of wood. EDTA treatment (the third step cleaning) removed the iron(Fe) and increased the whiteness of wood color. The ultrasonic treatment (the fourth step cleaning) removed the sodium(Na) remained after EDTA treatment and the fine mineral substances.

• 한국문화재보존과학회:학술대회논문집
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• 2005.03a
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• pp.165-166
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• 2005