• 한국정보디스플레이학회:학술대회논문집
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• 한국정보디스플레이학회 2002년도 International Meeting on Information Display
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• pp.697-700
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• 2002

Porous anodic aluminum oxide(AAO) templates prepared by anodizing method were used for growing multiwalled carbon nanotubes(CNTs). AAO templates with the homogeneous pore diameter and length were obtained by two step anodizing technique. Using AAO templates, vertically well-ordered two-dimensional carbon nanotube arrays were fabricated. We investigated the field emission property of CNTs grown using different catalyst metals in vacuum chamber (<$10^{-7}$ Torr) on AAO Template. To explain the different emission property, the surface reaction between catalysts and alumina pores which inserted carbon species of $C_2H_2$ using High resolution transmission electron microscopy (HRTEM) was studied.

• 한국표면공학회지
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• 제43권5호
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• pp.243-247
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• 2010

The micro Vickers hardness and internal stress of Ni-Fe metal thin film synthesized by electrodeposition method at $25^{\circ}C$ were studied as a function of bath composition, and surface microstructure and atomic compositions of thin films were investigated by SEM and EDS. And the shape change of $200\;{\AA}$ Ni-Fe nanowires made using anodic aluminum oxide(AAO) templates by electrodeposition method were observed by SEM as a function of ultrasonic treatment time and bath composition. The Fe deposition contents on the substrate non-linearly increased with Fe ion concentration over total metal ion concentration. In case of low Fe contents film, the grain size is smaller and denser than high Fe contents deposited films, and the micro Vickers hardness increased with Fe contents of electrodeposited films. These results affected the shape change of nanowire after ultrasonic treatments.

• 한국표면공학회지
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• 제51권1호
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• pp.21-26
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• 2018

The $Cu_2(btc)_3$ metal-organic frameworks (MOF) coated anodic aluminum oxide (AAO) membrane was successfully prepared by layer-by-layer technique using hand spray method. It was confirmed that the $Cu_2(btc)_3$ layer, which has the pore sized in 2-3 nm, on surface of AAO exhibited the polycrystalline thin film structure by XRD analysis. More than 100 repetitive spray cycles were required to obtain more robust and thick MOFs on AAO and it was possible to uniformly coat both the top and bottom surfaces of the AAO. It should be noted that the MOFs also could be coated on surface of pores resulting in reduce the size of pore from 52 nm to 32 nm.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2018년도 춘계학술대회 논문집
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• pp.92.1-92.1
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• 2018

표면증강 라만 산란(Surface Enhancement Raman Scattering, SERS) 기판의 경우, 규칙적인 배열을 갖는 나노구조 및 나노패턴 기판과 금속 나노구조의 고밀도 패킹이 고감도 화학물질 검출에 중요하다. 또한 폭넓은 응용 가능성에도 불구하고 기판 제작의 비용이 높고 재현성이 떨어져 상용화에 어려움을 겪고 있다. 본 연구에서는 다공성 알루미나(Anodic Aluminum Oxide, AAO)를 사용하여 Ag 나노입자가 코팅된 나노기둥 배열(Nanopillar array)을 갖는 고분자 필름의 SERS-active 기판을 제작하여 공정비용을 낮추고, 대면적화로 생산성을 높이고자 한다. 다단계 양극산화 공정과 복제 기술을 통해 다양한 지름과 높이를 갖는 맥주병 형상의 나노기둥 배열을 제조하였고, aspect ratio가 2.3인 나노기둥 배열에서 최대의 SERS 신호 강도와 높은 재현성을 확인하였다. SERS 신호의 세기는 Ag 나노입자가 코팅된 나노기둥 배열의 열처리 온도와 분석 물질의 농도에 따라 비례하며 이를 바탕으로 정량적인 고감도 진단, 바이오 화학 물질 센서에 매우 적합함을 알 수 있다.

• Journal of Magnetics
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• 제16권4호
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• pp.413-416
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• 2011

An array of FeCo nanotubes has been successfully fabricated in the pores of porous anodic aluminum oxide (AAO) templates by wetting templates method. The morphology and structure of the nanotube array were characterized by scanning electron microscopy, transmission electron microscopy and x-ray diffraction. The average diameter of the nanotubes was about 200 nm, and the length was more than 10 ${\mu}m$. Vibrating sample magnetometer and superconducting quantum interference device were used to investigate the magnetic properties of the nanotube array. Interaction between the nanotubes has been found to be demagnetizing as expected and the switching field distribution is broad.

• Bulletin of the Korean Chemical Society
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• 제29권4호
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• pp.758-760
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• 2008

Nanoporous AAO (Anodic Aluminum Oxide) membranes have many advantages as a template for variety of magnetic materials. Materials can be embedded into the pores by electrodeposition, sputtering or magnetic-field-assisted infiltration of magnetic nanoparticles. This work focuses on the fabrication of the magnetic structures in the AAO templates by electrodeposition. Our method allows the controlled growth of Co nanostructures within the porous alumina membrane in the form of dots, rods and long wires. The shape of Co nanostructures has been investigated by field emission scanning electron microscope (FESEM). The magnetic hysteresis loops of Co nanostructures were measured using SQUID at 5 K and 300 K. The magnetic properties of the Co nanostructures are proportional to their aspect ratios and can be controlled by changing the aspect ratios.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2016년도 추계학술대회 논문집
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• pp.115.2-115.2
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• 2016

Al alloys are being used widely for automobile, aerospace and mechanical components because of their high strength ratio to weight. However, still they suffer from abrasion or corrosion owing to insufficient resistances to friction or mechanical impact and chemical attack. Plasma electrolytic oxidation (PEO) method is one of the promising surface treatment methods for Al alloys which can render better hardness than aluminum anodic oxide (AAO) films prepared by conventional anodizing method in acidic solutions. In this presentation, some basic nature of PEO film formation and growth process on Al alloys will be presented based on the experimental results obtained and discussed in view of dielectric breakdown and reformation and the role of various anions in film breakdown and reformation of PEO films.

• Bulletin of the Korean Chemical Society
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• 제30권5호
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• pp.1131-1134
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• 2009

Preparation of graded materials displaying gradients of desired properties is one of the important issues and less-developed areas in materials chemistry. For the first time we demonstrate facile control of porosity and length in the pores of AAO template in lateral directions by controlled dipping method. To demonstrate the versatility of the proposed method, laterally graded silica nanotubes are also prepared by using the laterally graded AAO templates. The method demonstrated here will open numerous possibilities for obtaining a variety of graded materials with lateral gradients of catalytic, electrochemical, mechanical and optical properties on the nanoscale.

• Bulletin of the Korean Chemical Society
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• 제33권12호
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• pp.4165-4168
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• 2012

Magnetic fluorescent silica nanotubes were fabricated using reverse micro-emulsions coupled with conventional sol-gel methods. Anodic aluminum oxide templates were used to separate spatially the magnetic and the fluorescent moieties on individual nanotubes and so prevent quenching of the fluorescence. C18 and fluorescent layers were deposited sequentially on silica. Magnetism was then obtained by the introduction of pre-made magnetic nanoparticles inside the nanotubes. The photo- and chemical stabilities of nanotubes were demonstrated through dye release and photobleaching tests. The produced nanotubes did not show fluorescence quenching upon the addition of the nanoparticles, an advantage over conventional spherical fluorescent magnetic nanoparticles. High photostability of nanotubes, magnetism and biocompatiblily make them potentially useful in bioanalysis.

• KSBB Journal
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• 제27권1호
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• pp.45-50
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• 2012

In this paper, we investigated the effect of nanostructure on the cell behaviors such as adhesion and growth rate. Nanoporous structures with various diameters (30, 40, 45, 50, 60 nm) and 500 nm of the depth were fabricated using the anodizing method. The water contact angle of the surface consisting of nanopores with 30 nm diameter was 40 degree and those were 60~70 degree in cases of nanopores with over 40 nm diameter. Hela cells were cultivated on various nanoporous structure surface to investigate the cell behavior on nanostructure. As a result, Hela cells preferred 30 nm diameter nanoporous surface that has lower water contact angle. This result was confirmed by protein adsorption experiment and scanning electron microscope investigation.