• 제목/요약/키워드: Analytical Quality Control

검색결과 341건 처리시간 0.034초

Pareto Optimized EDCA Parameter Control for Wireless Local Area Networks

  • Kim, Minseok;Oh, Wui Hwan;Chung, Jong-Moon;Lee, Bong Gyou;Seo, Myunghwan;Kim, Jung-Sik;Cho, Hyung-Weon
    • KSII Transactions on Internet and Information Systems (TIIS)
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    • 제8권10호
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    • pp.3458-3474
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    • 2014
  • The performance of IEEE 802.11e enhanced distributed channel access (EDCA) is influenced by several interactive parameters that make quality of service (QoS) control complex and difficult. In EDCA, the most critical performance influencing parameters are the arbitration interframe space (AIFS) and contention window size (CW) of each access category (AC). The objective of this paper is to provide a scheme for parameter control such that the throughput per station as well as the overall system throughput of the network is maximized and controllable. For this purpose, a simple and accurate analytical model describing the throughput behavior of EDCA networks is presented in this paper. Based on this model, the paper further provides a scheme in which a Pareto optimal system configuration is obtained via an appropriate CW control for a given AIFS value, which is a different approach compared to relevant papers in the literature that deal with CW control only. The simulation results confirm the effectiveness of the proposed method which shows significant performance improvements compared to other existing algorithms.

The Power Analysis and Its Control of Two-phase Orthogonal Power Supply for the Continuous Casting

  • Ma, Fujun;Luo, An;Xiong, Qiaopo
    • Journal of Electrical Engineering and Technology
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    • 제10권3호
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    • pp.971-982
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    • 2015
  • In order to improve the quality of the billet continuous casting, a two-phase orthogonal power supply (TPOPS) for electromagnetic stirrer is researched, which is composed of three-phase PWM rectifier and three-leg inverter. According to the power analysis of system, the ripple of dc-link voltage is analyzed and its analytical expression is derived. In order to improve the performance of electromagnetic stirring, an integrated control method with feedforward control is proposed for PWM rectifier to suppress the fluctuations of dc-link voltage and provide a stable dc source for inverter. According to the simplified equivalent model, a composite current control method is proposed for inverter. This proposed method can combine the merits of feedforward control with feedback control to effectively improve the dynamic output performance of TPOPS. Finally, a 300kVA prototype of TPOPS is developed, and the results have verified the analysis and control method.

고시수재 의약품 중 암브록솔염산염 및 클렌부테롤염산염 함유 제제의 함량 시험법 개선 (Development of Analytical Method for Ambroxol Hydrochloride and Clenbuterol Hydrochloride Formulation in Korean Pharmaceutical Codex)

  • 이태웅;정래석;박수진;최란;심영훈;최보경;곽효선
    • 약학회지
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    • 제58권3호
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    • pp.190-199
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    • 2014
  • The Korean Pharmaceutical Codex (KPC) analytical method of ambroxol hydrochloride and clenbuterol hydrochloride formulation is complicated and needed to carry out multiple processes during the test. To improve the low efficiency of analytical procedure that makes pharmaceutical laboratory consume much time and high cost to conduct the test of this formulation, this study was performed for simplifying the pretreatment process and optimizing conditions of the HPLC assay. The analytical procedure using HPLC was developed to establish analytical specification for ambroxol hydrochloride and clenbuterol hydrochloride formulations. The newly developed analytical method has good linearity ($R^2$ >0.999), specificity, precision (RSD<1.0%) and the recovery ranges of 98.50~101.84% for ambroxol, 98.29~101.35% for clenbuterol syrup and 98.66~101.71% for clenbuterol tablets. The LOQs were 0.204 ${\mu}g/ml$ for ambroxol, 0.021 ${\mu}g/ml$ for clenbuterol syrup and 0.073 ${\mu}g/ml$ for clenbuterol tablets. The new method was performed with commercially available samples to confirm analytical conditions and validated to be suitable for saving time and cost to control the quality of routine manufactured products. This analytical method will be used for revising the monograph of ambroxol hydrochloride and clenbuterol hydrochloride formulation in next supplement of KPC.

An HPLC-UV-based quantitative analytical method for Chrysanthemum morifolium: development, validation, and application

  • Jung, Dasom;Jin, Yan;Kang, Seulgi;Lee, Heesoo;Park, Keunbae;Li, Ke;Kim, Jin Hak;Geum, Jeong Ho;Lee, Jeongmi
    • 분석과학
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    • 제32권4호
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    • pp.139-146
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    • 2019
  • A simple and reliable analytical method based on high-performance liquid chromatography-ultraviolet detection was established for the analysis of the flowers of Chrysanthemum morifolium (CM). Luteolin-7-O-glucoside (LU7G) was chosen as a target analyte considering its content, availability, and ease of analysis. Chromatographic separation of LU7G was achieved using a Phenomenex Gemini $C_{18}$ column ($250{\times}4.6mm$, $5{\mu}m$) run with a mobile phase consisting of 0.5 % acetic acid in water and 0.5 % acetic acid in acetonitrile at a flow rate of $1.0mL\;min^{-1}$. The detection wavelength and column temperature were set at 350 nm and $40^{\circ}C$, respectively. Method validation was performed according to the AOAC guidelines and the method was specific, linear ($R^2=0.9991$ for $50-300{\mu}g\;mL^{-1}$), precise (${\leq}3.91%$RSD), and accurate (100.1-105.7 %). The limits of detection and quantification were 3.62 and $10.96{\mu}g\;mL^{-1}$, respectively. The established method was successfully applied to determine the contents of LU7G in various batches of bulk CM extracts and labscale CM extract. The developed method is a readily applicable method for the quality assessment of CM and its related products.

Quality Control of Majoon-e-Nisyan and its Acute Oral Toxicity Study in Experimental Rats

  • Shaikh, Masud;Husain, Gulam M.;Naikodi, Mohammed Abdul Rasheed;Kazmi, Munawwar H.;Viquar, Uzma
    • 셀메드
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    • 제11권1호
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    • pp.2.1-2.8
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    • 2021
  • The clinical condition Amnesia causes difficulty in learning new information and the inability to recall past events. It is primarily concerned with recent memory loss. Majoon-e-Nisyan (MJN) is a polyherbal Unani formulation, present in a semi-solid form. It is widely used potent drug of the Unani System of Medicine (USM) for treating Nisyan (amnesia). In the present study polyherbal Unani formulation, MJN has been studied for its quality control and acute toxicity. Standardization (quality control) of drugs deals with drug identity, drug quality and purity determination. Standardization of MJN had been done as per the Unani pharmacopoeial parameters approved by World Health Organization (WHO) - Pharmacognostical parameters, Physico-chemical parameters, high-performance thin-layer chromatography (HPTLC), microbial load, aflatoxin, and heavy metals. Solvents and chemicals used in the study were of analytical grade and used instrument were calibrated. By conducting an acute oral toxicity study in rats, the safety of MJN was assessed. The limit test method of OECD guideline 425 was followed in the study. Results of standardization and standard operating procedures (SOPs) for preparation of MJN may serve as the standard reference in the future. The data generated in the study for the quality control of MJN proved the quality of formulation and shows that MJN is not toxic in rats following acute dosing up to 2000 mg/kg bw. The data obtained in the paper for MJN may be used as a standard guideline for preparation of the formulation which can save time, cost, and resources for future research endeavours.

The Quality Control Program for Industrial Hygiene Laboratories in Korea

  • Park, Hae Dong;Chung, Eun Kyo;Kim, Kiwoong
    • Safety and Health at Work
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    • 제8권3호
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    • pp.322-326
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    • 2017
  • In 1992, the quality control program was introduced in Republic of Korea to improve the reliability of the work environment monitoring, which was introduced in the 1980s. The commission entrusted by the Ministry of Employment and Labor, the Occupational Safety and Health Research Institute has conducted the program for industrial hygiene laboratories including designated monitoring institutions and spontaneously participating agencies. The number of institutions that participated in the program has increased from 30 to 161. The initial conformance ratio in the participants was 43% (organic solvents) and 52% (metals). Thereafter, the conformance ratio increased rapidly and it has remained in a stable state at more than 89% since 1996. As subject materials, 13 kinds of organic solvents and 7 kinds of metals were used. To improve the capability of measurement and analysis of private institutions, educational courses were conducted annually. An assessment at the actual sites of participants was additionally introduced into the program in 2013. Thus, the program turned into a system that administrates the overall process of participants. For the future, the scope of target materials will be extended through additional items. Thus, the reliability of the results of the work environment monitoring is expected to increase accordingly.

한국형모델의 신규 GNSS RO 자료 활용과 품질검사 개선에 관한 연구 (A Study on Improvement of the Use and Quality Control for New GNSS RO Satellite Data in Korean Integrated Model)

  • 김은희;조영순;이은희;이용희
    • 대기
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    • 제31권3호
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    • pp.251-265
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    • 2021
  • This study examined the impact of assimilating the bending angle (BA) obtained via the global navigation satellite system radio occultation (GNSS RO) of the three new satellites (KOMPSAT-5, FY-3C, and FY-3D) on analyses and forecasts of a numerical weather prediction model. Numerical data assimilation experiments were performed using a three-dimensional variational data assimilation system in the Korean Integrated Model (KIM) at a 25-km horizontal resolution for August 2019. Three experiments were designed to select the height and quality control thresholds using the data. A comparison of the data with an analysis of the European Centre for Medium-Range Weather Forecasts (ECMWF) integrated forecast system showed a clear positive impact of BA assimilation in the Southern Hemisphere tropospheric temperature and stratospheric wind compared with that without the assimilation of the three new satellites. The impact of new data in the upper atmosphere was compared with observations using the infrared atmospheric sounding interferometer (IASI). Overall, high volume GNSS RO data helps reduce the RMSE quantitatively in analytical and predictive fields. The analysis and forecasting performance of the upper temperature and wind were improved in the Southern and Northern Hemispheres.

Proficiency Test for Pharmaceutical Companies in Analyzing Drug Products (I) - Comparison of Criteria for Satisfactory Test Results

  • Cho, Jung-Hwan;Sung, Jun-Hyun;Choi, Seon-Hee;Choi, Jang-Duck;Lee, Seung-Kyung;Chae, Kab-Ryong;Moon, Byung-Woo
    • 대한약학회:학술대회논문집
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    • 대한약학회 2002년도 Proceedings of the Convention of the Pharmaceutical Society of Korea Vol.2
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    • pp.398.3-399
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    • 2002
  • Quality control by analytical ability with a certain level of precision and accuracy is important. This is true especially in pharmaceutical industries. for a failure in quality control can result in a failure in drug medication. in turn. sometimes a heavy damage to patient's health condition andlor the worst damage to company's reputation. On this backgroun, Kyungki KFDA prepared test pharmaceutical products, which were distributed to 114 pharmaceutical companies in kyungin Province in year 2000. (omitted)

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근적외 분광분석법에 의한 잎담배의 품질측정 자동화 (A Study for Automatic Analysis of Qualysis of Quality Components in Tabacco Leaves Using Non-destructive Analytical Method)

  • 조래광;이경희;이정환;권영길
    • Applied Biological Chemistry
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    • 제37권5호
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    • pp.349-355
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    • 1994
  • 비파괴 측정법의 하나인 근적외 분광분석법을 응용하여 국내산 황색종 잎담배의 품질에 관련된 주요성분인 수분, 니코틴, 전질소, 환원당 및 색깔 등을 신속, 정확하게 동시에 측정하기 위한 가능성을 조사하였다. 근적외 영역의 광학데이타와 기존 습식분석법에 의한 잎담배의 수분, 니코틴, 전질소, 환원당 및 L, a, b 측정치 간에 중회귀 분석을 행한 결과, 검정용 시료에 대한 측정오차(SEP)가 각각 0.28%, 0.25%, 0.07%, 1.25, 0.44 및 1.07이며, 시료의 전처리없이 30초 이내에 동시에 측정 가능함을 알 수 있었다. 아울러 잎담배 수매, 원료가공 및 제품담배 제조현장에 활용하기 위한 보급형 근적외 분광분석기의 개발 가능성도 검토하였다.

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Evaluation Metrics for Class Hierarchy in Object-Oriented Databases: Concurrency Control Perspectives

  • Jun Woo-Chun
    • 한국멀티미디어학회논문지
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    • 제9권6호
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    • pp.693-699
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    • 2006
  • Object-oriented databases (OODBs) have been adopted for managing non-standard applications such as computer-aided design (CAD), office document management and many multimedia applications. One of the major characteristics of OODBs is class hierarchy where a subclass is allowed to inherit the definitions defined on its superclasses. In this paper, I present the evaluation metrics for class hierarchy quality in OODBs. These metrics are developed to determine if a concurrency control scheme can achieve good performance or not on a given class hierarchy. I first discuss the existing concurrency control schemes for OODBs. Then I provide evaluation metrics based on structural information and access frequency information in class hierarchies. In order to discuss significance of the proposed performance metrics, an analytical model is developed. Analysis results show that the performance metrics are important factor in concurrency control performance. I consider both single inheritance and multiple inheritance. The proposed metrics can be used to provide guidelines on how to design class hierarchy of an OODB for maximizing the performance of concurrency control technique.

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