• Korean Journal of Medicinal Crop Science
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• v.3 no.3
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• pp.226-232
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• 1995

Extraction methods and instrumental analytical conditions were compared to establish a fast and appropriate analytical method to determine saikosaponins in Bupleurum falcatum. Using HPLC, analysis of diene-saikosaponin treated with 2% acid was faster than that of saikosaponin itself. Among various extraction methods, extraction by standing in methanol at room temperature showed highest efficieny, and extraction with boiling methanol was shorter in analytical time and showed good chromatogram. And we could analyze many samples faster using HPTLC but the analytical accuracy was low. In extraction and analysis of saikosaponins, extraction with boiling methanol and acidic treatment was fast and easy analytical method. And for selecting useful lines in component breeding, we think TLC method was better.

• Steel and Composite Structures
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• v.43 no.3
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• pp.327-340
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• 2022

A vast amount of experimental and analytical research has been conducted related to the seismic behavior and performance of concrete filled steel tubular (CFT) columns. This research has resulted in a wealth of information on the component behavior. However, analytical and experimental data for structural systems with CFT columns is limited, and the well-known behavior of steel or concrete structures is assumed valid for designing these systems. This paper presents the development of an analytical model for nonlinear analysis of composite moment resisting frame (CFT-MRF) systems with CFT columns and steel wide-flange (WF) beams under seismic loading. The model integrates component models for steel WF beams, CFT columns, connections between CFT columns and WF beams, and CFT panel zones. These component models account for nonlinear behavior due to steel yielding and local buckling in the beams and columns, concrete cracking and crushing in the columns, and yielding of panel zones and connections. Component tests were used to validate the component models. The model for a CFT-MRF considers second order geometric effects from the gravity load bearing system using a lean-on column. The experimental results from the testing of a four-story CFT-MRF test structure are used as a benchmark to validate the modeling procedure. An analytical model of the test structure was created using the modeling procedure and imposed-displacement analyses were used to reproduce the tests with the analytical model of the test structure. Good agreement was found at the global and local level. The model reproduced reasonably well the story shear-story drift response as well as the column, beam and connection moment-rotation response, but overpredicted the inelastic deformation of the panel zone.

• Analytical Science and Technology
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• v.15 no.1
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• pp.15-19
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• 2002

The pretreatment of tungsten added $BaTiO_x$ ceramics was performed to improve the recovery of Ba, Ti and W. $BaTiO_x$ ceramics were digested with HF : HCl ( 1 : 2 ) mixture in an acid digestion bomb at $220^{\circ}C$ for 3 hrs. The concentration of Ba, Ti and W were determined by ICP-AES. Recoveries of Ba, Ti and W were 99.6%, 99.8% and 99.2%, respectively. And their C.V. values were 1.02%, 0.73% and 1.79%. Using this method, the analytical results of Ba, Ti and W for a real sample were obainted to be 25.9% (w/w), 38.8% (w/w) and 3.31% (w/w), respectively.

• Analytical Science and Technology
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• v.24 no.4
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• pp.237-242
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• 2011

In this study, an analytical method was developed for residual metamizol in beef and pork using LC/MS/MS. 4-methylaminoantipyrin (MAA), the main metabolite of metamizol was targeted for analysis instead of its parent compound. MAA was simply extracted from meat by acetonitrile, purified and then analyzed by multiple reaction monitoring method (MRM). Standard addition method was used for calibration. The calibration curves showed the linearity of $r^2$ > 0.99 for both matrices included. The developed method was validated by six-time intra-lab tests and inter-lab tests with two other institutes. The validation of the whole procedure for beef showed the intra-lab accuracies of 78-102% (CV 5.5-9.1%) and the inter-lab accuracy of 98% (CV 14%); the intra-lab accuracies of 95-99% (CV 3.9-5.6%) and the inter-lab accuracy of 111% (CV 13%).

• Journal of Korean Society of Industrial and Systems Engineering
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• v.38 no.3
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• pp.87-94
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• 2015

Recently, management based on statistical data has become a big issue and the importance of the statistics has been emphasized for the management innovation in the defense area. However, the Military Management based on the statistics is hard to expect because of the shortage of the statistics in the military. There are many military information systems having great many data created in real time. Since the infrastructure for gathering data form the many systems and making statistics by using gathered data is not equipped, the usage of the statistics is poor in the military. The Analytical Defense Statistics System is designed to improve effectively the defense management in this study. The new system having the sub-systems of Data Management, Analysis and Service can gather the operational data from interlocked other Defense Operational Systems and produce Defense Statistics by using the gathered data beside providing statistics services. Additionally, the special function for the user oriented statistics production is added to make new statistics by handling many statistics and data. The Data Warehouse is considered to manage the data and Online Analytical Processing tool is used to enhance the efficiency of the data handling. The main functions of the R, which is a well-known analysis program, are considered for the statistical analysis. The Quality Management Technique is applied to find the fault from the data of the regular and irregular type. The new Statistics System will be the essence of the new technology like as Data Warehouse, Business Intelligence, Data Standardization and Statistics Analysis and will be helpful to improve the efficiency of the Military Management.

• Analytical Science and Technology
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• v.13 no.4
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• pp.412-422
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• 2000

The polymeric FAB materials of air shower used in clean room of wafer industry have been outgassed with the dynamic headspace (ca.$100^{\circ}C$) for half an hour, and analyzed using GC-MS. The air in the clean room running air shower was sampled using sorbent tube method, and the organic compounds adsorbed in the sorbent tube were extracted using Soxhlet extraction method, and analyzed using GC-MS. The analytical results from FAB materials of air shower (electric over current relay, acryl plate. polycarbonate window, filter, fan housing, steel galvanized cold plate and canvas buffer) indicated that most of chemicals were originated from polymer fragments of FAB materials. Their analytical results have been compared with those from the air of clean room running air shower. These comparative results could lead to identify whether the sources of trace organic contaminants in clean room air are originated from the polymeric FAB material of air shower.

• Analytical Science and Technology
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• v.34 no.3
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• pp.99-114
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• 2021

Substance identification is the first step in implementing chemical legislation, such that subsequent hazard and risk assessments can be accurately followed. Based on the web page and related guidance documents of the European Chemicals Agency and available consortia information, the procedure for substance identification carried out in Registration, Evaluation, Authorization and Restriction of Chemicals (REACH) is surveyed. In this study, the importance of substance identification and substance sameness check, as well as the necessity of generating a substance identity profile (SIP) are considered. In addition, the SIPs of several substance types are presented, which focused on information utilization in the instrumental analysis results and organization of information to generate the SIP. Analytical science can contribute to the accurate and effective implementation of chemical regulation at the starting stage of substance identification. However, understanding of the regulation and consequent final wrap-up of analytical results as a SIP should be followed for communication among registrants in Substance Information Exchange Forum (SIEF) as well as with related authorities.

• Journal of the Korean Geotechnical Society
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• v.23 no.4
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• pp.185-197
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• 2007

Limit analysis of upper and lower bound solutions has been well developed to provide the stability numbers for shallow tunnels in cohesive soil ($c_u$ material), cohesive-frictional soil (c'-$\phi$' material) and cohesionless soil ($\phi$'material). However, an extension of these methods to relatively deep circular tunnels in the cohesionless soil has been explored rarely to date. For this reason, the closed-form analytical solutions including lower bound solution based on the stress discontinuity concept and upper bound solution based on the kinematically admissible failure mechanism were proposed for assessing tunnel collapse load in this study. Consequently, the tunnel collapse load from those solutions was compared with both the finite element analysis and the previous analytical bound solutions and shown to be in good agreement with the FE results, in particular with the FE soil elements located on the horizontal tunnel axis.

• ETRI Journal
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• v.15 no.2
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• pp.1-9
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• 1993

Nitzberg has analyzed the detection performance of the clutter map constant false alarm rate (CFAR) detector using single pulse. In this paper, we extend the detection analysis to the clutter map CFAR detector that employs M-pulse noncoherent integration. Detection and false alarm probabilities for Swerling target models are derived. The analytical results show that the larger the number of integrated pulses M, the higher the detection probability. On the other hand, the analytical results for Swerling target models show that the detection performance of the completely decorrelated target signal is better than that of the completely correlated target.

• Journal of the Microelectronics and Packaging Society
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• v.7 no.4
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• pp.17-22
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• 2000

In this paper, methods to analyze wire sweep during the semiconductor chip encapsulation have been studied. The wire sweep analysis is used to analyze the deformation of bonding wires that connect the chip to the leadframe during encapsulation. The analysis is done using either analytical solutions or numerical simulation. The analytical solution is used for rough but fast calculation of wire sweep. The results from the numerical simulation are closest to the experimental results.