• Journal of Sensor Science and Technology
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• v.16 no.6
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• pp.395-400
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• 2007

Ambient drying sol-gel processing was used for monolithic silica ambigels in the temperature range of $130-250^{\circ}C$. A new method of mesopore ambigels, which mean the aerogels prepared by ambient pressure drying process synthesis, is suggested at first. This method includes two important approaches. The first point is that $SiO_{2}$ surface modification of wet gel was performed by trimethylchlorosilane in n-butanol solution. This procedure is provided the silica gel mesopore structure formation. The second point is a creation of the ternary azeotropic mixture water/n-butanol/octane as porous liquid, which is effectively provided removing of water such a low temperature by 2 step drying condition under ambient pressure. The silica aerogels, which were prepared by ambient pressure drying from azeotropic mixture of water/n-butanol/octane, are transparent, crack-free and mesoporous (pore size ${\sim}$ 5.6 nm) with surface area of ${\sim}$ $923{\;}m^2/g$, bulk density of $0.4{\;}g/cm^3$ and porosity of 85 %.

• Journal of the Korean Society of Food Science and Nutrition
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• v.25 no.3
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• pp.453-459
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• 1996

This study was carried out to determine the changes in quality during the drying process and the optimum drying condition for utilizing soybean curd residue. The quality criteria for soybean curd residue were acid value, peroxide value, fatty acid composition and microbial concentration. The acid values of soybean curd residue were 7.5, 4.5 and 5.9 KOH mg/g upon 12 hour drying with open-air sun, ambient-air blast and warm-air blast, respectively. The numbers of total aerobic bacteria and molds increased remarkably during drying with open-air sunlight, ambient-air blast and warm-air blast except for hot air blast. Among different drying methods, the hot air blast drying(1kg of sample) was the most effective methods, which completed in three hours. Also, the drying method demonstrated a typical drying curve ; settling down, constant rate drying and falling rate drying period were shown within one hour, from one and three hours and after three hours, respectively. Moreover, there was significant variation in the constant drying period for the quality of soybean curd residue.

• Journal of Sensor Science and Technology
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• v.16 no.1
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• pp.77-83
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• 2007

Nanoporous silica aerogels with various surface modifiers were prepared by ambient drying process. Tetraethylorthosilicate (TEOS) were used a raw material. Ambient drying process for various surface modifier was studied in the point of view of a crack-free monolith and thin films and low cost. Various kinds of surface modifiers like as hexamethyldisilazane (HMDSZ), trimethlychlorosilane (TMCS), methlytriethoxylsilane (MTES), and methlytrimethoxysilane (MTMS) were studied in order to enhance hydrophobicity for the silica aerogel. Surface modified aerogels were evaluated by FT-IR, TG, BET, SEM and wetting angle measurement. Homogeneous and crack-free aerogels were obtained by modifying the HMDSZ and the TMCS. However silica xerogel was obtained when modified with MTMS, MTES.

• Journal of Biosystems Engineering
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• v.23 no.3
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• pp.229-244
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• 1998

This study was performed to determine proper fan and heater management schemes for natural air drying of rough rice in round steel bin with stirring device under Korean weather conditions. A computer simulation model was developed to predict moisture content changes, energy requirements, and drymatter losses during drying of rough rice by natural air. Drying test was conducted to validate the simulation model using round steel bin of holding capacity of 300ton at Rice Processing Complex in Jincheon. The bin was filled with rough rice every day and mixing by stirring device. Moisture contents, ambient air temperatures, relative humidities, static pressures in plenum chamber in the bin, airflow rates, and electrical and fuel energy were measured. Relative errors of moisture content changes predicted by the simulation model were below 5ft, and relative errors of final moisture content, final grain weight, required energy ranged from 0.9% to 6%. These not levels indicated that the simulation model can satisfactorily predict the performance factors of natural air drying system such as drying rates and energr consumptions comparing error level of 10% to 15% in other drying simulation models generally used in dryer desists. Twelve different fan and heater management schemes were evaluated using the computer simulation model based on three hourly weather data from Suweon for the period of 1952-1994. The best management schemes were selected comparing the drymatter losses, required drying times, required energy consumptions. Operating fan without heating only when ambient relative humidity was below 85% or 90% appeared to be the most effective method of In operation in favorable drying weather. Under adverse drying climates or to reduce required drying time, operating fan continuously, and heating air with $1.5^{\circ}C$ temperature rise only when ambient relative humidity was over 85% appeared to be the most suitable method.

• Proceedings of the Korean Society for Agricultural Machinery Conference
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• 1993.10a
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• pp.896-905
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• 1993

Thin-layers of wheat and barley are dried at near-ambient temperatures(3.5$^{\circ}C$ -5$0^{\circ}C$) in order to obtain the intrinsic drying data. The well established apparatus was modified to enable it to record all the sample weight data in still air by using a purpose -built automatically controlled sliding valve. The air could be diverted in less than 0.5seconds and a 7 second period was required to attain a steady weight reading. With this apparatus, very smooth drying curves were obtained. The data of sample weight , drying temperature and dew point temperature wee recorded continuously . The drying process was terminated when the moisture content change in 24 hours was less than 0.004 d.b. This was achieved by drying a sample for about a week . The final points were recorded as the dynamic equilibrium moisture content(EMC). The drying data were than fitted to the exponential Newton model and the dynamic EMC data were fitted to the Modified-Chung-Pfost Model . All the fitted parameters are given and comparison is made with previous published data. The comparisons who that the current drying constants are lower than the previous data, the dynamic EMC data obtained for wheat and barely agree with the previous data. The results show that to obtain the drying constant in the exponential Newton model, adequate drying time is necessary.

• Particle and aerosol research
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• v.14 no.4
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• pp.191-203
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• 2018

IIn this study, we have developed drying systems for reducing the error by humidity on measuring particulate matter (PM) in the ambient air with optical particle measuring instruments. Two types of drying systems were designed: drying systems using heating and dilution methods. In addition, 3 types of drying systems using a heating method were designed: Type A (1 hole), B (3 holes) and C (7 holes). After making them, the laboratory and field tests were carried out to evaluate the developed drying systems. As a result, it was shown that the PM concentrations obtained by PM monitoring devices with drying systems agree well with that of the reference devices. Therefore, it could be concluded that the drying systems can be applied to PM monitoring devices for real-time monitoring of the ambient aerosols.

• Journal of Sensor Science and Technology
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• v.15 no.3
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• pp.173-178
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• 2006

Silica aerogel with ultra low density and high porosity has been focused on versatile application due to its fascinating properties. Ambient drying process of waterglass, in this study was researched to fabricate a crack-free monolith body in the point view of cost effective way. Wet gel was obtained by removing of $Na^{+}$ ions in waterglass, which contains 8 wt% of $SiO_{2}$. Xylene, which has a low vapor pressure, was used as a solution substitutor to prevent the formation a cracks during drying. Various surface modifiers like as hexamethyldisilazane (HMDSZ), trimethylchlorosilane (TMCS), methyltriethoxylsilane (MTES), methyltrimethoxysilane (MTMS) and phenyltriethoxysilane (PTES) were used in order to improve hydrophobicity of the waterglass Silica aerogel. Some physical properties of the surface modified aerogels were investigated by FT-IR, TGA, BET and SEM. Hydrophobicity and hydrophilicity of Silica aerogel is attributed to the Si-OH bond and the non-polar C-H bond groups on the surface of aerogel. Crack-free waterglass aerogel with >90 % of porosity, 17 nm of pore size and <0.15 $g/cm^{3}$ of density was prepared. HMDSZ and TMCS are effective as a surface modifier

• Journal of Sensor Science and Technology
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• v.15 no.5
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• pp.371-377
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• 2006

Nano porous, transparent silica aerogels monoliths were prepared under ambient drying (1 atm, $270^{\circ}C$) condition by the combination of sol-gel process and surface modification with subsequent heat treatment. Three kinds of solvent, n-hexane, n-heptane and xylene, were selected in the point view of low surface tension and vapor pressure in order to restrain a formation of cracks during drying. Crack-free silica aerogels with over 93 % of porosity and below $0.14g/cm^3$ of density were obtained by solvent exchange and surface modification under atmosphere condition. Optimum solvent was confirmed n-heptane among these solvents through estimation of FT-IR, TGA, BET and SEM. Modified silica aerogel exhibited a higher porosity and pore size compare to unmodified aerogels. Hydrophobicity was also controled by C-H and H-OH bonding state in the gel structure and heat treatment over $400^{\circ}C$ effects to the hydrophobicity due to oxidation of C-H radicals.

• Proceedings of the Materials Research Society of Korea Conference
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• 2006.11a
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• pp.7.2-7.2
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• 2006

• Journal of the Korean Ceramic Society
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• v.45 no.2
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• pp.87-89
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• 2008

A nano structured silica aerogel thin film was manufactured from inexpensive sodium silicate (water glass) using an ambient pressure drying method. High purity silicic sol was prepared by passing a water glass solution through an ion exchange resin, and the gel films were prepared on a modified glass substrate via dip coating. The dip coating conditions, such as coating time and solvent, were optimized. The optical and physical properties of the obtained silica aerogel thin film were characterized using a UV-visable spectrometer and a scanning electron microscope.