• 한국자기학회지
• /
• 제1권2호
• /
• pp.60-68
• /
• 1991

급속냉각기술로 제조된 $Nd_{14}Fe_{76}Co_{4}B_{6}$ 및 $Nd_{10.5}Fe_{79}Co_{2}Zr_{15}B_{7}$ 자성분말을 사용하여 성형체와 본드자석을 제조하였다. 자기특성, 최적충진률 등의 분말입도 및 형상비에 따른 거동은 합금조성에 따라 달리 나타난다. Co/Fe 비가 작은 저밀도의 $Nd_{10.5}Fe_{79}Co_{2}Zr_{1.5}B_{7}$ 합금이 같은 성형압력에서 성형체의 성형밀도 및 최적충진률이 높아 자기특성이 우수하였으나 반면에 분말입도에 따라 자기특성이 변화하였다. 성형밀도(p)와 성형압력(P) 사이 에는 ${\phi}(g/cm^{2})=5.2~5.6{\times}P^{0.045~0.065}(ton/cm^{2})$의 관계식이 성립된다. 높은 Nd/Fe 비를 갖는 급속냉각된 $Nd_{14}Fe_{76}Co_{4}B_{6}$ 합금의 초미세립(50~60 nm)으로써 높은 보자력($iH_{c}=14~15kOe$)을 보유하나, Nd/Fe비가 낮은 $Nd_{10.5}Fe_{79}Co_{2}Zr_{1.5}B_{7}$ 합금은 결정립이 조대하고(150~400 nm)Nd-rich한 입경계상의 발달이 부진하여 자벽고착기구가 주 보자력 기구 로 판명된 두 합금에서 고착지점으로서의 역할이 불충분하여 보자력이 낮은 것으로 판명되었다.

• 동력기계공학회지
• /
• 제19권1호
• /
• pp.64-69
• /
• 2015

Aluminum alloy is a material with a high strength-weight ratio and excellent thermal conductivity. It neither readily corrodes nor quickly weakens at low temperatures, but can be easily recycled. Because of these features, aluminum heat exchangers are widely used in aluminum alloy. In addition, the aluminum alloy used in other areas is expected to gradually increase. As a result, researchers have been continuously studying the cutting patterns of aluminium alloy. However, such studies are fewer than those on the cutting patterns of ordinary steel. Moreover, the research on ball endmilling with aluminium alloys has not received much attention. Therefore, in this study, an attempt was made to find the optimal cutting pattern among the seven cutting patterns for the machining of the commonly used aluminum alloy using ball endmilling for a heat exchanger. The optimal pattern was found by comparing the different shapes and surface roughness values produced by the seven patterns.

• 한국수소및신에너지학회논문집
• /
• 제3권2호
• /
• pp.9-15
• /
• 1992

Electroless copper plating method using an alkaline bath have been employed in copper coating of the (LM)Ni4.5Co0.1MnO.2A10.2 hydrogen storage alloy powders for electrode preparation. The plating were conducted without any pretreatment of alloy powders. For the preparation of the electrodes, about 0.12g of the copper coated alloy powder (copper to alloy ratio 1/3 by weight) was compacted with pressure of 6 tons/cm2 at room temperature. The disk-type compacts had a diameter of 10mm and thickness of about 0.24mm. The electrode characteristics were examined through SEM observations and electrochemical measurements in a half cell. The electrochemical measurement showed that the maximum discharge capacity of the electrodes prepared by using alkaline bath were 245mAh per gram of coated alloy (327mAh per gram of alloy) and appeared a considerable degradation with increasing number of cycles. The decrease of the discharge capacity after 100 cycles was about 30% It can be suggested that, with a slight of improvement, this electroless copper plating method could be applied to the preparation of the rare earth-nickel based alloy electrode.

• 한국해양공학회지
• /
• 제6권1호
• /
• pp.96-104
• /
• 1992

Aircraft structures and engineering structures are always subject to variable amplitude loads. Variable amplitude loads include some kind of loading history; for example, constant amplitude load, single peak overload and block overload etc. Crack growth under variable amplitude loading exhibits retardation effect. In this study, the 4 point bending fatigue test was performed by hydrolic servo fatigue testing machine on 7075-T6 Al-alloy. The retardation effect of overload ratio and numbers of overload cycle was quantitatively studied. 1) Change of retardation effect against increment of overload ratio is more evident when the multiple overload is applied than single overload is done. 2) The number of overload cycle is very important factor about the crack growth retardation effect when the overload ratio is more than 1.75; that is not when the overload ratio is less than 1.75. 3) Overload affected zone size increased gradually by increment of crack growth retardation effect. 4) Crack driving force is more greatly reduced when the crack tip branched off two direction than it sloped to one direction.

• 열처리공학회지
• /
• 제31권5호
• /
• pp.213-219
• /
• 2018

This study was carried out to investigate the effect of hot forging ratio and solution treatment temperature on the mechanical properties of incoloy 825 alloy. With an increasing of the hot forging ratio, grain size and range of grain size was decreased. With an increasing of the solution treatment temperature after 90% forging, grain size and range of grain size was increased. Cr carbides and Ti nitrides was precipitated at below $900^{\circ}C$ and volume fraction of precipitate was increased with an decreasing of the solution treatment temperature. With an increasing of the hot forging ratio, hardness, tensile strength and elongation, toughness was increased. With an increasing of the solution treatment temperature after 90% forging, hardness and strength was increased, elongation and toughness was decreased by grain refinement. With an increasing of the forging ratio, effect of solution treatment temperature on the hardness, strength and elongation was small, but on the toughness was large.

• 대한기계학회논문집A
• /
• 제23권6호
• /
• pp.1001-1010
• /
• 1999

Thermo-mechanical behavior of discontinuous shape memory alloy(SMA) reinforced polymeric composite has been studied using modified shear lag theory and finite element(FE) analysis with 2-D multi-fiber model. The aligned and staggered models of short-fiber arrangement are employed. The effects of fiber overlap and aspect ratio on the thermomechanical responses such as the thermal expansion coefficient are investigated. It is found that the increase of both tensile stress(resistance stress) in SMA fiber and compressive stress in polymer matrix with increasing aspect ratio is the main cause of low thermal deformation of the composite.

• 대한기계학회:학술대회논문집
• /
• 대한기계학회 2000년도 춘계학술대회논문집A
• /
• pp.153-158
• /
• 2000

Atomic Force Microscope (AFM) was used to study cross sectional profiles and dimensions of fatigue striations in 2017-T351 aluminum alloy. Their widths (SW) and heights $(SH,\;SH_h)$ were measured from the cross sectional Profiles of three-dimension AFM images. The following results that will be helpful to understand the fatigue crack growth mechanism were obtained. (1) Coincidence of the crack growth rate with the striation width was found down to the growth rate of $10^{-5}$ mm/cycle. (2) The relation of $SH={\alpha}(SW)^{1.2}$ was obtained. (3) The ratio of the striation height to its width SH/SW and did not depend on the stress intensity factor range ${\Delta}K$ and the stress ratio R. From these results, the applicability of the AFM to nano-fractography is discussed.

• 열처리공학회지
• /
• 제2권4호
• /
• pp.19-26
• /
• 1989

Fundmental fatigue crack propagation tests with C-T type specimens were conducted at various load ratios (R) such as 0.1, 0.3 and 0.5 in T6 and Thermomechanically treated (TMT) conditions of 7039 Al alloy. Better mechanical properties from monotonic test as well as fatigue crack propagation were obtained by TMT process owing to uniform distribution of fine microstructures and non-existence of precipitation free zone (PFZ). Through the measurement of Kop and ${\Delta}K$ at various R the concept of effective stress intensity factor range ratio, U was reviewed to asses the load ratio effect on fatigue crack propagation. A relationship between U and variables such as ${\Delta}K$ and R was obtained empirically. This may enable us to predict ${\Delta}K_{eff}$ that is of critical importance for prediction of fatigue crack propagation rate.

• 헤리티지:역사와 과학
• /
• 제57권1호
• /
• pp.146-159
• /
• 2024

본 연구에서는 강진 고성사 청동보살좌상을 대상으로 과학적 분석을 통해 불상의 제작기술 및 납 원료산지에 대한 연구를 실시하였다. 불상에서 수습한 극미량의 시료를 대상으로 미세조직 관찰결과 주조 공정을 통해 제작되었음을 알 수 있었다. 이어 SEM-EDS를 통한 합금조성비 분석결과 구리(Cu) 81.26wt% 주석(Sn) 16.42wt%, 납(Pb) 1.72wt%의 삼원계 합금으로 확인되었다. 열이온화질량분석기(TIMS)를 이용한 납동위원소비 분석결과를 한반도 납동위원소비 분포도에 대입한 결과 전라도와 충청도 지역, 경상남·북도 지역에 도시되었다. 불상이 봉안된 강진 고성사는 해당영역의 사이에 위치하고 있다. 이러한 과학적 분석결과를 종합해 볼 때 강진 고성사 청동보살좌상은 구리, 주석, 납을 합금하여 주조하였으며, 불상제작 시 사용된 납 원료는 고성사 인근 지역에서 수급하여 사용한 것으로 판단된다. 이때 주목할 점은 해당 불상이 높이 51cm의 중·대형 불상임에도 불구하고 합금조성비 분석결과 기존 선행연구에서 제시한 소형 청동 및 금동제 불상의 납 함량비와 유사한 경향성을 보이고 있다는 것이다. 이에 불상의 크기와 납 함량비 간의 연관성을 고찰하고자 고성사 청동보살좌상과 조성연대가 유사한 청동 및 금동제 불상의 형태학적 특징 및 합금조성비 등 전반적인 제작기술을 비교분석 하였다. 비교결과 청동 및 금동제 불상의 합금조성비를 결정하는 요인에는 불상의 크기 뿐만 아니라 양식적인 특징, 조성연대 등 다양한 요인이 존재할 수 있으며, 이에 따라 불상을 조성할 당시 합금조성비 또는 주조기술을 적절히 조절하였을 가능성을 확인하였다. 즉, 불상의 제작기술 연구를 위해서는 방사선 투과촬영조사 등을 활용한 내부구조 관찰, 미세조직관찰 및 합금조성비 분석 등의 과학적 분석결과 뿐만 아니라 양식적 특징 및 조성연대에 관한 고고·미술사학적 연구를 함께 진행함으로서 보다 종합적인 불상 제작기술체계에 대한 규명이 이루어져야 할 것으로 판단된다.

• 대한금속재료학회지
• /
• 제46권5호
• /
• pp.289-295
• /
• 2008

The effect of the alloy elements(Si/Mn) ratio on the coating quality including wettabilty with molten zinc, galvannealing kinetics and crater has been investigated in interstitial-free high strength steel(IFHSS) containing Si and Mn. When the Si/Mn ratio was below 0.75, IF-HSS exhibited a good wettability leading to a good galvannealed coating quality after annealing at $800^{\circ}C$ for 40s in $15%H_2-N_2$ mixed gas with dew point $-60^{\circ}C$. In contrast, the wettability and galvannealed coating quality were deteriorated in the Si/ Mn ratio above 0.75. It is shown that they have relevance to oxides forms by selective oxidation on the steel surface. The oxide particles dispersed on the steel surface with a surface coverage of below 40% resulted in good wettability and galvannealed coating quality. The oxide particle is mainly consisted of $Mn_2SiO_4$ with low contact angle in molten zinc. On the other hand, the continuous oxide layer on the steel surface, such as network- and film-type,caused to poor wettability and galvannealed coating quality. The coverage of oxide layer was above 80%, and its chemical species was $SiO_2$ with high contact angle in molten zinc. Consequently, the Si/Mn alloy ratio played an importance role in galvannealed coating quality of IF-HSS.