• Journal of Powder Materials
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• 제14권2호
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• pp.123-126
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• 2007

In this work, the dispersion behavior of $Y_2O_3$ particles in binary aluminum (Al)-copper (Cu) cast alloy was investigated with respect to Cu contents of 20 (hypoeutertic), 33 (eutectic) and 40 (hypereutectic) wt.%. In cases of hypo and hypereutectic compositions, SEM images revealed that the primary Al and ${\theta}$ phases were grown up at the beginning, respectively, and thereafter the eutectic phase was solidified. In addition, it was found that some of $Y_2O_3$ particles can be dispersed into the primary Al phase, but none of them are is observed inside the primary 6 phase. This different dispersion behavior of $Y_2O_3$ particles is probably due to the difference in the val- ues of specific gravity between $Y_2O_3$ particles and primary phases. At eutectic composition, $Y_2O_3$ particles were well dispersed in the matrix since there is few primary phases acting as an impediment site for particle dispersion during solidification. Based on the experimental results, it is concluded that $Y_2O_3$ particles are mostly dispersed into the eutectic phase in binary Al-Cu alloy system.

• Journal of Powder Materials
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• 제17권3호
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• pp.190-196
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• 2010

In this paper, rapid solidified Mg-4.3Zn-0.7Y (at.%) alloy powders were prepared using an inert gas atomizer, followed by a severe plastic deformation technique of high pressure torsion (HPT) for consolidation of the powders. The gas atomized powders were almost spherical in shape, and grain size was as fine as less than $5\;{\mu}m$ due to rapid solidification. Plastic deformation responses during HPT were simulated using the finite element method, which shows in good agreement with the analytical solutions of a strain expression in torsion. Varying the HPT processing temperature from ambient to 473 K, the behavior of powder consolidation, matrix microstructural evolution and mechanical properties of the compacts was investigated. The gas atomized powders were deformed plastically as well as fully densified, resulting in effective grain size refinements and enhanced microhardness values.

• Journal of the Korean Magnetics Society
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• 제9권3호
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• pp.154-158
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• 1999

Magnetic properties and microstructure of nanocrystalline $\alpha$-(Fe, Co)-based Nd-(Fe, Co)-B-Nb-Cu alloys have been investigated. $Nd_x(Fe_{0.9}Co_{0.1})_{90-x}B_6Nb_3Cu_1$(x=2, 3, 4, 5, 6) alloys prepared by rapid solidification process show amorphous phase except the one with x=2. By a proper annealing, the amorphous in the alloy is changed to a nanocrystalline phase. It is confirmed that the nanocrystalline alloys are composed of $\alpha$-(Fe, Co) and $Nd_2(Fe, Co)_{14}B_1$ phase. The optimally annealed $Nd_3(Fe_{0.9}Co_{0.1})_87B_6Nb_3Cu_1$ alloy shows the highest remanence of 1.55 T. The coercivity increases with the increase of Nd content The maximum coercivity of 4.6 kOe is obtained from an optimally annealed $Nd_6(Fe_{0.9}Co_{0.1})_84B_6Nb_3Cu_1$ alloy, resulting in the maximum energy product of 10.6 MGOe.

• Korean Journal of Metals and Materials
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• 제47권12호
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• pp.797-810
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• 2009

A study was made of the effects of a Sn addition on the microstructure and microfracture mechanism of squeeze cast AZ51-xSn magnesium alloys. Microstructural observation, in situ fracture testing, and fractographic observations were conducted on these alloys to clarify the microfracture process. The microstructural analyses indicated that $Mg_2Sn$ particles as well as $Mg_{17}Al_{12}$ particles precipitated mainly along the solidification cell boundaries; the volume fraction of these hard particles increased as the amount of added Sn increased, with increased the strength. From in situ fracture observations of the AZ51-7Sn alloy, coarse precipitates located on the cell boundaries worked as easy crack propagation sites and caused abrupt intercellular fracturing. On the other hand, the overall fracture properties of the AZ51-3Sn alloy improved because crack propagation proceeded into the Mg matrix rather than into the cell boundaries as twins developed actively, as confirmed by an R-curve analysis. These findings suggest that the addition of 3~5 wt.% Sn is effective in improving both the tensile and fracture properties on the basis of well-developed twins, the blocking of crack propagation, and crack blunting.

• Korean Journal of Materials Research
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• 제6권1호
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• pp.12-21
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• 1996

AI-1wt%Si합금을 대상으로하여 가열주형을 이용한 수평식연속주조법에 의해 경면에면서 일방향고조직을 가진 주괴를 얻기위한 주조조건을 조사하였으며, 일방향응고된 주괴를 이용하여 신선가공하였을 경우의 다이스배열과 작업조건, 연속주조조건과 신선가공시의 단선율과의 관계를 검토하였다. 그 결과, 직경 8mm 및 4mm 주괴 모두 공정 Si상이 비교적 균일하게 분포되어 있음을 확인할 수 있었고, 이들 주괴를 중간소둔없이 20$\mu\textrm{m}$까지의 초극세선가공이 가능했다. 본 연구에서 실시한 극세선의 신선가공중에 발생한 단선은 신선가공중의 작업조건의 불충분에 기인하는 것으로 사료되었다. 따라서, 본 연구에서 얻어진 일방향응고주괴는 극세선제조에 매우 우수한 원소재임을 보여주었다.

• Journal of applied mathematics & informatics
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• 제30권3_4호
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• pp.499-510
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• 2012

Here we consider the inertial effect in a horizontal mushy layer during solidification of a binary alloy. Using perturbation technique, we obtain two systems, one of zero order and the other of first order. We consider a mushy layer with an impermeable mush-liquid interface and of constant permeability. The analysis reveals that the effect of inertial parameter is stabilizing in the sense that the critical Rayleigh number at the onset of motion increases by the inertial effect.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 한국소성가공학회 2003년도 추계학술대회논문집
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• pp.60-63
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• 2003

Semi-solid forming is the process of stirring alloy during solidification, making the mixture of liquid and solid, solidifying it, reheating it to the solid-liquid coexistent temperature, and then injecting this semi solid slurry into dies. In the semi-solid die casting process, it is very important to find out the correlation of injection condition, microstructure and mechanical properties. Especially, an improper injection condition is the main cause of liquid segregation and non-homogeneous mechanical properties due to the difference of solid fraction according to the position of the products. To ensure the database requisite to the semi-solid die casting product, it is essential to acquire the mechanical properties considering liquid segregation to the injection condition. In this study, the effect of injection condition on liquid segregation, formability, microstructure and mechanical properties in a thin product was investigated.

• Journal of the Korean institute of surface engineering
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• 제17권2호
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• pp.29-40
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• 1984

The structure of rapidly solidified Al-Si-based alloys and its relationship to subsequent anodic film growth in near neutral and acid solutions have been investigated. Solidification of the alloys proceeds via pre-dendritic nuclei, associated with rugosity of the casting surface, from which cellular-type growth, comprised of aluminium-rich material surrounded by silicon-containing material, emanates. Observation of ultramicrotomed sections of the alloys and their anodic films reveals the local oxidation of the silicon-rich phase and its incorporation into the anodic alumina film, formed in near neutral solutions. Such incorporation occurs but resultant isolation of the silicon-rich phase is not possible for anodizing in phosphoric acid, and a three-dimensional network of the oxidized silicon-containing phase, with continuing development of porous anodic alumina, is observed.

• Laser Solutions
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• 제4권1호
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• pp.39-48
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• 2001

This study was performed to evaluate basic characteristics of electron beam weldability for high strength aluminum alloys. The aluminum alloys used were A5083 and A6N01, and A7N01. The principal welding process parameters, such as accelerating voltage, beam current, welding speed and chamber pressure were investigated. The dimension and microstructure of welds were evaluated with OLM, and SEM (EDAX). In addition, weldability variation(cracking) due to process parameters was also evaluated. The degree of cracking in the EB fusion zone appears to be affected mainly by aspect ratio, such that as aspect ratio increases the cracking tendency also increases. The alloying element itself may also affect the hot cracking resistance, but its role is considered to be indirect effect such that the relatively higher vaporization pressure elements of Zn and Mg give deeper weld penetration and thus results in greater cracking tendency.

• Journal of Korea Foundry Society
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• 제10권6호
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• pp.495-502
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• 1990

A basic heat flow model has been developed to estimate the heat transfer coefficient at the casting/mold interface during squeeze casting. Based on the measured temperature profiles in squeeze casting of Al-4.5%Si alloy, heat transfer coefficients which vary with time were calculated by numerical method. The influences of the load and the amount of fraction solid on the heat transfer coefficient have also been studied. Using the calculated heat transfer coefficient two dimensional solidification analysis in the squeeze casting process was carried out by the finite difference method, and the results were in good agreement with the experiments. It may be concluded that heat flow analysis in the squeeze casting process with accurate heat transfer coefficient at the casting /mold interface is important for a proper design of cooling in die and finally for improving productivity and die life as well.