• Title/Summary/Keyword: Al$_2$O$_3$/Al composite

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Preparation of $Al_2O_3-SiC$ Composite Powder by SHS Method (SHS법에 의한 $Al_2O_3-SiC$ 복합분말의 합성)

  • 이형민;이홍림;이형직
    • Journal of the Korean Ceramic Society
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    • v.32 no.1
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    • pp.11-16
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    • 1995
  • High reaction heat evolved from the oxidation of Al was used to synthesize SiC, which might be difficult to be formed by SHS. Al2O3-SiC composite powder was easily manufactured using KNO3 as an ignition and reaction catalyst. Unreacted Si and C were observed after reaction dependent upon the composition of starting powders, reaction atmosphere and relative densities of compacted bodies. The unreacted carbon could be removed by calcining at $600^{\circ}C$ and the remaining Si could be removed by dissolving in NaOH solution. The final powder particles were smaller than 1${\mu}{\textrm}{m}$ in size.

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Study on Properties of Al2O3-TiO2 Composites by Wet Method I. Mechanical Properties of Al2O3-TiO2 Composites(2) (습식법에 의한 Al2O3-TiO2 복합체의 합성 및 특성연구 I. Al2O3-TiO2 복합체의 기계적 특성(2))

  • Ryu, Su-Chak
    • Journal of the Korean Ceramic Society
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    • v.39 no.2
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    • pp.153-158
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    • 2002
  • $Al_2O_3$ composites powders with 1∼11 wt% $TiO_2$ were prepared by wet method and sintered at 1350$^{\circ}C$, 1450$^{\circ}C$ for 2h. Mechanical properties and microstructural evolution were investigated in this study. $Al_2O_3$-3 wt% $TiO_2$ composite were high bulk density of 2.37 g/$cm^3$ and low apparent porosity of 6.3%. The composites containing of 3 wt% $TiO_2$ showed moderately high bending strength of 68.9 MPa and the young's modulus of 35.5 MPa. The composites with increasing $TiO_2$ contents exhibit reduced thermal expansion coefficient due to the formation of $Al_2TiO_5$ phase.

Synthesis and Application of Nanoparticulate Aluminosilicate Sols (II) Mixed Al_2O_3-SiO_2$ Sols (극미세 입자 Aluminosilicate계 졸의 합성 및 응용 (II) Al_2O_3-SiO_2$계 혼합졸)

  • 현상훈;김승구;이성철
    • Journal of the Korean Ceramic Society
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    • v.32 no.1
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    • pp.63-70
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    • 1995
  • A crack-free ceramic composite membrane with micropores has been synthesized by the pressurized sol-gel coating technique using the mixed Al2O3-SiO2 sols. The mixed sols were prepared by mixing nanoparticulate SiO2 and boehmite sols. These sols were more stable at lower pH, but very unstable when their copositions were in the range of 50~75mol% of SiO2 at the same pH. The mixed Al2O3-SiO2 membrane prepared from the mixed sol (0.2mol/$\ell$ of solid content and pH=2) containing 40mol% of SiO2 had the mean pore radius of 0.80nm and the specific surface area of 280$m^2$/g. The nitrogen permeability through the coated Al2O3-SiO2 layer was 42$\times$107mol/$m^2$.s.Pa. It was found that the thermal stability of aluminosilicate membranes, even through similar to that of SiO2 membranes, was much improved in comparison with ${\gamma}$-alumina membranes.

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Fabrication of 4.25 Co0.53Fe0.47-Al2O3 Composite by High Frequency Induction Heated Combustion Synthesis (고주파유도가열 연소합성에 의한 4.25 Co0.53Fe0.47-Al2O3 복합재료 제조)

  • Park, Na-Ra;NamKung, Hoon;Ko, In-Yong;Shon, In-Jin
    • Journal of Powder Materials
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    • v.16 no.2
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    • pp.91-97
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    • 2009
  • Nanopowders of $Co_3O_4$ and FeAl were fabricated by high energy ball milling. Dense 4.25 $Co_{0.53}Fe_{0.47}-Al_2O_3$ composite was simultaneously synthesized and consolidated by high frequency induction heated combustion method within 2 min from mechanically activated powders. Consolidation was accomplished under the combined effects of a induced current and mechanical pressure of 80 MPa.

Mechanical Properties of ZTA Composites Fabricated by Reaction Bonding (반응결합에 의해 제조된 ZTA복합체의 기계적 특성)

  • 장복기;백용혁;문종하;이종호
    • Journal of the Korean Ceramic Society
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    • v.34 no.6
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    • pp.577-582
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    • 1997
  • The mechanical properties of Al2O3-ZrO2 composites fabricated by RBAO(reaction bonded aluminium oxide) process were investigated. As the amount of ZrO2 increased the sinstered density of Al2O3-ZrO2 composites decreased slightly, but wear resistance was enhanced. Bending strength of Al2O3-ZrO2 composites increased in proportion to the amount of al in case of a fixed ZrO2 content. When the amount of Al was fixed bending strength reached its maximum value at 25 wt% ZrO2. The fracture toughness(K1c) increased with increasing content of ZrO2, but decreased with increasing Al amount. On the other hand, the fracture mode of Al2O3-ZrO2 composites was the mixed mode of inter-and transgranular fracture.

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Microstructure and Mechanical Properties of Platelet Reinforced Mullite-Zirconia Composites (Platelet 강화 Mullite-Zirconia 복합체의 미세구조와 기계적 성질)

  • 박상엽
    • Journal of the Korean Ceramic Society
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    • v.29 no.10
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    • pp.757-764
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    • 1992
  • The platelet reinforced mullite-zirconia composites were prepared by pressurelss sintering with addition of Al2O3 or SiC platelets. The sintered density of 10 vol% Al2O3 platelet reinforced mullite-zirconia composite was 98.3% at 1700$^{\circ}C$. The fracture strength (290 MPa) and fracture toughness (4.9 MPa$.${{{{ SQRT { m} }}) in the Al2O3 platelet reinforced mullite-zirconia composite were enhanced compared with those of mullite-zirconia due to the crack deflection and load transfer effect of platelets. Whereas, the SiC platelet reinforced mullite-zirconia composite sintered at 1650$^{\circ}C$ showed relatively lower density (95.7%), fracture strength (170 MPa), and fracture toughness (3.9 MPa$.${{{{ SQRT { m} }} than the Al2O3 platelet reinforced mullite-zirconia composite.

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Compositing Modes and Microstructures of $Cu-X(=Al_2O_3,W)_p$ Composite by Centrifugal Spray-Cast Deposition (원심분사주조법에 의한 $Cu-X(=Al_2O_3,W)_p$ 복합재료의 미세조직 및 복합화)

  • Bae, Cha-Hurn;Jeong, Hae-Yong
    • Journal of Korea Foundry Society
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    • v.17 no.5
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    • pp.480-487
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    • 1997
  • Particle reinforced metal matrix composites(MMCs) via a centrifugal spray-cast deposition(CSD) process were fabricated by injecting second phase particles($Al_2O_3$<40${\mu}m$, W<17.3${\mu}m$) into copper melt on the atomizing disc. Compositing modes were investigated by combining microstructures and mathematical modeling between Cu droplets and the reinforced particles injected. The $Cu/W_P$ powders were shown that the W particles penetrate and get embedded in the Cu droplets. It is considered that the W particles composite preferentially in Cu melt on the atomizing disc. On the other hand, the $Al_2O_3$, particles did not penetrate into the Cu droplets on the atomizing disc but get attached in surface of Cu droplets during the flight. It is considered that the compositing may be attained in the flight distance which the relative velocity between Cu droplet and $Al_2O_3$, particle is maximum. The microstructure of the $Cu/W_P$ and the $Cu/(Al_2O_3)_p$ composite preform was strongly influenced by compositing modes of droplets, and after subsequent deposition it was comprised as it is called the dispersed type and the cell type of microstructure, respectively.

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