• Title/Summary/Keyword: Aging heat treatment

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The Study of Restoration Technique of Wax-Treated Volume for the Annals of the Joseon Dynasty(II) - Evaluation of aging characteristics of Korean traditional paper, Hanji as the restoration material of the annals - (조선왕조실록 밀랍본 복원기술연구(제2보) - 실록의 복원용지 탐색을 위한 전통한지의 열화특성 평가 -)

  • Jeong, Seon-Hwa;Jeong, So-Young;Seo, Jin-Ho
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.40 no.2
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    • pp.43-56
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    • 2008
  • The purpose of the experiment was to evaluate the material stability of the paper of the annals of Joseon Dynasty for the conservation purpose and the categories were as listed below : 1. Procuring traditional Hanji and semi-Hanji from different regional hanji paper mill. 2. Artificial accelerated aging treatment to examination its stability (UV irradiation, dry heat) 3. Analysis of optical, physical characteristic. The suitable Hanji for categories would be used as a reconstruction material for the waxel paper in the papers of the annals of Joseon Dynasty.

Precipitation Behavior of Al-Zn-Mg-Cu-(Sc) Alloy (Al-Zn-Mg-Cu-(Sc) 합금의 석출특성)

  • Choi, G.S.;Mun, H.J.;Woo, K.D.
    • Journal of the Korean Society for Heat Treatment
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    • v.19 no.5
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    • pp.257-261
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    • 2006
  • Scandium(Sc) in Al-Zn-Mg-Cu based Al alloy on precipitation phenomenon was compared to a 7001(Al-7.2%Zn-3.2%Mg-1.8%Cu) Al alloy. GP zone and ${\eta}^{\prime}$ phases were the main strengthening phases at low aging temperature under $100^{\circ}C$, but ${\eta}^{\prime}$ and $Al_3Sc$ phases were the main strengthening phases at high aging temperature above $1600^{\circ}C$ in Sc added 7000(Al-7.7%Zn-2.0%Mg-1.9%Cu-0.1%Zr) Al alloy. With the addition of 0.1%Sc in 7000 Al alloy, the activation energy for the GP zone, ${\eta}^{\prime}$ and ${\eta}$ phase decreased compared to the 7001 Al alloy. This result indicates that the Sc accelerated the precipitation for the GP zone, ${\eta}^{\prime}$ and ${\eta}$ phases in 7000 Al alloy. Al-7.7%Zn-2.0%Mg-1.9%Cu-0.1%Zr-0.1 Sc alloy has higher strength than 7001 Al alloy, which has high strength.

Effects of Rare Earth Metals Addition and Aging Treatment on the Corrosion Resistance and Mechanical Properties of Super Duplex Stainless Steels

  • 박용수;김순태;이인성;송치복
    • Transactions of Materials Processing
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    • v.8 no.3
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    • pp.309-309
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    • 1999
  • Effects of rare earth metals addition and aging treatment on corrosion resistance and mechanical properties of super duplex stainless steels were investigated using optical/SEM/TEM metallographic examination, an X-ray diffraction test, a potentiodynamic anodic polarization test and a tensile test. The performance of the experimental alloy with 0.32% REM addition was compared with commercial super duplex stainless steel such as SAF 2507 when they were exposed to solution annealing heat treatment and aging treatment. The corrosion resistance in CF environments and mechanical properties of the experimental alloy were found superior to those of the commercial duplex stainless steel. The REM with larger atomic radii than those of Cr, Mo and W may fill vacancies inside the matrix and around the grain boundaries, retarding formation of harmful intermetallic σ and χ phases. In addition, fine REM oxides/oxy-sulfides (1-3㎛) seemed to enhance the retardation effects. With REM additions, strength and ductility increased due to the phase and grain refinement caused by fine REM oxides and oxy-sulfides.

Effect of long-term thermal aging on the microstructural and mechanical characteristics of nickel-based alloy weldment (니켈계 합금 용접부의 미세조직 및 기계적 특성에 대한 장기 열적 시효의 영향)

  • Yoo, Seung Chang;Ham, Junhyuk;Kim, Ji Hyun
    • Transactions of the Korean Society of Pressure Vessels and Piping
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    • v.12 no.1
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    • pp.41-48
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    • 2016
  • To investigate the effect of long-term thermal aging on the microstructural and mechanical characteristics of weldment made of nickel base alloy and its weld metal, an accelerated heat treatment was applied to simulate the process of long-term thermal aging in the operating condition of nuclear power plant. A representative nickel-based weldment with Alloy 600 and Alloy 182 was fabricated and heat-treated at $400^{\circ}C$ for 1,713 h and 3,427 h to simulate the thermal aging for the period equivalent to 15 and 30 years in operating pressurized water reactors, respectively. The microstructural and mechanical characteristics were analyzed by using optical microscopy, scanning electron microscopy and Vickers microhardness measurement. Changes were observed in precipitation behavior and microhardness of each specimen, and these changes were mainly attributed to the change in precipitated morphology and residual stress across the weld during the thermal aging process.

Effect of Dewaxing Ratio of Beeswax-treated Hanji by Heat and Pressure Method on Aging Behavior of Dewaxed Hanji (가온 가압법에 의한 밀랍도포한지의 탈랍율이 탈랍지의 열화 거동에 미치는 영향)

  • Cho, Byoung-Uk;Choi, Do-Chim;Jo, Byoung-Muk
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.44 no.3
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    • pp.15-21
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    • 2012
  • The optimum dewaxing ratio in dewaxing treatment by the heat and pressure method was investigated by considering aging stability of dewaxed Hanji. Commercial Hanji was coated with beeswax and thermally aged at $150^{\circ}C$ for 24 hours. Then it was dewaxed using the laboratory sheet press equipped with hot plates on both top and bottom sides. Dewaxing ratio was controlled by pressing temperature and time. Four type of dewaxed Hanji samples with different dewaxing ratio were prepared and thermally aged at $150^{\circ}C$. Then the aging stability of dewaxed Hanji samples was evaluated in terms of optical and strength properties. It was found that the aging stability of dewaxed Hanji was superior with higher dewaxing ratio. The result concluded that, in the aspect of aging stability, the coated beeswax in beeswax-treated Hanji shall be completely removed if the coated wax would be dewaxed.

Effect of Content on the Mechanical Properties of a 18 Ni Maraging Steel (18 Ni 마르에이징 강의 기계적 성질에 미치는 Mo 첨가량의 영향)

  • Kim, Hak-Mo;Kim, In-Bae;Park, Se-Yoon
    • Journal of the Korean Society for Heat Treatment
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    • v.4 no.3
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    • pp.7-12
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    • 1991
  • Effects of Mo content and aging conditions on the amount of retained austenite and mechanical properties of 18 Ni maraging steels were investigated. Maraging steels were fabricated with variation of Mo content. 3, 5, 7, 9% and heat treated by austenitizing at $840^{\circ}C$ for 1 hour and then aged at $480^{\circ}C$ for 0.5~100 hours. It was found that the amount of retained austenite after aolution treatment was negligible up to 5% Mo. 8 and 11 volume percents of retained austenite were obtained with 7 and 9% Mo respectively. The maximum hardness and yield strength without great loss of impact toughness were attained in the range of 4~8 hours of aging time at $480^{\circ}C$ with 5% Mo. It was concluded, as a result, that the optimum Mo content for the good combination of strength and toughness is to be 5% Mo.

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Aging Behavior and Effect of Heat Treatment on High Temperature Mechanical Properties in Ti-15V-3AI-3Cr-3Sn (Ti-15V-3Al합금의 시효거동과 열처리에 따른 고온 기계적 특성)

  • Lee Jae Won;Lee Back-Hee;Lee Kyu Hwan;Kim Young Do
    • Korean Journal of Materials Research
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    • v.14 no.1
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    • pp.13-18
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    • 2004
  • Titanium alloys are the one of promising candidate materials for medium high temperature parts in the aircraft, automobile, petrochemistry and electrochemistry because of their high strength with low density in medium high temperature. In this study, the effects of aging and heat treatments on the mechanical properties of Ti-15-3 alloy in medium high temperature, which was $400^{\circ}C$, were studied. Solid solution treatment was performed at $8000^{\circ}C$ of $\beta$ phase region for 1 h and the alloy was quenched in water. The alloy was aged at $5000^{\circ}C$ of $\alpha$ and $\beta$ two-phase region for 1, 2, 4, 8, ... and 100 h to increase the mechanical property. The $\beta$ single phase was observed at all parts of specimens in Ti-15-3 alloy after ST. As the aging at $500^{\circ}C$, fine precipitates of a phase was generated from matrix of $\beta$ phase and the microstructure was consisted of weaving structure such as Widmanstiitten a phase. The most suitable aging time is 24h in$ 400^{\circ}C$. At this time, strength is 1164 MPa and elongation is about 12%. In room temperature, elongation of Ti-15-3 alloy aged at $500^{\circ}C$ for 16 h is poor (=3%) in spite of high tensile strength (1458 MPa).

Microstructural Evolutions and Microhardness of the Heat Treated Ni-base Superalloy Weldment (Ni기 초합금 용접부의 열처리에 따른 미세조직 변화와 미세경도)

  • Kim, G.S.;Ji, J.H.
    • Journal of the Korean Society for Heat Treatment
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    • v.18 no.5
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    • pp.297-304
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    • 2005
  • This study was performed to determine the repair weldability of the damaged Ni type superalloy used for gas turbine blade. The experimental works included the evaluation of the microstructures of the damaged blade, selection of the repair welding procedure, characterization of repair weldment and finding the heat treatment procedures for repaired weldment. The morphology of the microstructure for the base metal was composed of austenite matrix with cubical ${\gamma}^{\prime}$ phase, MC type coarse precipitates located within grain and fine $M_{23}C_6$ type precipitates decorated at grain boundaries. The repair welding process using 90 amp current exhibited the best weld properties showing no weld microcracks. The solution and aging heat treatments of the repaired weldment could recover the original service properties of the damaged blade.

Effects of Different Heat Treatments on Damping Capacity of Cu-55%Mn Alloy (Cu-55%Mn 합금의 진동감쇠능에 미치는 각종 열처리의 영향)

  • Chung, Tae-Shin;Jun, Joong-Hwan;Lee, Young-Kook;Choi, Chong-Sool
    • Journal of the Korean Society for Heat Treatment
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    • v.11 no.1
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    • pp.27-34
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    • 1998
  • Effects of different heat treatments on microstructure and damping capacity of Cu-55%Mn alloy were investigated to find an optimum heat treatment condition for a maximum damping capacity. The alloy showed the high level of damping capacity in case of the aging at 375 and $400^{\circ}C$. This is ascribed to the FCC${\rightarrow}$FCT martensitic transformation and microstructural changes from mottled to tweed band type. The damping capacity had a maximum value of 0.33 in logarithmic decrement when the alloy was aged at $375^{\circ}C$ for 14 hours followed by 20 times of thermal cycling between room temperature and $250^{\circ}C$. The refinement of tweed structure by thermal cycling is thought to be responsible for the highest damping capacity.

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A study on the heat treatment processing of 7050 aluminum alloy (7050Al 합금의 열처리공정 개발에 관한 연구)

  • Lee, H.S.;Nam, T.W.;Lee, B.K.
    • Journal of the Korean Society for Heat Treatment
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    • v.9 no.2
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    • pp.139-146
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    • 1996
  • The aero-industry is union industry which includes a research development type, a knowledge accumulation type and a developed country type. The aero-industry of Korea is in semi-developed type stage but departed later than that of other country such as Taiwan, Indonesia etc. Therefore, the necessity of domestic airplane material is required. This study on 7050Al extruded alloy aims to suggest an adequate heat treatment conditions of T73, T74 and T76. The results of this study show that; 1. The optimum conditions of T7x heat treatment in extruded 7050Al alloy show this; $$T73:121^{\circ}C{\times}7hr+177^{\circ}C{\times}14hr$$. $$T74:121^{\circ}C{\times}7hr+177^{\circ}C{\times}10hr$$. $$T76:121^{\circ}C{\times}7hr+163^{\circ}C{\times}21hr$$. 2. The 2nd step aging heat treatment such as T73, T74 and T76 etc. is efective in 7050Al alloy but the variation otf microstructure and mechanical property with dispersive inclusions produced for extrusion process causes some troubles. Accordingly, in order to produce a good 7050Al alloy, a careful attention is needed in manufacturing process.

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