• Title/Summary/Keyword: Aging Property

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A Study on the Correlation between Advanced Small Punch Test and Charpy V-notch Test on X20CrMoV121 and 2.25Cr1Mo steels Weldment (X20CrMoV121강과 2.25Cr1Mo강 용접부의 ASP 시험과 CVN 충격 시험의 상관관계에 대한 연구)

  • Lee, Dong-Hwan;Kim, Hyoung-Sup
    • Journal of Welding and Joining
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    • v.26 no.3
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    • pp.37-44
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    • 2008
  • Charpy V-Notch test is commonly used to evaluate fracture toughness. However, since the region to be evaluated is limited to bulk material due to the specimen size required, individual evaluation of micro-structures on weldment is very difficult. In this study, ASP(Advanced Small Punch) test was carried out to evaluate material degradation and fracture toughness on the B.M, W.M and each micro-structures of HAZ for X20CrMoV121 and 2.25Cr1Mo steels with artificial aging time. In addition, to evaluate fracture toughness and material degradation of B.M and W.M of X20CrMoV121 steels with aging times, CVN (Charpy V-notch) test was performed. And then the correlation between ASP and CVN test on X20CrMoV121 steels was obtained. Furthermore, through this correlation, material degradation property of each micro-region of the HAZ in weldment, which was impossible to be evaluated by the CVN test, can be estimated and determined.

Preparation and Interface Properties of Colloidal Silica (콜로이드 실리카의 제조 및 계면특성)

  • Lee, Han Chul;Kim, Jong Hyub;Chang, Yoon Ho
    • Applied Chemistry for Engineering
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    • v.17 no.4
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    • pp.386-390
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    • 2006
  • Colloidal silica which has high surface area and excellent surface properties are chemically stable inorganic materials and used for various applications in industry. Silica sol was prepared from sodium silicate solution by acid neutralization method and ion exchange treatment to remove sodium ions. Through the experimental analysis for controlling factors of particle growth rate, such as temperature, pH, and aging time, the uniform size distribution of silica sol could be obtained. The size distribution and shape of silica sol was measured by TEM and dynamic light scattering method. Zeta potential change and gelling phenomena of silica sol and its rheological properties also investigated.

Effect of Soxhlet Extraction Condition on Dewaxing Efficiency of the Beeswax-Treated Paper (속실렛 추출법에 의한 밀랍지의 탈랍처리 효과분석)

  • Choi, Kyoung-Hwa;Jang, Hye-Mi
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.45 no.5
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    • pp.64-70
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    • 2013
  • In this study, the effect of soxhlet extraction on dewaxing of the aged beeswax-treated paper was examined. To do this, soxhlet extraction of the aged beeswax-treated paper performed with different reflux conditions and then measured the dewaxing efficiency and change in the various properties such as tensile strength, folding endurance, color and brightness. Also, an artificial aging test was executed in order to investigate the effect of soxhlet extraction on the preservability of the dewaxed paper. As the result of FT-IR analysis, a peak area of CH and COOH group, which are main band of beeswax, was decreased or removed after soxhlet extraction. The decreasing rate of each peaks were increased depending on reflux time. After dewaxing, the physical property such as MIT type folding endurance and tensile strength was decreased. And $L^*$ value and brightness were increased while $a^*$ and $b^*$ value were decreased due to the remove of color compounds in beeswax. The more color deviation (${\Delta}E$) is expected with higher reflux times. As the result of artificial aging, preservability of two dewaxed papers except of DP_SE(C) sample was higher than that of untreated paper i.e. beeswax-treated paper.

Tracking Performance Test of Polymer Insulator with Salt Solution which is added Surface Active Agent (계면활성제가 첨가된 염수용액에 따른 폴리머 애자의 트래킹 성능 평가)

  • Cho, Han-Goo;Han, Dong-Hee;Lee, Un-Yong;Lim, Kee-Joe;Choi, In-Hyuk
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.07b
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    • pp.1121-1124
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    • 2004
  • Aging test to estimate life property of polymer insulator is executed through several international standard such as IEC 61109 and CEA tracking wheel test, but is not getting clear conclusion yet. There are two methods in the diagnosis method of polymer insulator such as off-line and on-line. The diagnosis methods in off-line are external condition analysis by the eye, contaminant analysis on surface, surface analysis, pollution withstand voltage test, power frequency flashover voltage test, lightning impulse flashover test, tensile fracture load test and flexural load test. The diagnosis methods in off-line most are the method for virgin and last aged sample. However, the diagnosis method in on-line is method that can be evaluate sample state as progressing continuously aging test in beginning, The diagnosis method in on-line is arranged as following: leakage current measurement, electric field, surface state investigation, thermal image, emitting light measurement and then so. In this paper, the tracking performance of polymer insulator with salt solution which is added surface active agent. The diagnosis of insulator sample has been analyzed by leakage current and visual examination.

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Cure Characteristics, Mechanical Properties, Abrasion Property and Thermal Properties of EVM/EPM Blends Containing Flame Retardants

  • Sung, Il Kyung;Lee, Won Ki;Park, Chan Young
    • Elastomers and Composites
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    • v.52 no.2
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    • pp.105-113
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    • 2017
  • The curing behavior, mechanical properties, hot-air aging resistance, abrasion properties,thermal properties, etc., of EVM/EPM/APP (ammonium polyphosphate)/DPER (dipentaerythritol)/EG (expandable graphite) and EVM/EPM/ATH (aluminium trihydroxide) flame retarding systems in ethylene vinyl acetate rubber (EVM) blends with EPM (ethylene propylene rubber) were sequentially examined. For both flame retarding systems, the torque values increased with the content of EPM rubber and with the vulcanization time. As the content of EPM rubber increased, the scorch time became shorter, whereas the optimum cure time followed an increasing trend. For the EVM/EPM/APP/DPER/EG flameretarding system, as the content of EPM rubber increased, the hardness did not change,whereas the tensile strength and elongation at break decreased. A hot-air aging resistance test at $150^{\circ}C$ showed that the heat resistance decreased with the EPM content regardless of the kinds and contents of flame retardants. As the EPM content increased, the abrasion rate became higher and the abrasion resistance of the EVM/EPM/APP/DPER/EG flame retarding systems exceeded that of the EVM/EPM/ATH flame retarding counterparts. In comparison with the EVM/EPM/ATH flame retarding systems, the thermal stability of the EVM/EPM/APP/DPER/EG flame retarding system showed an increasing tendency.

Lifespan-extending Effects of Allium hookeri Leaves in Caenorhabditis elegans (삼채 잎 추출물의 예쁜꼬마선충에 대한 수명연장 효과)

  • Ki, Byeolhui;Lee, Eun Byeol;Kim, Jun Hyeong;Yang, Jae Heon;Kim, Dae Keun;Kim, Young-Soo
    • Korean Journal of Pharmacognosy
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    • v.48 no.4
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    • pp.314-319
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    • 2017
  • To evaluate the longevity property of Allium hookeri (Liliaceae) leaves, this study was performed. Ethanol extract of A. hookeri was successively partitioned as methylene chloride, ethyl acetate, n-butanol and $H_2O$ soluble fractions, and lifespan-extending effects of the fractions were checked using Caenorhabditis elegans model system. The most active ethyl acetate-soluble fraction elevated heat stress tolerance, and increased expression of stress resistance protein. Further studies were performed to investigate several aging-related factors such as reproduction, food intake, growth and movement of C. elegans. The results revealed that there were no significant changes in aging-related factors including reproduction and food intake, however, ethyl acetate-soluble fraction treatment led to up-regulation of locomotory ability and growth of aged worms, suggesting ethyl acetate-soluble fraction affected healthspan as well as lifespan of nematode.

Accelerated Weathering Test of Urethane Paint for Heavy Construction Equipment (중장비용 우레탄 도료 내후성 가속시험)

  • 김대용;김영준
    • Journal of Applied Reliability
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    • v.1 no.2
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    • pp.79-93
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    • 2001
  • Recently, new aspects of paints such as a beautiful appearance, use of environmentally friendly paints, etc., in addition to the superior performance of paints have been requested for industrial paints including the paints for heavy construction equipment and others. Particularly, the quality of appearance of coating affects the sales of heavy construction equipment. And the necessity for the paints to have a superior weather-proof property without changing the luster or color even after long-time exposure to the open air is emphasized. The change in the surface color and luster of the paint due to the natural environment progresses very slowly, and it takes a long time to verify material properties when developing new paints. In order to improve such methods, weathering tests are performed in many laboratories as a test for accelerating aging of coating, and the lifetime of the products is estimated through evaluation of the weathering (environment-proof) quality of paints. However, not a great deal of research activity has been conducted up to the present time since the interrelationship between the actual results of testing and field data is different for each paint and it takes a long time to study relevant materials. Therefore, introduced in the present study is the estimation of the change in the quality of appearance of coating in the field through the accelerated aging test among the cases of improvement of the quality of appearance of the urethane paint for heavy construction equipment.

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Study on Accelerated Life-time Test of O-ring Rubber by Thermal Stress (열 스트레스에 의한 고무 오링의 가속수명시험에 관한 연구)

  • Shin, Young-Ju;Chung, Yu-Kyung;Choi, Kil-Yeong;Shin, Sei-Moon
    • Journal of Applied Reliability
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    • v.7 no.1
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    • pp.31-43
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    • 2007
  • The function of O-ring seals is to prevent leakage during the service life of the components in which they are installed. The life prediction of O-ring is very important at various industry fields. Generally, to evaluated the long-term performance of O-ring in severe environments has applied a life prediction technique based on accelerated life test (ALT). In this work, Accelerated thermal aging test(l20, 130, 140, $150^{\circ}C$) of O-ring was applied for life prediction of O-ring. The property changes after thermal aging test was measured using TGA, DSC, FT - IR, Video Microscope and SEM. Shape parameter and life prediction were obtained using MINITAB program.

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Effect of Surface Morphology and Adhesion Force on the Field Emisson Properties of Carbon Nanotube Based Cathode (탄소나노튜브 캐소드의 전계방출 특성에 대한 표면 형상과 부착력의 영향)

  • Jung, Hyuk;Cho, You-Suk;Kang, Young-Jin;Kim, Do-Jin
    • Korean Journal of Materials Research
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    • v.18 no.5
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    • pp.277-282
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    • 2008
  • The effects of the field emission property in relation to the surface morphology and adhesion force were investigated. The single-wall-nanotube-based cathode was obtained by use of an in-situ arc discharge synthesis method, a screen-printing method and a spray method. The morphologies of the formed emitter layers were very different. The emission stability and uniformity were dramatically improved by employing an in-situ arc discharge synthesis method. In this study, it was confirmed that the current stability and uniformity of the field emission of the cathode depend on the surface morphology and adhesion force of the emitters. The current stability of the field emission device was also studied through an electrical aging process by varying the current and electric field.

Evolution of Microstructure and Mechanical Properties of Porous Al Alloy Under Various Heat Treatment (열처리에 따른 다공성 알루미늄 합금 재료의 미세구조와 기계적 성질 변화)

  • 류관무;권영재;김준규;조원승;조남희;황진명;유연철
    • Transactions of Materials Processing
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    • v.12 no.6
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    • pp.588-596
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    • 2003
  • The relationships between evolution of microstructure and mechanical properties of porous Al-3Si-2Mg-2Cu alloy after the foaming and various heat treating were investigated. The foamed alloy having various densities were manufactured by powder compact foaming and heat treated. Then compression test was performed with deformation rate of 0.5/s. The ultimate compression strength was not changed after solution heat treatment but the flow curve after ultimate strength showed very smooth and uniform plateau region. This change of flow curve means that the deformation mechanism is altered from brittle fracture to ductile deformation and the energy absorption property of Al foam is dramatically improved. The improvement of energy absorption without any detriment of mechanical properties is due to that the very brittle precipitation like Al-Cu and Al-Mg was uniformly dissolved in Al matrix after solution heat treatment. And various mechanical properties of Al alloy porous material were improved by 40% with aging of $200^{\circ}C$ and 50min. These improvements are ascribe to the various fine precipitates like $\Omega$ and $\theta$'.