• Title/Summary/Keyword: Age Hardening

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Rapidly Solidified Microstructure and Phase Decomposition of Al-Cr alloys by the Single Roller Method (Single Roller법에 의한 Al-Cr 계 합금의 급냉응고 조직과 상분해)

  • Cho, Soon-Hyoung;Yoon, Eui-Pak
    • Journal of Korea Foundry Society
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    • v.7 no.2
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    • pp.108-113
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    • 1987
  • Al-Cr alloy with composition in the range from 1.5 wt% to 10 wt% Cr were rapidly solidified from the melt by the single roller method. The supersaturated solid solution was obtained up to 6 wt% Cr in Al-Cr alloy for $20{\mu}m$ thickness. Lattice parameter decreased with increasing Cr content at the rate of 0.00456A per wt% Cr up to 6 wt% Cr. Microhardness increased with increasing Cr content at the rate of $10\;Kg/mm^2$ per wt% Cr up to 6 wt% Cr. Microhardness measurements on the Al-6 wt% Cr supersaturated solid solution annealed isothermally showed no sign of age hardening. Decomposition temperature, determined by lattice parameter changes and microhardness changes, was $470^{\circ}C$ for Al-6 wt% Cr supersaturated solid solution. Transmission electron microscopy showed that decomposition within one hour below $400^{\circ}C$ occurred at grain boundaries only, and also the additional decomposition within grains being evident at $450^{\circ}C$ The coarse precipitate structure showed at $500^{\circ}C$ and $550^{\circ}C$, respectively. The coarse precipitate structure is considered $Al_7Cr$.

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Evaluation of Age-Hardening Characteristics of Rheo-Cast A356 Alloy by Nano/Micro Hardness Measurement (나노/마이크로 경도 측정에 의한 레오캐스트 A356 합금의 시효경화특성 평가)

  • Cho S. H.;Youn S. W.;Kang C. G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2005.05a
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    • pp.471-474
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    • 2005
  • This study investigates the nano/microstructure, the aging response, and the mechanical/tribological properties of the eutectic regions in rheoformed A356 alloy-T5 parts using nano/micro-indentation and mechanical scratching, combined with optical microscopy and atomic force microscope (AFM). Most eutectic Si crystals in the A356 alloy showed a modified morphology as fine-fibers. The loading curve for the eutectic region was more irregular than that of the primary Al region due to the presence of various particles of varying strength. The aging responses of the eutectic regions in the rheoformed A356 alloys aged at $150^{\circ}C$ for different times (0, 2, 4, 8, 10, 16, 24, 36, and 72 h) were investigated. Both Victors hardness $(H_v)$ and indentation $(H_{IT})$ test results showed a similar trend of aging curves, and the peak was obtained at the same aging time of 10 h. A remarkable size-dependence of the tests was found.

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Effects of Zn Addition on Hardness and Microstructure of Discontinuous Precipitates in Isothermally Aged Mg-Al-(Zn) Alloys (등온 시효한 Mg-Al-(Zn) 합금에서 불연속 석출물의 경도와 미세조직에 미치는 Zn 첨가의 영향)

  • Jun, Joong-Hwan
    • Journal of the Korean Society for Heat Treatment
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    • v.35 no.4
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    • pp.177-184
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    • 2022
  • The present study aims to investigate the influence of Zn addition on hardness and microstructural characteristics of discontinuous precipitates (DPs) formed by isothermal aging in Mg-9%Al and Mg-9%Al-1%Zn alloys. To obtain large DPs volume fractions in the microstructure, the alloy specimens were solution-treated at 688 K for 24 h followed by water quenching, and then aged at 413 K for 48 h. The aged Mg-9%Al-1%Zn alloy had higher DPs content than the Mg-9%Al alloy, indicating that the Zn addition plays a beneficial role in enhancing age-hardening response. The DPs in the Zn-containing alloy possessed the higher hardness than those of the Zn-free alloy. Microstructural examination revealed that the increased hardness of the DPs resulting from the Zn addition is closely associated with the lower α-(Mg)/β(Mg17Al12) interlamellar spacing and the higher volume fraction of β phase layer of the DPs.

Characteristics of Intrusion MO and Perception of Target Hardening of Burglars (침입절도범 재소자의 수법 특성과 타겟하드닝 관련 인식)

  • Park, Hyeonho;Kim, Kang-Il;Kim, Hyo-gun
    • Korean Security Journal
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    • no.60
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    • pp.33-61
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    • 2019
  • It is quite difficult to actually prove the effectiveness of so-called target-hardening, one of the various strategies used to reduce crime, one of the serious problems in society recently. In particular, three to five minutes is often used as golden time for intruders to give up or stop, which is based on foreign and some indirect research cases in Korea, but there were no studies that more directly identified the average break-in operation time or the abandonment time based on the elapsed time when the shield hardware resists intruders. This study was the first of its kind in Korea to investigate and verify samples of 90 inmates of break-in burglars who were imprisoned in August 2018 by profiling the average criminal experience, education level, age, height and weight of typical Korean professional break-in thieves, and specific criminal methods, average break-in operation time, and the criteria for giving up if not breached. According to the analysis results, in the survey on the number of pre-invasion theft crimes by intruders, many of the respondents who participated in the survey were criminals of professional invasions, and by their physical characteristics, there was not much difference from ordinary adult men. Residential facilities were the highest in the world, followed by commercial and educational facilities. According to the survey on the types of facilities that committed intrusion into residential facilities, it was not safe to say that single-family housing accounted for the largest portion of single-family housing, multi-family housing, apartment high-rise (more than three stories), and apartment low-rise (more than one to three stories) among residential facilities, and that the ratio of apartment high-rise was higher than expected. Based on the average time required to break into a place for an intrusion crime, it is assumed that the psychological time worked in a place where the break-in was difficult, since the break-in was not performed while measuring the time of the break-in operation. In the case of time to give up a crime, more than half of the respondents said they would give up the crime even in less than four minutes, suggesting that a significant number of intrusive crimes can be prevented even if the facility has four minutes of intrusion resistance. This proves that most intruders will give up the break-in if the break-in resistance performance of the security facility is exercised for more than five minutes.

Engineering Character of Ultra Rapid Hardening Concrete-Polymer Composite using CAC and Gypsum Mixed CAC (CAC 및 석고혼입 CAC를 사용한 초속경 콘크리트-폴리머 복합체의 공학적 특성)

  • Koo, Ja Sul;Yoo, Seung Yeup;Kim, Jin Man
    • Journal of the Korea Institute of Building Construction
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    • v.16 no.2
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    • pp.97-105
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    • 2016
  • Recently, application case of the ultra rapid hardening concrete-polymer composite(URHCPC) are increasing to repair for the deterioration of pavement. But it is a major disadvantage that the main material is expensive and has environmental load. For these reasons, the development of the economic, eco-friendly materials is needed. Calcium Aluminate Composite (CAC), produced by rapid cooling of atomizing method with molten ladle furnace slag, is a material capable of improving the economic feasibility and reducing the environmental load of URHCPC. In this paper, the properties of CAC and gypsum mixed CAC (GC) as alternative materials of RSC according to the types of polymer dispersion were studied. The results were as follows; compressive strength, tensile strength, flexural strength, bonding strength and modulus of elasticity of the composites using CAC or GC showed higher values than those of plain proportion in 3 hour. In later age, they were at the same level as the general proportions. URHCPC using BPD as polymer dispersion had superior strength properties generally. But modulus of elasticity was the same level as the case of using a SBR latex. According to these results, CAC or GC can partially substituted for RSC to product the URHCPC. When URHCPC uses the BPD as the polymer dispersion, it can be improved performance.

Manufacturing Properties and Hardening Characteristic of CO2 Reactive Hardening Cement (이산화탄소 반응경화 시멘트 제조 및 경화특성 연구)

  • Ki-Yeon Moon;Byung-Ryeol Kim;Seung-Han Lee;Moon-Kwan Choi;Kye-Hong Cho;Jin-Sang Cho
    • Resources Recycling
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    • v.31 no.6
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    • pp.52-59
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    • 2022
  • Calcium silicate based cement (CSC) is a low-carbon cement that emits less CO2 by up to 70% compared to ordinary Portland cement during its manufacture. Most developed countries have commercialized CSC, whereas Korea is still investigating the manufacturing characteristics and basic properties of CSC. This paper provides a review of methods for manufacturing CSC using domestic raw materials and discusses the possibility of CSC localization based on an evaluation of the basic physical properties of manufactured CSC. The experimental results of this study indicate that the primary mineral components of CSC were CS, C3S2 C2S, and unreacted SiO2. This suggests the possibility of manufacturing CSC using domestic raw materials that exhibit mineral compositions similar to that of theoretical CSC. The compressive strength of CSC mortar is less than 1MPa at the age of 7 d under wet curing. This implies that hydration does not affect the property development of CSC mortar. Meanwhile, during carbonation curing, the compressive strength is 56 MPa or higher after 7 d, which indicates excellent early strength development. Furthermore, results of Thermogravimetric Analysis Differential scanning calorimetry (TG/DSC) show that a significant amount of CaCO3 is formed, which is consistent with the results of previous studies. This implies that carbonation is associated significantly with the properties of CSC.

An Experimental Study on the Evaluation of Early-Age Mechanical Properties of Polymer-Based Thin Spray-on Liners (폴리머 기반 박층 라이너의 초기재령 특성 평가를 위한 실험적 연구)

  • Chang, Soo-Ho;Lee, Gyu-Phil;Han, Jin-Tae;Park, Young-Taek;Choi, Soon-Wook;Hwang, Gwi-Sung;Choi, Myung-Sik
    • Tunnel and Underground Space
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    • v.23 no.5
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    • pp.413-427
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    • 2013
  • Thin Spray-on Liners(TSLs) based on polymer materials have been considered as an alternative to shotcrete and wire mesh in relatively fair rock conditions, and used in mines since 1990s. Nevertheless, Few experimental studies on their mechanical properties necessary for the evaluation of their bearing capacities as a support member have been carried out. In this study, tensile and bond strengths of two kinds of TSLs with different material compositions were measured at the age of 7 days. In addition, two kinds of bending tests proposed by EFNARC (2008) to simulate representative failure mechanisms of TSLs were carried out on the same materials and curing age as in tension and pull-out tests. From the tests, tensile strength of a TSL is shown to increase as its content of polymer is higher. In contrast, its bond strength seems to be in inverse proportion to its polymer content. Especially, the TSL material in which a cementitious component is included with relatively smaller polymer content shows a faster hardening characteristic which results in higher resistance to de-bonding between a TSL and a substrate. As a result, it is shown that the performance of TSLs might be dependent upon its corresponding polymer content.

Autogenous Shrinkage of Very-Early Strength Latex-Modified Concrete with Latex Contents (라텍스함량 변화에 따른 VES-LMC의 자기수축)

  • Park, Won-Il;Choi, Pan-Gil;Yun, Kyong-Ku;Lee, Bong-Hak
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.11 no.3
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    • pp.1059-1065
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    • 2010
  • Very-early strength latex-modified concrete (VES-LMC) was developed for the purpose of fast-track overlay of a concrete bridge deck under heavy traffic, concentrated on the workability, durability, and strength gain so that it can be opened to the traffic only three hours after its placement. The mixture of VES-LMC might accompany very high heat of hydration at early-age because of its inherent rapid hardening property and could have susceptibility to autogenous shrinkage because of its relatively low water-cement ratio. This study evaluated the effect of the latex-cement ratio(L/C) both of the constant and variable slumps on the autogenous shrinkage of VES-LMC by carrying out simple temperature rise test and early-age shrinkage experiment. Test results are as follows: The latex contributes on the enhancement of the concrete durability but has little effect on its hydration and the accompanied heat of hydration in VES-LMC. Autogenous shrinkage increased with the increase in latex-cement ratio at variable slumps and its pattern followed regularly a logarithmic increase. However, the influence of water-cement ratio and latex-cement ratios for the test specimens at constant slump on early-age autogenous shrinkage property was found to be minor due to the simultaneous effect of the two experimental variables.

Strength and Friction Behavior of Cement paste poured in the Bored Pile (매입말뚝의 시멘트풀 강도 및 마찰거동에 관한 연구)

  • Park, Jong-Bae
    • Journal of the Korean GEO-environmental Society
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    • v.5 no.3
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    • pp.31-39
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    • 2004
  • The bored pile is widely used as a low noise and vibration piling method in Korea. However, there is design tendency to minimize the friction capacity of the bored pile because of uncertainty and the quality control specification is not set up. This research analysed the strength characteristics of cement paste after the uniaxial compression test with various condition. Test results show that the compressive strength of cement paste with w/c=0.83 was up to $156.0kgf/cm^2$, and the lower w/c ratio and the longer age, the strength of cement paste increased. Also the higher soil mixing ratio, the strength of soil cement decreased, and too high soil mixing ratio caused the malfuction of soil cement. Also this research analysed the 188 dynamic pile test results which were performed before and after hardening of cement paste. Analysis result showed that the average ultimate unit friction capacity was $9.1tf/m^2$ and this result surpassed the common design criteria of the bored pile.

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Strength Development and Freeze-Thaw Resistance of Concrete Incorporating High Volume Blast-Furnace Slag Subjected to Initial Frost Damage (초기동해를 받은 고로슬래그 다량 혼입 콘크리트의 강도발현 및 동결융해 저항성)

  • Koh, Kyung-Taek;Ryu, Gum-Sung
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.6 no.3
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    • pp.79-87
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    • 2011
  • Concrete incorporating high volume blast-furnace slag placed in cold weather regions might be in danger of initial frost damage because dependently on the mix proportions, the setting and the hardening would be remarkably delayed. Therefore, this study investigated to effect of the degree of frost on the strength development and the resistance to freezing and thawing of the concrete incorporating blast-furnace slag when being subjected to freeze at early age. As the experimental results, the concrete incorporating blast-furnace slag attacked by initial frost damage showed the remarkable reduction of both the compressive strength development and the resistance to freezing and thawing. Especially, the resistance to freezing-thawing of the concrete incorporating high volume blast-furnace slag became much lower than that of the normal concrete.

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