• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.05a
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• pp.289-293
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• 2007

The effect of temperature on the forming limit diagram was investigated for AZ31B magnesium alloy sheet through the limit dome height test in the range from room temperature to $300^{\circ}C$. The formability of AZ31B sheet was improved significantly according to the increasing temperature. Also we studied the springback characteristics through the 2D draw bending test with different blank holding forces at elevated temperatures. Springback quantity was considerably reduced as temperature went up. The blank holding force in the range used, however, had little influence on springback. Experimental results obtained in this study may provide a material database for AZ31B sheet.

• Transactions of Materials Processing
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• v.20 no.8
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• pp.601-610
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• 2011

Based on the facts that AZ31 magnesium alloy can be blow formed just like superplastic aluminum alloys and that most superplastic alloys fail by cavitation, the present study was undertaken to investigate the cavitation behavior of a fine-grained AZ31 sheet during blow forming at the elevated temperature. Other points of interest included the much lower strain rate and temperature dependencies of the magnesium alloy compared with conventional superplastic alloys. It was also aimed to find if cavitation in the AZ31 alloy can be suppressed by hydrostatic pressure, as is the case in most superplastic alloys. Interestingly, the application of hydrostatic pressure did not increase the blow formability of AZ31 sheet, even though it reduced the degree of cavitation. A possible reason for this behavior is discussed.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.10a
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• pp.281-284
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• 2007

The effect of Ca addition on the microstructure evolution and deformation behavior of AZ31 magnesium alloy produced by hot extrusion was investigated. For this purpose, Ca was added into AZ31 melts to the level of 0.7 and 2.0 wt.% Ca. Then, AZ31 base alloy and Ca modified AZ31 alloys were extruded at $383^{\circ}C$. Ca added alloys showed finer grain size and increased hardness value rather than AZ31 base alloy. After isothermal hot compression, the shape of tested specimen exhibited a noticeable anisotropy due to the crystallographic texture effect. The ratio of major and minor axes of ovality was not directly related to test condition and Ca amount. Flow stress level increases with the increase of Ca addition at temperature below $300^{\circ}C$ because of fine microstructure. However, at high temperature and low strain rate region ($400^{\circ}C$ and $10^{-3}s^{-1}$), reverse tendency was observed since main deformation mechanism changes from dislocation slip to grain boundary sliding or diffusional process at high temperature.

• Journal of the Korean institute of surface engineering
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• v.55 no.4
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• pp.196-201
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• 2022

This paper deals with anodic oxidation behavior of AZ31 Mg alloy in aqueous solutions containing various NaF concentrations from 0.01 M to 1 M. Three different voltage-time curves and anodic oxide formation behaviors appeared with concentration of NaF in deionized water. When NaF concentration is lower than 0.02 M, the voltage of AZ31 Mg alloy increased linearly and then reached a steady-state value more than 200 V, and large size pits and thin oxide layer were formed. When NaF concentration is between 0.05 M and 0.1 M, the voltage of AZ31 Mg alloy showed large periodic fluctuations of about 30 ~ 50 V around more than 200 V and large number of small particles were observed. If NaF concentration is higher than 0.2 M, PEO films can be formed without visible arcs under solution pH 6.5 ~ 7.5 by F^- ions without help of OH^- ions.

• Journal of Korea Foundry Society
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• v.23 no.5
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• pp.251-256
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• 2003

Effects of Ca addition on grain refinement, microstructure and mechanical properties of AZ31 Mg alloy were investigated. Due to Ca addition to Mg alloy (AZ31), the microstructure was refined, the quantity of $Mg_{17}Al_{12}$phase was reduced, and new $Al_2Ca$ phase was formed. The tensile property of AZ31 was increased with the minor addition of Ca, but was decreased rapidly over 0.2 wt.% of Ca content. The $Al_2Ca$ phase was considered to be detrimental to the mechanical property of AZ31 Mg alloy.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2008.05a
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• pp.480-481
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• 2008

The aim of this work is to compare the microstructure, the texture, of an AZ31 Mg alloy processed via cold rolling process. Initial AZ31 Mg alloy sheet samples with strong {0002} texture were cut along the angles of 12.5 and 25 degrees to normal direction (ND). These specimens were rolled in room temperature condition. The microstructure was characterized by optical microscopy and the texture was measured by X-ray diffraction.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2017.05a
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• pp.97-97
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• 2017

This study investigated the corrosion protection by electrodeposited copper layer on AZ31 Mg alloy with and without additional silver layer by immersion test, salt spray test, OCP transient and potentiodynamic polarization experiment. The single electrodeposited Cu layer on AZ31 Mg alloy showed a nodular structure with many imperfections of crevices between the nodules, which resulted in the fast initiation of pitting corrosion within first few hours of immersion. Double-layer coating of Cu and outer Ag layer slightly increased the initiation time for pitting corrosion. Triple-layer coatings of Cu/Ag/Cu exhibited the most efficient corrosion protection of AZ31 Mg alloy, compared to the single- and double-layer coatings. Surface morphology of the outer Cu layer in the triple-layer was changed from the nodular structure to fine particle structure with no crevices due to the presence of an additional Ag layer. Thus, the improved corrosion resistance of AZ31 Mg alloy by electrodeposited Cu/Ag or Cu/Ag/Cu layers is readily ascribed to the decreased number of imperfections in the electrodeposited layers due to the additional silver layer. It is concluded that the additional silver layer provides many nucleation sites for the second Cu plating, resulting in the formation of finer and denser structure than the first Cu electrodeposit.

• Transactions of Materials Processing
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• v.31 no.3
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• pp.160-166
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• 2022

The purpose of this study is to investigate the effects of combined addition of Ca and Y on the precipitation and age-hardening behavior of an extruded AZ91 alloy by conducting the aging treatment at 200 ℃ for hot-extruded AZ91 and AZ91-0.3Ca-0.2Y alloys. In the AZ91 alloy, many Mg₁₇Al₁₂ discontinuous precipitate (DP) bands formed during air cooling immediately after extrusion are present, whereas in the AZ91-0.3Ca-0.2Y alloy, a few DP bands and numerous Al₂Y, Al₈Mn₄Y, and Al₂Ca phase particles are distributed along the extrusion direction. The peak-aging time of the AZ91-0.3Ca-0.2Y alloy is 16 hours, twice that of the AZ91 alloy. Although both alloys have similar hardness before aging treatment, the hardness after peak-aging treatment (i.e., peak hardness) of the AZ91-0.3Ca-0.2Y alloy is higher than that of the AZ91 alloy, as 93.1 and 88.7 Hv, respectively. The microstructures of both peak-aged alloys comprise DPs and continuous precipitates (CPs). However, the peak-aged AZ91-0.3Ca-0.2Y alloy has a smaller amount of DPs and a larger amount of CPs than the peak-aged AZ91 alloy. Additionally, the inter-particle spacings of DPs and CPs in the former are significantly narrower than those in the latter. These results demonstrate that the addition of small amounts of Ca and Y to a commercial AZ91 alloy considerably affects the formation rate, size, and amount of CPs and DPs during aging and resultant age-hardening behavior.

• Advances in materials Research
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• v.1 no.3
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• pp.169-182
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• 2012

In this paper the intrinsic influence of micron-sized nickel particle reinforcements on microstructure, micro-hardness tensile properties and tensile fracture behavior of nano-alumina particle reinforced magnesium alloy AZ31 composite is presented and discussed. The unreinforced magnesium alloy (AZ31) and the reinforced nanocomposite counterpart (AZ31/1.5 vol.% $Al_2O_3$/1.5 vol.% Ni] were manufactured by solidification processing followed by hot extrusion. The elastic modulus and yield strength of the nickel particle-reinforced magnesium alloy nano-composite was higher than both the unreinforced magnesium alloy and the unreinforced magnesium alloy nanocomposite (AZ31/1.5 vol.% $Al_2O_3$). The ultimate tensile strength of the nickel particle reinforced composite was noticeably lower than both the unreinforced nano-composite and the monolithic alloy (AZ31). The ductility, quantified by elongation-to-failure, of the reinforced nanocomposite was noticeably higher than both the unreinforced nano-composite and the monolithic alloy. Tensile fracture behavior of this novel material was essentially normal to the far-field stress axis and revealed microscopic features reminiscent of the occurrence of locally ductile failure mechanisms at the fine microscopic level.

• Transactions of Materials Processing
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• v.16 no.8
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• pp.614-620
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• 2007

Deformation characteristics and damage evolution during warm backward extrusion of bulk AZ31 Mg alloy were investigated using finite element analyses. AZ31 Mg alloy was assumed as a hardening viscoplastic material. The tensile tests of AZ31 Mg alloy in previous experimental works showed the ductile fracture even at the warm temperature of $175^{\circ}C$. In this study, damage evolution model proposed by Lee and Dawson, which was developed based on the growth of micro voids in hardening viscoplastic materials, was combined into DEFORM 2D. Effects of forming temperature, punch speed, extrusion ratio and size of work piece on formability in warm backward extrusion as well as on mechanical properties of extruded products were examined. In general, finite element predictions matched the experimental observations and supported the analyses based on experiments. Distributions of accumulated damage predicted by the finite element simulations were effective to identify the locations of possible fracture. Finally, it was concluded that the process model, DEFORM2D combined with Lee & Dawson#s damage evolution model, was effective for the analysis of warm backward extrusion of AZ31 Mg alloys.