• Journal of Welding and Joining
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• 제20권5호
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• pp.87-92
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• 2002

Weldability of Friction Stir Welded(FSW) AZ31B-H24 Mg alloy sheet with 4m thick was evaluated by changing welding speed. The sound welding conditions mainly depended on the suffiicient welding heat input during the process. The insufficient heat input resulted in the void like defect in the weld zone. Higher welding speed caused a larger inner void or lack of bonding. The defects were distributed at the stir zone or the transition region between stir zone and thermo-mechanical affected zone (UE). The size of defects slightly increased with increasing welding speed. These defects had a great effect on the joint strength of weld zone. The weld zone was composed of stir zone, TMAZ and heat affected zone. The stir zone was cosisted of fine recrystallized structure with $5-8\mu\textrm{m}$ in the mean grain size. The hardness of weld zone was near the 60HV, which was slightly lower than that of base metal. The maximum joint strength was about 219MPa that was 75% of that of base metal and the yield strength was also lower than that of base metal partly due to the existance of defects.

• 소성∙가공
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• 제21권4호
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• pp.258-264
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• 2012

The forming failure of AZ31 alloy sheet during deep drawing processes was predicted by the FEM and ductile fracture criteria. Uniaxial tensile tests of round-notched specimens and FE simulations were performed to calculate the critical damage values for three ductile fracture criteria. The critical damage values for each criterion were expressed as a function of strain rate at various temperatures. In order to determine the best criterion for failure prediction, Erichsen cupping test under isothermal conditions at $250^{\circ}C$ were conducted. Based on the plastic deformation histories obtained from the FE analysis of the Erichsen cupping tests and the critical damage value curves, the initiation time and location of fracture were predicted under bi-axial tension deformation. The results indicate that the Cockcroft-Latham criterion had good agreement with the experimental data. In addition, the FE analysis combined with the criterion was applied to another deep drawing process using an irregular shaped blank and these additional results were verified with experimental tests.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2012년도 춘계학술발표회 논문집
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• pp.322-323
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• 2012

This study discussed the formation of phosphate conversion coatings on AZ31 Mg alloy (AZ31) from the zinc phosphating bath with various concentrations of sodium fluoride (NaF). The effects of NaF on the formation, structure, composition and electrochemical behavior of the phosphate coatings were examined using scanning electron microscopy (SEM), X-ray diffraction (XRD) weight balances, open circuit potential (OCP) transients, potentiodynamic polarization curves and immersion test. The coatings were composed of two layers: an outer $Zn_2(PO_4)_3.4H_2O$ (hopeite) crystal layer and an inner amorphous of $MgZn_2(PO_4)_2$. NaF concentration is emphasized to be highly effective in the formation of the hopeite crystal and etching and coating rates. Potentiodynamic polarization and immersion test showed that the coatings formed in the zinc phosphating bath with addition of NaF have much higher corrosion resistance than bare AZ31.

• 대한금속재료학회지
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• 제48권6호
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• pp.498-505
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• 2010

Wrought magnesium alloys show a low formability at room temperature, and a remarkable anisotropy of mechanical properties make it difficult to use them in a deformation process in industry. The microstructure and crystallographic texture of metals are developed during thermo-mechanical processes, and they are significant to the understanding of the mechanical properties of metals. This work studies the microstructure, texture development and tensile properties of the extruded AZ31 Mg alloy after rolling at 100 and $300^{\circ}C$. After 40% rolling at $100^{\circ}C$, many deformed twins were observed and a relatively weak texture developed. The basal poles were split and rotated towards the rolling direction about $20^{\circ}$. During 60% rolling at $300^{\circ}C$, the dynamic recrystallization (DRX) took place and developed a strong <0001>II ND fiber texture, which influenced the poor formability at room temperature.

• 대한금속재료학회지
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• 제47권1호
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• pp.1-6
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• 2009

Magnesium alloys are drawing a lot of attention and have been extensively studied. The major obstacle to the practical application of the alloys is the poor formability at room temperature, originating basically from the insufficient number of slip system. Development of a proper texture is one promising solution to improve the formability. In the present work, after extrusion and full annealing, microstructures, texture developments and tensile properties of AZ31 Mg alloys are studied. After full annealing strong <1010>||ED fiber texture and weak <1120>+<1230>||ED fiber texture (c-axes in the radial direction) were developed. The textures are distinctly influencing the tensile properties, which can be understood in terms of the activation of basal slip modes. With the random orientation, which is developed in the $45^{\circ}$ sample to the extrusion direction, the better workability can be achieved at room temperature.

• Advances in nano research
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• 제13권4호
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• pp.407-416
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• 2022

In this study, the gravitating mechanical stir casting method was used to fabricating the Nb₂O₅/AZ31 magnesium matrix nanocomposites. Niobium pentoxide (Nb₂O₅) used as reinforcement with two different weight percentages (3 wt % and 6 wt %). The influence of Nb₂O₅ on microstructure and mechanical properties has been investigated. The microstructure analysis showed that the composites are mainly composed of the primary α-magnesium phase and phase β-Mg₁₇Al₁₂ secondary phase. The secondary phase was dispersed evenly along the grain boundary of the Mg phase. The Nb₂O₅/AZ31 nanocomposites revealed that the grain size and its lamellar shape (β-Mg₁₇Al₁₂) were gradually refined. Different strengthening mechanisms were assessed in terms of their contributions. Results showed that composite material properties of hardness, yield strength, and fracture study were directly related to Nb₂O₅ as a reinforcement. The maximum values of the mechanical properties were achieved with the addition of 3 wt% Nb₂O₅ on the AZ31 alloy.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2007년도 추계학술대회 논문집
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• pp.306-309
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• 2007

Recently, magnesium alloys have been widely used in automotive, aerospace and electronic industries with the advantages such as lightweightness, high specific strength and stiffness. However, magnesium alloy has quite low formability at room temperature due to its hexagonal close-packed crystal structure. Warm deep drawing is one of the forming technologies to improve the formability of magnesium alloy sheet and the lubrication condition is an important process parameter in that. In this study, the drawing tests of AZ31 alloy sheet at elevated temperature for various kinds of lubricant were carried out and the effects of lubrication conditions on drawbility were investigated.

• 한국생산제조학회지
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• 제23권5호
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• pp.519-524
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• 2014

The use of light weight magnesium alloy offers significant potential towards improvement of the automotive fuel efficiency. However, the application of formed magnesium alloy components in auto-body structures is restricted due to the low formability at room temperature and lack of knowledge for processing magnesium alloys at elevated temperatures. In this study, a warm tensile test of magnesium alloys was performed to measure tensile strength and elongation. An improvement in formability was confirmed at increased temperatures above about $250^{\circ}C$. Car body warm forming technology was conducted for forming forming reinforced dash components of the magnesium alloy AZ31B sheet at elevated temperatures.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2017년도 춘계학술대회 논문집
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• pp.96.2-96.2
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• 2017

This research was conducted to investigate the electrochemical properties of the thin air-formed oxide film-covered AZ31 Mg alloy. In this work, native air-formed oxide films on AZ31 Mg alloy samples were prepared by knife-abrading method and the changes in the electrochemical properties of the air-formed oxide film were investigated in seven different electrolytes containing the following anions $Cl^-$, $F^-$, $SO{_4}^{2-}$, $NO_3{^-}$, $CH_3COO^-$, $CO{_3}^{2-}$ and $PO{_4}^{3-}$. It was observed from open circuit potential (OCP) transients that the potential initially decreased before gradually increasing again in the solutions containing only $CO{_3}^{2-}$ or $PO{_4}^{3-}$ ions, indicating the dissolution or transformation of the native air-formed oxide film into new more protective surface films. The Nyquist plots obtained from electrochemical impedance spectroscopy (EIS) showed that there was growth of new surface films with immersion time on the air-formed oxide film-covered specimens in all the electrolytes; the least resistive surface films were formed in fluoride and sulphate baths whereas the most protective film was formed in phosphate bath. The potentiodynamic polarization curves illustrated that passive behaviour of AZ31 Mg alloy under anodic polarization appears only in $CO{_3}^{2-}$ or $PO{_4}^{3-}$ ions containing solutions and at more than $-0.4V_{Ag/AgCl}$ in $F^-$ ion containing solution.

• 동력기계공학회지
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• 제9권4호
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• pp.96-101
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• 2005

Magnesium alloys have been widely used for many structural components of automobiles and aircraft because of high specific strength and good cast ability in spite of hexagonal closed-packed crystal structure of pure magnesium. In this study, uniaxial tension tests at high temperature and creep tests are done in order to investigate the characteristics of high temperature and mechanisms for creep deformation of AZ31 Mg alloy. Yield stress and ultimate tensile stress decreased with increasing temperature, but elongation increased from results of uniaxial tension test at high temperature. The apparent activation energy Qc, the applied stress exponent n and rupture life have been determined during creep of AZ31 Mg alloy over the temperature range of 473K to 573K and stress range of 23.42 MPa to 93.59 MPa, respectively, in order to investigate the creep behavior. Constant load creep tests were carried out in the equipment including automatic temperature controller, whose data are sent to computer. At around the temperature of $473K{\sim}493K$ and under the stress level of $62.43{\sim}93.59%MPa$, and again at around the temperature of $553K{\sim}573K$ and under the stress level of $23.42{\sim}39.00MPa$, the creep behavior obeyed a simple power-law relating steady state creep rate to applied stress and the activation energy for the creep deformation was nearly equal, respectively, and a little low to that of the self diffusion of Mg alloy including aluminum. Also rupture surfaces at high temperature have had bigger dimples than those at lower temperature by SEM.