• Transactions of the Korean Society of Pressure Vessels and Piping
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• v.19 no.2
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• pp.102-108
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• 2023

A Chloride-induced stress corrosion cracking (CISCC) of austenite stainless steel in dry cask storage system (DCSS) can occur with extending service time than originally designed. Cold spray coating (CSC) not only form a very dense microstructure that can protect from corrosive environments, but also can generate compressive stress on the surface. This characteristic of CSC process is very helpful to increase the resistance for CISCC. CSC with several powders, such as 304L, 316L and Ni can be optimized to form very dense coating layer. In addition, the impact energy generated as the CSC powder collides with the surface of base metal at a speed of Mach 2 or more can remove the residual tensile stress of welding area and serve the compress stress. CSC layers include no oxidation and no contamination with under 0.2% porosity, which is enough to protect from the penetration of corrosive chloride. Therefore, the CSC coating layer can be accompanied by a function that can be disconnected from the corrosive environment and an effect of improving the residual stress that causes CISCC, so the canister's CISCC resistance can be increased.

• Nuclear Engineering and Technology
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• v.56 no.6
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• pp.2131-2140
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• 2024

The chloride-induced stress corrosion cracking (CISCC) is one of the major integrity concerns in dry storage canisters made of austenitic stainless steels (ASSs). In this study, an advanced duplex stainless steel (DSS) with a composition of Fe-19Cr-4Ni-2.5Mo-4.5Mn (ADCS) was developed and its performance was compared with that of commercial ASS and DSS alloys. The chemical composition of ADCS was determined to obtain greater pitting and CISCC resistance as well as a proper combination of strength and ductility. Then, the thermomechanical processing (TMP) condition was applied, which resulted in higher strength than ASSs (304L SS and 316L SS) and better ductility than DSSs (2101 LDSS and 2205 DSS). The potentiodynamic polarization and electrochemical impedance spectra (EIS) results represented the better pitting corrosion resistance of ADCS compared to 304L SS and 316L SS by forming a better passive layer. The CISCC tests using four-point loaded specimens showed that cracks were initiated at 24 h for 304L SS and 144 h for 316L SS, while crack was not found until 1008 h for ADCS. Overall, the developed alloy, ADCS, showed better combination of CISCC resistance and mechanical properties as dry storage canister materials than commercial alloys.

• Steel and Composite Structures
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• v.50 no.3
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• pp.281-298
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• 2024

Stainless steel bolts (SSB) are increasingly utilized in bolted steel connections due to their good mechanical performance and excellent corrosion resistance. Fire accidents, which commonly occur in engineering scenarios, pose a significant threat to the safety of steel frames. The post-fire behavior of SSB has a significant influence on the structural integrity of steel frames, and neglecting the effect of temperature can lead to serious accidents in engineering. Therefore, it is important to evaluate the performance of SSB at elevated temperatures and their residual strength after a fire incident. To investigate the mechanical behavior of SSB after fire, 114 bolts with grades A4-70 and A4-80, manufactured from 316L austenitic stainless steel, were subjected to elevated temperatures ranging from 20℃ to 1200℃. Two different cooling methods commonly employed in engineering, namely cooling at ambient temperatures (air cooling) and cooling in water (water cooling), were used to cool the bolts. Tensile tests were performed to examine the influence of elevated temperatures and cooling methods on the mechanical behavior of SSB. The results indicate that the temperature does not significantly affect the Young's modulus and the ultimate strength of SSB. Up to 500℃, the yield strength increases with temperature, but this trend reverses when the temperature exceeds 500℃. In contrast, the ultimate strain shows the opposite trend. The strain hardening exponent is not significantly influenced by the temperature until it reaches 500℃. The cooling methods employed have an insignificant impact on the performance of SSB. When compared to high-strength bolts, 316L austenitic SSB demonstrate superior fire resistance. Design models for the post-fire mechanical behavior of 316L austenitic SSB, encompassing parameters such as the elasticity modulus, yield strength, ultimate strength, ultimate strain, and strain hardening exponent, are proposed, and a more precise stress-strain model is recommended to predict the mechanical behavior of 316L austenitic SSB after a fire incident.

• Journal of the Korean Society for Nondestructive Testing
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• v.28 no.6
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• pp.477-482
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• 2008

The influence of dislocation substructure of metallic materials on ultrasonic velocity has been experimentally investigated. The test materials of pure Cu, brass (Cu-35Zn), 2.25Cr-1Mo steel, and AISI 316 with different stacking fault energy (SFE) are plastically deformed in order to generate dislocation substructures. The longitudinal wave velocit $(C_L)$ decreases as a function of tensile strain in each material. The $C_L$ of Cu-35Zn and AISI 316 decreases monotonously with tensile strain, but $C_L$ of Cu and 2.25Cr-1Mo steel shows plateau phenomena due to the stable dislocation substructure. The variation of ultrasonic velocity with the extent of dislocation damping and dislocation substructures is discussed.

• Proceedings of the Korean Vacuum Society Conference
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• 2008.08a
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• pp.318-318
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• 2008

• Proceedings of the Korean Vacuum Society Conference
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• 2008.08a
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• pp.319-319
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• 2008

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2010.06a
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• pp.316-316
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• 2010

SOP-L 기술은 LTCC기술과 다른 SOP 기술과 비교해서 이종의 물질을 접합하는데 용이하고 공정비용이 저렴하다. 또한 전자제품이나 부품 또는 재료들의 소형화가 많이 이루어지고 있는 추세이다. 본 연구에서는 6 layer의 다층형 diplexer를 제작하여 면압에 따른 층간 두께의 변화를 관찰하였고, 이를 통하여 두께 변화에 따른 특성 값의 변화를 통해 가장 최적화된 공정을 연구해보자고 한다.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2007.11a
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• pp.155-156
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• 2007

AISI316L강에 저온 프라즈마 침탄과 저온 프라즈마 질화를 연속적으로 실시하여 표면경도와 내식성을 동시에 증가시키는 처리법에서 질화처리 시 처리시간 및 온도에 따른 표면특성변화를 조사하였다. 모든 시편의 표면에 N에 의해 확장된 오스테나이트(${\gamma}_N$)가 형성되었으며, 형성된 ${\gamma}_N$로 인하여 표면경도가 약 $3{\sim}4$배 증가하였다. 처리시간과 온도가 증가함에 따라 ${\gamma}_N$층의 두께와 표면의 N농도가 증가 하였다. 표면처리한 모든 시편은 표면의 N의 영향으로 내식성이 증가 하였다.

• Corrosion Science and Technology
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• v.3 no.5
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• pp.222-225
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• 2004

A portable RF HTS SQUID-based susceptometer was applied to the measurement of fatigue behavior for type 316L(N) stainless steel containing 0.04% to 0.15% nitrogen content. Strain-controlled low cycle fatigue (LCF) tests were conducted at RT and $600^{\circ}C$ in air an atmosphere, and the magnetic moments were measured after the fatigue test using HTS SQUID. The magnetic moment of an as-received sample is higher than that of a fatigued sample in all the temperature ranges irrespective of the nitrogen content. The fatigue life decreased with an increasing test temperature up to $500^{\circ}C$, but increased at $600^{\circ}C$. The change of the magnetic moments by LCF test is attributed to the stress induced micro defects.

• Journal of Periodontal and Implant Science
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• v.27 no.2
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• pp.329-346
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• 1997

Dental implants have been developed for enhancement of osseointegration. Biocompatibility, bone affinity and surface characteristics of dental implants are very important factors for osseointegration. The aim of the present study was to determine the cytotoxicity and the bone affinity of titanium phosphide(Ti-P) implant material. The Ti-P surface was obtained by vacuum sintering of titanium within compacted hydroxyapatite powder. The composition and the chemical change of the surface were determined by Auger electron spectroscopy. The in vitro cytotoxicity was evaluated by the viability of the bone cells and macrophages obtained from chicken embryo and rat,s peritonium, respectively. For the comparative evaluation, 316L stainless steel, commercially pure titanium and Ti-P materials, prepared in size of 1O.0mm in diameter and 5.0mm in height, were immersed separately in bone cells and macrophages for 10 days. For the evaluation of the in vivo bone affinity, 316L stainless steel, commercially pure titanium and Ti-P materials, prepared in size of 5.0mm in diameter and 10.0mm in length, were implanted after drilling in diameter 5.5mm in femurs of 2 dogs weighing 10Kg more or less. Six weeks after implantation the specimens were prepared for histopathological examination and were observed under light microscope. In comparison of in vitro bone cell viability, Ti-P and commercially pure titanium groups were not significantly different from control group (p>O.1), but 316L stainless steel group was significantly lower than control group(p<0.05). There was no statistical difference in the viability of macrophages between 3 different groups and control group(p>O.l). In comparison of in vivo study, 316L stainless steel and commercially pure titanium showed fibrous encapsulation, but Ti-P showed remarkable new bone formation without any fibrous tissue. The results demonstrate that Ti-P has favorable biocompatibility and bone affinity, and suggest that dental implants with Ti-P surface may enhance osseointegration.