• Journal of Welding and Joining
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• 제34권5호
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• pp.33-40
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• 2016

The microstructures and the creep rupture properties of dissimilar welds between the Ni-based superalloy Inconel 740H and the non-stabilized austenitic stainless steel TP316H have been characterized. The welds were produced by shielded metal arc (SMA) welding process with the AWS A5.11 Class ENiCrFe-3 filler metal, commonly known as Inconel 182 superalloy. Postweld heat treatment at $760^{\circ}C$ for 4 hours was conducted to form ${\gamma}^{\prime}$ strengthener in Inconel 740H. The austenitic weld metal produced by Inconel 182 had a dendritic microstructure, and grew epitaxially from the both sides of Inconel 740H and TP316H base metals. Since both Inconel 740H and TP316H did not undergo any solid-state transformation during welding process, there were no heat-affected-zone (HAZ) sub-regions and the coarsoned grains near the weld interface were limited to a narrow region. The hardness of Inconel 182 weld metal was ~220 Hv. The gradual hardness decrease was detected at HAZ of TP316H, and the TP316H base metal displayed the lowest hardness value (~180 Hv) whilst the Inconel 740H showed the highest hardness value (~400 Hv). Fracture after creep occurred at the center of weld metal, regardless of creep condition. It was found that during creep the cracks initiated and propagated along interdendritic regions and grain boundaries at which Laves particles enriched in Nb, Si and Cr were present. The appropriate design of weld metal was discussed to suppress the creep-induced cracking of the present dissimilar weld.

• 한국표면공학회지
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• 제50권1호
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• pp.35-41
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• 2017

$TiO_2$, $Al_2O_3$, and $TiO_2-Al_2O_3$ nanolaminated films were grown by atomic layer deposition (ALD) on the 316L stainless steel (SS316L) substrates at a temperature of $150^{\circ}C$. The growth kinetics of $ALD-TiO_2$ and $Al_2O_3$ thin films were systematically investigated in order to precisely control the thickness of each layers in the $TiO_2-Al_2O_3$ nanolaminated films using a high-resolution transmission electron microscopy. And, the exact deposition rates of $ALD-TiO_2$ on $Al_2O_3$ surface and $ALD-Al_2O_3$ on $TiO_2$ surface were revealed to be 0.0284 nm/cycle and 0.11 nm/cycle, respectively. At given growth conditions, the microstructures of $TiO_2$, $Al_2O_3$ and $TiO_2-Al_2O_3$ nanolaminated films were amorphous. The potentiodynamic polarization test revealed that the $TiO_2-Al_2O_3$ nanolaminated film coated SS316L had a best corrosion resistance, although all ALDcoated SS316L exhibited a clear improvement of the corrosion resistance compared with a bare SS316L.

• Journal of Periodontal and Implant Science
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• 제27권2호
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• pp.329-346
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• 1997

Dental implants have been developed for enhancement of osseointegration. Biocompatibility, bone affinity and surface characteristics of dental implants are very important factors for osseointegration. The aim of the present study was to determine the cytotoxicity and the bone affinity of titanium phosphide(Ti-P) implant material. The Ti-P surface was obtained by vacuum sintering of titanium within compacted hydroxyapatite powder. The composition and the chemical change of the surface were determined by Auger electron spectroscopy. The in vitro cytotoxicity was evaluated by the viability of the bone cells and macrophages obtained from chicken embryo and rat,s peritonium, respectively. For the comparative evaluation, 316L stainless steel, commercially pure titanium and Ti-P materials, prepared in size of 1O.0mm in diameter and 5.0mm in height, were immersed separately in bone cells and macrophages for 10 days. For the evaluation of the in vivo bone affinity, 316L stainless steel, commercially pure titanium and Ti-P materials, prepared in size of 5.0mm in diameter and 10.0mm in length, were implanted after drilling in diameter 5.5mm in femurs of 2 dogs weighing 10Kg more or less. Six weeks after implantation the specimens were prepared for histopathological examination and were observed under light microscope. In comparison of in vitro bone cell viability, Ti-P and commercially pure titanium groups were not significantly different from control group (p>O.1), but 316L stainless steel group was significantly lower than control group(p<0.05). There was no statistical difference in the viability of macrophages between 3 different groups and control group(p>O.l). In comparison of in vivo study, 316L stainless steel and commercially pure titanium showed fibrous encapsulation, but Ti-P showed remarkable new bone formation without any fibrous tissue. The results demonstrate that Ti-P has favorable biocompatibility and bone affinity, and suggest that dental implants with Ti-P surface may enhance osseointegration.

• 전력전자학회:학술대회논문집
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• 전력전자학회 2008년도 하계학술대회 논문집
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• pp.646-648
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• 2008

The multi-films of a metallic film and a transparent conducting oxide (TCO, indium-tin oxide, ITO) film were formed on the stainless steel 316 and 304 plates by a sputtering method and an E-beam method and then the external metallic region of the stainless steel bipolar plates was converted into the metal nitride films through an annealing process. The multi-film formed on the stainless steel bipolar plates showed the XRD patterns of the typical indium-tin oxide, the metallic phase and the metal substrate and the external nitride film. The XRD pattern of the thin film on the bipolar plates modified showed two metal nitride phases of CrN and $Cr_2N$ compound. Surface microstructural morphology of the multi-film deposited bipolar plates was observed by AFM and FE-SEM. The electrical resistivity of the stainless steel bipolar plates modified was evaluated.

• Journal of Magnetics
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• 제20권3호
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• pp.312-316
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• 2015

Unlike conventional Eddy Current Test (ECT), Pulsed Eddy Current (PEC) uses a multiple-frequency current pulse through the excitation coil. In the present study, the detection of subsurface cracks using a specially designed probe that allows the detection of a deeper crack with a relatively small current density has been attempted using the PEC technique. The tested sample is a piece of 304 stainless steel (SS304) with a thickness of 30mm. Small electrical discharge machining (EDM) notches were put in the test sample at different depths from the surface to simulate the subsurface cracks in a pipe. The designed PEC probe consists of an excitation coil and a Hall sensor and can detect a subsurface crack as narrow and shallow as 0.2 mm wide and 2 mm deep. The maximum distance between the probe and the defect is 28 mm. The peak amplitude of the detected pulse is used to evaluate the cracks under the sample surface. In time domain analysis, the greater the crack depth the greater the peak amplitude of the detected pulse. The experimental results indicated that the proposed system has the potential to detect the subsurface cracks in stainless steel plates.

• Biomaterials and Biomechanics in Bioengineering
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• 제5권1호
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• pp.37-50
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• 2020

Development of lightweight implant plates are important to reduce the stress shielding effect for a prosthesis of femur bone fractures. Stainless steel (SS-316L) is a widely used material for making implants. Stress shielding effect and other issues arise due to the difference in mechanical properties of stainless steel when compared with bone. To overcome these issues, composite materials seem to be a better alternative solution. The comparison is made between two biocompatible composite materials, namely Ti-hydroxyapatite and Ti-polypropylene. "Titanium (Ti)" is fiber material while "hydroxyapatite" and "polypropylene" are matrix materials. These two composites have Young's modulus closer to the bone than stainless steel. Besides the variety of bones, present paper constrained to femur bone analysis only. Being heaviest and longest, the femur is the most likely to fail among all bone failures in human. Modelling of the femur bone, screws, implant and assembly was carried out using CATIA and static analysis was carried out using ANSYS. The femur bone assembly was analyzed for forces during daily activities. Ti-hydroxyapatite and Ti-polypropylene composite implants induced more stress in composite implant plate, results less stress induced in bone leading to a reduction in shielding effect than stainless steel implant plate thus ensuring safety and quick healing for the patient.

• Journal of Advanced Marine Engineering and Technology
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• 제36권8호
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• pp.1061-1068
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• 2012

오늘날 지구온난화, 환경오염 및 주요 에너지원인 화석연료의 고갈에 대한 우려가 높아지면서, 전세계적으로 신재생에너지 및 청정에너지에 대한 관심이 급격하게 증가하고 있다. 따라서 화석연료의 대체 및 SOX, NOX와 같은 오염물질을 적게 배출하는 청정에너지로써 LNG가 폭넓게 사용되고 있다. 그로인해 LNG의 소비는 급격하게 증가하고 있으며, 그것을 운반하기 위한 LNG선의 수요 또한 수십 년 동안 크게 증가하였다. 본 연구에서는 LNG선의 생산성을 향상시키기 위해 LNG선용 스테인리스강에 대한 용접에 고출력 파이버 레이저를 이용하였다. 사용된 재료는 탄소 함유량이 0.03% 이하의 STS316L이며 두께는 8mm이다. 최대출력 5kW의 파이버 레이저를 열원으로 사용하여 비초점거리, 겹치기 용접 그리고 맞대기 용접에 대한 실험을 진행하였다. 실험결과, 겹치기 용접의 경우 2.0m/min, 맞대기 용접의 경우 3.0m/min의 용접속도까지 접합이 가능하였다.

• 대한기계학회논문집A
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• 제35권5호
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• pp.453-458
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• 2011

본 논문은 TP316L 스테인리스강 재료에 대한 표면 기계가공 및 열처리에 의한 잔류응력의 생성 및 변화에 대해 연구한 것이다. 연구를 위해서 TP316L 시편에 대해 방전가공, 밀링, 연마의 3 가지 기계가공을 수행하고 표면의 잔류응력을 측정하였다. 동일한 방법으로 기계가공한 다른 시편은 열처리를 수행한 후에 표면잔류응력을 측정하여 열처리를 수행하지 않은 시편과의 차이를 비교하였다. 잔류응력측정은 엑스선회절법을 사용하였다. 또한 각 시편에 대해 비커스경도를 측정하여 열처리 수행전과 수행후의 경도를 비교하였다. 본 연구를 통해서 기계가공 방법에 따라 잔류응력의 형태가 달라지며 열처리에 의해서 대부분의 잔류응력이 제거됨이 확인되었다. 경도는 잔류응력의 인장 또는 압축의 방향에는 관계없이 크기에만 관련성이 있는 것으로 관찰되었다.

• 한국분말재료학회지
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• 제27권3호
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• pp.219-225
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• 2020

The directed energy deposition (DED) process of metal 3D printing technologies has been treated as an effective method for welding, repairing, and even 3-dimensional building of machinery parts. In this study, stainless steel 316L (STS316L) and Inconel 625 (IN625) alloy powders are additively manufactured using the DED process, and the microstructure of the fabricated STS316L/IN625 sample is investigated. In particular, there are no secondary phases in the interface between STS316L and the IN625 alloy. The EDS and Vickers hardness results clearly show compositionally and mechanically transient layers a few tens of micrometers in thickness. Interestingly, several cracks are only observed in the STS 316L rather than in the IN625 alloy near the interface. In addition, small-sized voids 200-400 nm in diameter that look like trapped pores are present in both materials. The cracks present near the interface are formed by tensile stress in STS316L caused by the difference in the CTE (coefficient of thermal expansion) between the two materials during the DED process. These results can provide fundamental information for the fabrication of machinery parts that require joining of two materials, such as valves.

• 한국압력기기공학회 논문집
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• 제15권2호
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• pp.9-18
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• 2019

The objective of this study is to investigate the feasibility of simulating the mechanical properties of irradiatied austenitic stainless steels by cold-working. In this study, the tensile properties, cyclic hardening behaviors and fracture toughness of cold-worked TP316L stainless steel were compared with those of austenitic stainless steels irradiated by neutrons. It showed that cold-working can properly simulate the increase in strength and the decrease in ductility and fracture resistance of austenitic stainless steels by neutron irradiation, even though it could not perfectly simulate the microstructures of irradiated austenitic stainless steels. Also, cold-working can appropriately simulate the hardening behaviors of neutron irradiated austenitic stainless steels under monotonic and cyclic loading conditions.