• Title/Summary/Keyword: 309L

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Study on the hydrogen embrittlement crack susceptibility of stainless steel overlaid weld metal (1) (스테인레스강 Overlay용접부의 수소취화 균열감수성에 관한 연구 1)

  • 이영호
    • Journal of Welding and Joining
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    • v.8 no.3
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    • pp.39-52
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    • 1990
  • The research is to insure the soundness of the stainless steel overlaid weld metal(21/4Cr-IMo steel + SUS 309L) for a pressure vessel application. Detail studies were conducted for the PWHT influence on the micrstructure and intergranular corrosion characteristics of the overlaid weld metal as well as initiation of hydrogen embrittlement crack(or Disbonding) when welded metal are exposed to the hydrogen atmosphere. Hydrogen was experimentally charged to the overlaid weld metal in order to study PWHT effect on the susceptibility of hydrogen embrittlement crack. The results of this research are as follows: 1. At the bond region, austenite grain of the stainless steel side became coarsed and Cr23C6 type carbide was precipitated at the coarsed austenitic grain boundaries. Intergranular Corrosion width(by Straiss test) increased with increasing PWHT temperature and PWHT time.

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한국산 인삼, 장뇌삼 및 중국산 장뇌삼의 항산화 활성에 관한 연구

  • Hwang, Yu-Jin;Yang, Hui-Jin;Lee, Su-Won
    • Proceedings of the Korean Society for Food Science of Animal Resources Conference
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    • 2006.05a
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    • pp.309-311
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    • 2006
  • 한국산 인삼, 장뇌삼 및 중국산 장뇌삼의 각 추출 용매에 따른 항산화 활성을 측정하였다. 추출 용매에 따른 전자 공여 능력은 모든 시료에서 농도 의존적인 결과를 나타냈으며, 그 중 한국산 장뇌삼의 hexane 추출물 $600{\mu}g/mL$에서 71.4%로 가장 높은 전자 공여능을 보였다. Superoxide anion radical 소거 능력에 대해서는 $H_2O$, hexane, butanol, chloroform 및 total 추출물 순으로 높은 활성을 보였고, 시료별로는 한국산 장뇌삼이 가장 활성이 높았고, 그 다음으로 중국산 장뇌삼, 한국산 인삼의 순으로 나타났다.

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A New Triterpene, Phytolaccagenic Acid from Phytolacca americana (상륙(商陸)의 신(新) 성분(成分) Phytolaccagenic Acid에 관한 연구)

  • Woo, Won-Sick;Kang, Sam-Sik
    • Korean Journal of Pharmacognosy
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    • v.5 no.2
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    • pp.125-127
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    • 1974
  • 상륙(商陸) (Phytolacca americana L.)의 근(根)에서 얻은 조(粗)saponin을 산(酸) 가수분해(加水分解)하면 5(종)種의 genin을 얻을 수 있다. 그 중(中) 2종(種)의 성분(成分)에 대하여는 아직 그 구조(構造)가 밝혀지지 않았다. 그 중(中) 한 성분(成分), $C_{31}H_{48}O_{6},\;(mp\;309-311^{\circ})$에 대하여 이화학적(理化學的) 성질(性質)을 검토(檢討)한 바 I과 같은 구조식(構造式)을 추정(推定)할 수 있었으며 본성분(本成分)은 신화합물(新化合物)이므로 phytolaccagenic acid라고 명명(命名)하였다 Phytolaccagenic acid의 가수분해산물(加水分解産物)은 제(第)2의 미지성분(未知成分)과 같고 이것은 P. esculenta에서 얻은 esculentic acid와 동일(同一)하다.

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Analysis of Carbon Migration with Post Weld Heat Treatment in Dissimilar Metal Weld. (이종금속 피복용접부의 후열처리에 따른 탄소이동 해석)

  • Kim, Byeong-Cheol;Ann, Hui-Seong;Kim, Seon-Jin;Song, Jin-Tae
    • Korean Journal of Materials Research
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    • v.1 no.1
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    • pp.29-36
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    • 1991
  • Pressurized Water Reactor (PWR) pressure vessels are made of forged low alloy steel plates internally clad with an austenitic stainless steel by welding to improve anti-corrosion properties. They display a characteristic behavior of dissimilar metal weld interface during post weld heat treatment (PWHT) and service at high temperature and pressure. In this Study, Metallugical structure of weld interface of SA 508 Class 3 forged steel clad with 309L, Austenitic stainless steel after PWHT was investigated. To estimate the width of the carburized/decarburized bands quantitatively, a model for carbon diffusion was proposed and a theoretical equation was derived.

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The Effect of Processing Parameters on the Mechanical Properties of TiN Films by the Pulsed DC PACVD (펄스형 DC PACVD 법에의해 미치는 공정인자의 영향)

  • 김진관;변응선;백운승;이구현;제창웅;윤재홍;이상로
    • Journal of the Korean institute of surface engineering
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    • v.30 no.5
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    • pp.298-309
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    • 1997
  • Hard Tin coating on tool steel substrate were prepared using the pulsed PACVE. An orthogonal experimental design was employed to find the best deposition conditions for TiN coating and to systematically understand the effect of processing parameters. The small size Taguchi matrix called the L16 was used for experiment and ANOVA(ANalysis of VAriance) was followed to study the effect of main parameters on hardness and adhesion TiN coatings. In conclusion, pulse on/off time ratio and pulsing frequency were the major deposition parameters to determine hardness and adhesion of TiN coating in the pulsed DC PACVE process. (200) preferred orientation, columnar growth and dome-shaped surface morphology of the TiN films gave rise to a high hardness and a good adhesion to the substrates.

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Synthesis and Antitumor Evaluation of 3-(2-Chloroethyl)-hydantoins from Some Amino Acids (아미노산으로부터 3-(2-Chloroethyl) hydantoin들의 합성과 그들의 항암작용 평가)

  • 김정균;윤이규;고영심;윤웅찬;박무영;문경호
    • YAKHAK HOEJI
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    • v.27 no.4
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    • pp.309-314
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    • 1983
  • Six hydantoin derivatives, 3-(2-chloroethyl) hydantoin (6a), 3-(2-chloroethyl)-5-isopropylhydantoin (6b), 3-(2-chloroethyl)-5-isobutylhydantoin (6c), 3-(2-chloroetbyl)5-(2-butyl) hydantoin (6d), 3-(2-chloroethyl)-5-benzylhydantoin (6e), 3-(2-chloroethyl)-5-(indolyl-3-methyl) hydantoin (6f), were prepared by the treatment of the corresponding salt of amino acids with 2-chloroethyl isocyanate in cold water, followed by refluxing in concentrated HCl solution. Anticancer activity of the synthesized hydantoin derivatives were examined on murine leukemia L1210 cells growing in Fischer medium. Among them, 3-(2-chloroethy)-5-isobutyl-hydantoin (6c) showed substantially low $ED_{50}$ value of $9.6{\mu}g/ml$.

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Ulcer Healing Effects of Vitamin E on Chronic Gastric Ulcer Induced by Alcohol in Young Adult Rats (알코올로 유도한 만성위궤양 흰쥐 모델에서 비타민 E 보충이 위궤양 치유에 미치는 영향)

  • Mo, Jung-Min;Lee, Sun-Hye;Park, Mi-Na;Lee, Yeon-Sook
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.37 no.3
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    • pp.309-316
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    • 2008
  • This study was carried out to examine the effects of vitamin E on chronic gastric ulcer induced by alcohol treatment in rats. Chronic gastric ulcer model was established by oral administration of 70% ethanol at one time and supply of 15% ethanol for additional 7 days. Male Sprague-Dawley rats, approximately 200 g, were fasted for 24 hours and orally gavaged with 1 mL of 70% ethanol for the induction of acute ulcer. A supply of 15% ethanol dissolved in distilled water for 7 days were followed to maintain chronic gastric ulcer. Acute ulcer group was sacrificed at 3 hours after oral administration of 1 mL of 70% ethanol. Chronic groups were divided into three groups according to vitamin E levels; low-vitamin E (LVE, 0 mg/mL oil/day), normalvitamin E (NVE, 1 mg/mL oil/day) and high-vitamin E (HVE, 10 mg/mL oil/day). These groups were fed vitamin E free diets which were made of vitamin E free vitamin mix followed AIN-93M pattern for 7 days. Histological findings of congestion, hemorrhage and necrosis in gastric tissue were shown severely in acute ulcer group and LVE group of chronic ulcer groups. The concentration of gastrin in serum was significantly higher in LVE group. The content of histamine in stomach was lower in acute ulcer group but there was no significant difference among the chronic groups regardless of vitamin E levels. Content of malondialdehyde (MDA) in gastric tissue was higher in HVE group and activities of antioxidant enzyme, glutathione peroxidase (GPx) and catalase, were lower in HVE group. Myeloperoxidase (MPO) activities as a marker of neutrophils infiltration was significantly higher in LVE group. These results suggested that vitamin E supplementation has positive effects on healing of alcohol-induced chronic gastric ulcer through alleviation of gastric tissue injuries and reduction of the MPO activity in gastric tissue and gastrin in serum.

Effects of Various LEDs on the Seed Germination, Growth and Physiological Activities of Rape (Brassica napus) Sprout Vegetable (몇 가지 LED가 유채의 종자발아, 초기 생장 및 생리활성에 미치는 영향)

  • Cho, Ja-Yong;Son, Dong-Mo;Kim, Jong-Man;Seo, Beom-Seok;Yang, Seung-Yul;Kim, Byoung-Woon;Heo, Buk-Gu
    • Korean Journal of Plant Resources
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    • v.21 no.4
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    • pp.304-309
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    • 2008
  • All the seeds of rape (Brassica napus) sprout vegetables were germinated within three days after seeding irrelevant to the light colors. The total fresh weight of rape sprout vegetables at 6 days after seeding have been increased when grown under green and white color lights by 0.339g/10plants and 0.339g/10plants compared with the control. The total flavonoid contents in rape sprouts were increased under red and blue lights by 72.5 and 70.9mg${\cdot}L^{-1}$. Those DPPH radical scavenging activities at 2,000mg${\cdot}L^{-1}$ were increased by 90.0 and 90.3% which were sprouted and grown under blue and white lights. Nitrite radical scavenging activity of sprouts were most decreased compared with the control when grown under the red light by 57.4mg${\cdot}L^{-1}$. And mushroom tyrosinase inhibition activity of rape sprouts was extremely increased under the green light by 22.5mg${\cdot}L^{-1}$.

Anti-cancer Activity of Flavonoids from Aceriphyllum rossii (돌단풍(Aceriphyllum rossii)에서 분리한 플라보노이드의 항암활성)

  • Ahn, Eun-Mi;Han, Jae-Taek;Kwon, Byoung-Mog;Kim, Sung-Hoon;Baek, Nam-In
    • Applied Biological Chemistry
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    • v.51 no.4
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    • pp.309-315
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    • 2008
  • The methanol extract from the aerial parts of Aceriphyllum rossii was fractionated into ethyl acetate, n-BuOH and $H_2O$ layers through solvent fractionation. Repeated silica gel column chromatography of EtOAc and n-BuOH layers afforded five flavonol glycosides. They were identified as astragalin (1), kaempferol 3-O-${\alpha}$-L-rhamnopyranosyl (1${\rightarrow}$6)-${\beta}$-D-glucopyranoside (2), rutin (3), kaempferol 3-O-${\alpha}$-L-rhamnopyranosyl (1${\rightarrow}$4)-${\alpha}$-L-rhamnopyranosyl 1${\rightarrow}$6)-${\beta}$-D-glucopyranoside (4), and quercetin 3-O-${\alpha}$-L-rhamnopyranosyl (1${\rightarrow}$4)-${\alpha}$-L-rhamnopyranosyl (1${\rightarrow}$6)-${\beta}$-D-glucopyranoside (5) on the basis of spectroscopic data. All of them showed an inhibition in farnesyl protein tranferase (FPTase) activity, and rutin (3) inhibited the growth of rat H-ras cell and the cell migration of human umbilical vein endothelial cells (HUVECs).

Classification of Safflower(Carthamus tinctorius L.) Collections by Agronomic Characteristics (홍화의 작물학적 특성에 의한 품종군 분류)

  • Bang, Kyong-Hwan;Kim, Young-Guk;Park, Hee-Woon;Seong, Nak-Sul;Cho, Joon-Hyeong;Park, Sang-Il;Kim, Hong-Sig
    • Korean Journal of Medicinal Crop Science
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    • v.9 no.4
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    • pp.301-309
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    • 2001
  • This study was conducted to provide the basic information on safflower collections and to identify the variations which could be utilized in safflower breeding programs. The agronomic characteristics was used to clarify the genetic relationships among safflower collections and to classify them into distint genetic groups. There were 21 early maturing collections with less than 80 days in number of days from planting to flowering. The number of primary and secondary branches ranged ${3.8{\sim}14.8\;and\;0{\sim}26.9}$, respectively, and two collections, IT201434 and IT202723, were found to be high branch types. The 101 safflower collections were classified into 11 groups based on the complete linkage cluster analysis using agronomic characteristics. The I, II, III, IV, IX, X and ? groups included the 25%, 33%, 14%, 8%, 2%, 1% and 1% of the collections, respectively. All the collections in the group III were Korean landraces. The collections in group X could be characterized as early emergence, late flowering and high yield components such as the number of capitula per plant, number of seeds per capitula and seed weight per plant. The number of capitula per plant and seed weight per plant, i.e., the two main yield components, had the highly significant positive correlations with stem diameter, number of the primary branches, number of the secondary branches, number of leaves and leaf length.

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