• Analytical Science and Technology
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• v.6 no.2
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• pp.157-165
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• 1993

The potentiostatic etching dissolution method, which had been used for the quantification of precipitates in steel, was applied to investigate the origin of cracks occurred in 304 stainless steel during processing. The morphology of crack propagation was observed by SEM. EDS and EPMA were used for the analysis of chemical composition of large precipitates on the grain boundary. The crystal structure of these large precipitates was determined by X-ray diffraction and electron diffraction. In both a stainless steel plate and a wire, the crack propagated along the grain boundary. Large precipitates on the grain boundary were identified to be $M_2C$ and $M_{23}C_6$. Potentiostatic etching dissolution method was found to be appropriate to the sample preparation for the analysis of precipitates in stainless steel.

• Korean Journal of Materials Research
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• v.17 no.3
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• pp.179-183
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• 2007

A plate heat exchanger (PHE) normally uses vacuum brazing technology for connecting plates and fins. However, the reliability of high temperature brazing, especially with nickel-based filler metals containing boron the formation of brittle intermetallic compounds (IMCs) in brazed joints is of major concern. since they considerably degrade the mechanical properties. This research was examined the vacuum brazing of commercially SUS304 stainless steel with BNi-2 (Ni-Cr-B-Si) filler metal, and discussed to determine the influence of brazing temperatures on the microstructure and mechanical strength of brazed joints. In the metallographic analysis it is observed that considerable large area of Cr-B intermetallic compound phases at the brazing layer and the brazing tensile strength is related to removal of this brittle phase greatly. The mechanical properties of brazing layer could be stabilized through increasing the brazing temperature over $100^{\circ}C$ more than melting temperature of filler metals, and diffusing enough the brittle intermetallic compound formed in the brazing layer to the base metal.

• Journal of the Korean Ceramic Society
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• v.45 no.8
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• pp.472-476
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• 2008

The surface region of commercial stainless steel 304 and 316 plates has been modified through deposition of the multi-layered coatings composed of titanium film ($0.1{\mu}m$) and gold film ($1-2{\mu}m$) by an electron beam evaporation method. XRD patterns of the stainless steel plates deposited with conductive metal films showed the peaks of the external gold film and the stainless steel substrate. Surface microstructural morphologies of the stainless steel bipolar plates modified with multi-layered coatings were observed by AFM and FE-SEM images. The stainless steel plates modified with $0.1{\mu}m$ titanium film and $1{\mu}m$ gold film showed microstructure of grains of under 100 nm diameter. The external surface of the stainless steel plates deposited with $0.1{\mu}m$ titanium film and $2{\mu}m$ gold film represented somewhat grain growth of Au grains in FE-SEM image. The electrical resistance and water contact angle of the stainless steel bipolar plates modified with multi-layered coatings were examined with the thickness of the gold film.

• Proceedings of the Korean Vacuum Society Conference
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• 2012.08a
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• pp.268-268
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• 2012

Atmospheric pressure microwave induced plasmas are used to excite and ionize chemical species for elemental analysis, for plasma reforming, and for plasma surface treatment. Microwave plasma differs significantly from other plasmas and has several interesting properties. For example, the electron density is higher in microwave plasma than in radio-frequency (RF) or direct current (DC) plasma. Several types of radical species with high density are generated under high electron density, so the reactivity of microwave plasma is expected to be very high [1]. Therefore, useful applications of atmospheric pressure microwave plasmas are expected. The surface characteristics of SUS304 stainless steel are investigated before and after surface modification by microwave plasma under atmospheric pressure conditions. The plasma device was operated by power sources with microwave frequency. We used a device based on a coaxial transmission line resonator (CTLR). The atmospheric pressure plasma jet (APPJ) in the case of microwave frequency (880 MHz) used Ar as plasma gas [2]. Typical microwave Pw was 3-10 W. To determine the optimal processing conditions, the surface treatment experiments were performed using various values of Pw (3-10 W), treatment time (5-120 s), and ratios of mixture gas (hydrogen peroxide). Torch-to-sample distance was fixed at the plasma edge point. Plasma treatment of a stainless steel plate significantly affected the wettability, contact angle (CA), and free energy (mJ/$m^2$) of the SUS304 surface. CA and ${\gamma}$ were analyzed. The optimal surface modification parameters to modify were a power of 10 W, a treatment time of 45 s, and a hydrogen peroxide content of 0.6 wt% [3]. Under these processing conditions, a CA of just $9.8^{\circ}$ was obtained. As CA decreased, wettability increased; i.e. the surface changed from hydrophobic to hydrophilic. From these results, 10 W power and 45 s treatment time are the best values to minimize CA and maximize ${\gamma}$.

• Journal of Welding and Joining
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• v.32 no.6
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• pp.64-69
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• 2014

The applications by using fiber laser have increased recently. However, due to high beam quality of fiber laser, it is inappropriate to apply the existing laser welding monitoring technology to the fiber laser welding as it is. On this study, thus, we analyzed emission signal with RMS and FFT for the in-process monitoring during fiber laser welding. 12mm-thick 304L stainless steel sheet was used in fiber laser welding and the result showed as follows: The intensity changes in RMS did not clarify the distinction between full penetration and partial penetration. However, as welding speed increases, specific frequency also increases in regards of frequency analysis by using FFT.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 2002.10b
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• pp.173-174
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• 2002

To study the effects of mating materials on the tribological properties of DLC films. we used a ball-on-plate reciprocating friction tester in dry air and mating materials of martensite stainless steel (hardened, annealed SUS440C), austenite stainless steels (SUS304), and bearing steel (hardened, annealed SUJ2). At a light load of 0.6 N, the friction coefficient always exceeded ${\mu}>0.3$. Tribological properties of DLC film were still excellent above 0.6 N, except in sliding against annealed SUJ2. Analysis using micro-laser Raman spectroscopy showed that the difference between annealed SUJ2 and others materials appears mainly due to structural change in film.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2005.06a
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• pp.1087-1090
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• 2005

In precision machinery systems for medical and chemical applications, micropumps with a low pulsation have been demanded and investigated for accurate delivery of a small amount of liquid. This study proposes sheet type check valves instead of ball type check valves for PZT pumps and performs some tests on dynamics characteristics of check valves having different design parameter with variable frequency. The selected materials of check valves is NBR, PP film, Polyimide and Stainless steel(SUS304). In the experiment, dynamic characteristics of stainless steel thin plate have better performance than others.

• Journal of the Architectural Institute of Korea Structure & Construction
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• v.35 no.4
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• pp.157-165
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• 2019

Recently, lean duplex stainless steel, STS329FLD with less nickel (reduced to 0.5~1.5%) has been developed as a substitute of austenitic stainless steel (8%~10.5% nickel in STS304) and included in Korean standards (KS). This paper investigates the block shear behavior of cold-formed duplex stainless steel (STS329FLD, nominal plate thickness of 1.5mm) fillet-welded connection with base metal fracture. Main variables are weld lengths in the longitudinal and the transverse directions of applied force ranged from 20mm to 50mm. As a result, specimens failed by typical block shear facture (the combination of gross section tensile fracture and shear fracture or shear yielding) and ultimate strength of the specimens got higher with the increase of weld length. Block shear fracture strengths predicted by current design specifications (KBC2016/AISC2016 and EC3) and existing proposed equations for welded connections by Topkaya, Oosterhof & Driver and Lee et al. were compared with test strengths. KBC2016/AISC2016 and EC3 design specifications underestimated block shear strength of STS329FLD welded connections by on average 24%, 29%, respectively and Oosterhof & Driver, Topkaya and Lee et al's equations overestimated the ultimate strength of the welded connection by the range of 3% to 44%.

• Transactions of the Korean Society of Machine Tool Engineers
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• v.17 no.5
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• pp.1-10
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• 2008

Residual stress caused in the weldments with high restraint force are often during welding observed in the weldments of large size nozzles or radial tanks. The reason is that quantitative analysis about thermal stresses during welding is lack for this weldments. To verify Finite Elements Method(FEM) theory, the temperature was measured with thermocouple in a real time in this paper. Also analysis of the thermal stress for welding condition is performed by ABAQUS program package on various welding condition in 304 stainless steel butt welding.

• Transactions of the Korean Society of Mechanical Engineers
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• v.12 no.6
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• pp.1320-1326
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• 1988

This paper deals with the behavior of surface crack growth and the characteristics of surface micro-crack distribution under creep and creep-fatigue with 1 min. and 10 min. of load holding times at 593.deg.C, in air. The test specimen is a plate type with a small artificial defect of type 304 the small defect has been carried out by the surface replica method and optical microphotography. The experimental results have been interpreted from the view-point of fracture mechanics. It can be concluded that the longer the hold time the longer the total life time. Most of surface micro-cracks initiate at grain boundaries before the specimen reaches 20% of its total life time, a few of them lead to fracture by coalescence with the main crack.