• 조명전기설비학회논문지
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• 제28권5호
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• pp.115-121
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• 2014

The intrinsic simplicity, ruggedness, and simple power electronic drive requirement of a Switched Reluctance Motor(SRM) make it possible to use in many commercial adjustable speed application. The simple magnetic circuit results in a high efficiency drive and low temperature rise, and the drive system provides a good drive characteristics. This paper is provides two phase 4/3 SRM that is similar to two phase 6/3 SRM as aspect to magnetic structure. Although 6/3 SRM does not experience any flux reversal as the flux is in the same direction whether phase A or B is excited, but two phase 4/3 SRM experiences a flux reversal in small part of stator yoke. The flux reversal in two phase 4/3 SRM could be relieved by an adjustment of stator yoke structure. The magnetic analysis and design considerations of the two phase 4/3 SRM have been obtained by the finite element method analysis (FEM).

• Journal of Electrical Engineering and Technology
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• 제9권6호
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• pp.2194-2200
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• 2014

This paper presents a design of novel 2-phase 6/5 switched reluctance motor (SRM) for an air-blower application. This type of motor is suitable for the applications that require high speed and only one directional rotation as air-blower. The desired air-blower is unidirectional application, and requires a wide positive torque region without torque dead-zone. In order to get a wide positive torque region without torque dead-zone during phase commutation, asymmetric inductance characteristic with non-uniform air-gap is considered. The proposed motor can be operated at any rotor position. The proposed 6/5 SRM uses short flux path technique that achieved by means of winding configuration and lamination geometry. The purpose of short flux path is to reduce the core loss and the absorption MMF in the stator. The proposed 2-phase 6/5 SRM is verified by finite element method (FEM) analysis and Matlab-Simulink. In order to verify the design, a prototype of the proposed motor was manufactured for practical system.

• 조명전기설비학회논문지
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• 제28권5호
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• pp.92-97
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• 2014

The SRM is a doubly salient, singly excited machine. The torque is developed by the tendency for the magnetic circuit to adopt a configuration of minimum reluctance, i.e. for the rotor to move into in line with the stator poles and to maximize the inductance of the coils excited. It is common practice to combine them into groups of poles which are excited simultaneously; for example, 8/6 SRM (8 stator poles and 6 rotor poles) for 4 phases, 6/4, 12/8 SRM for 3 phases, 4/2, 6/3 SRM for 2 phases. Small number of phases in two-phase SRMs allows more cost savings with regards to the switching devices in the converter. The stator back irons of two phase 6/3 SRM and C-core 4/3 SRM does not experience any flux reversal as the flux is in the same direction whether phase A or B is excited. In this study, the similarities, the differences, and structural characteristics between the two SRMs was studied, The magnetic analysis also has been carried out by the finite element method analysis (FEM).

• 대한전기학회:학술대회논문집
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• 대한전기학회 2015년도 제46회 하계학술대회
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• pp.673-675
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• 2015

This paper presents a design of a high speed 2-phase 6/5 switched reluctance motor (SRM) for an air-blower application. This type of motor is suitable for the applications that require high speed and only one directional rotation as air-blower. The desired air-blower is unidirectional application, and requires a wide positive torque region without torque dead-zone. In order to get a wide positive torque region without torque dead-zone during phase commutation, asymmetric inductance characteristic with non-uniform air-gap is considered. The proposed motor can be operated at any rotor position. The proposed 6/5 SRM uses short flux path technique that achieved by means of winding configuration and lamination geometry. The purpose of short flux path is to reduce the core loss and the absorption MMF in the stator. The proposed 2-phase 6/5 SRM is verified by finite element method (FEM) analysis and Matlab-Simulink. In order to verify the design, a prototype of the proposed motor was manufactured for practical system.

• Journal of international Conference on Electrical Machines and Systems
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• 제1권2호
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• pp.38-45
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• 2012

A novel kind of switched reluctance motor (SRM) with short flux path is proposed in this paper. Phase excitation in the SRM gives short flux paths, hence reducing the magnetomotive force required to drive the machine, resulting in significant reduction of copper wire and core losses compared to the typical SRM with diametric circulation of magnetic flux. To verify the performance, the characteristics analysis of a double-stator SRM, a 6/5 SRM with C-core structure, and a 4/5 two-phase SRM, which all have short flux paths, and a comparison with conventional SR motors are executed. The comparison demonstrates that the proposed motor offers some advantages in terms of torque and efficiency.

• 약학회지
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• 제48권3호
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• pp.207-212
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• 2004

An analytic method was developed for the quantitation of $\Delta$$^{9}-$ tetrahydrocannabinol (THC) and 11-nor-9-carboxy THC (THC-COOH) in human hair. After hair samples were pulverized using Freezer Mill, deuterated internal standards were added and digested in 1 N NaOH at $100^{\circ}C$ water bath for 30 min. Digest solutions were extracted by 5 ml hexane：ethyl acetate (90：10) after acidification with acetic acid. The organic phase was evaporated under N 2 and derivatized by BSTFA (with 1% TMCS) at $85^{\circ}C$ for 45 min. The derivatized solution was separated on HP-5MS column ($30m{\times}0.25mm{\times}0.25mm$) and detected using EI-GC-MS with selective ion monitoring mode. The assay of calibration was ranged from 5 to 100 ng/50 mg hair ($r^2$＞0.99) for THC and THC-COOH. Within and between-run precision were calculated at 6, 30, 60 ng/50 mg hair with coefficients of variation less than 11%. Within and between run accuracies at the same concentrations were$\pm$14% and $\pm$30% of target for both analytes, respectively. Absolute and relative recovery at 10 and 100 ng were 60∼91％. The method was used to detect and quantify THC and THC-COOH in cannabis abuser's hairs (N = 16) and SRM (N=5, THC 1 ng/mg, NIST). We detected THC and THC-COOH in only one hair sample. In SRM, % accuracy was 93% (range 86∼103%) and precision (% CV) was 8.14. We began to set up a quantitative analysis of THC and THC-COOH using EI-GC-MS. Continuously, we need to modify and develop this method in order to apply for identification in cannanbis users' hair.

• Bulletin of the Korean Chemical Society
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• 제31권7호
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• pp.1976-1980
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• 2010

A simple and reliable method has been developed to selectively separate and concentrate trace amounts of Fe(III) ions from water and food samples by using flame atomic absorption spectrometry. A new reagent, 5-hydroxy-4-ethyl-5,6-di-pyridin-2-yl-4,5-dihydro-2H-[1,2,4] triazine-3-thione, was synthesized and characterized by using FT-IR spectroscopy and elemental analysis. Effects of pH, concentration and volume of elution solution, sample flow rate, sample volume and interfering ions on the recovery of Fe(III) were investigated. The optimum pH was found to be 5. Eluent for quantitative elution was 10 mL of 2 M HCl. The preconcentration factor of the method, detection limit (3s/b, ${\mu}gL^{-1}$) and relative standard deviation values were found to be 25, 4.59 and 1%, respectively. In order to verify the accuracy of the method, two certified reference materials (TMDA 54.4 lake water and SRM 1568a rice flour) were analyzed. The results obtained were in good agreement with the certified values. The method was successfully applied to the determination of Fe(III) ions in water and food samples.

• 한국환경보건학회지
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• 제35권4호
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• pp.322-333
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• 2009

In this study, a measurement method was evaluated for the determination of polycyclic aromatic hydrocarbons (PAHs) in the ambient atmosphere. PAHs were sampled by high-volume samplers, and were then analysed with a GC/MS system. Particulate PAHs were collected on $8"{\times}10"$ quartz fiber filter, while vapor phase PAHs were adsorbed on polyurethane foam (PUF). Target compounds included a total of 36 PAHs, which are known to be frequently detected in the urban atmosphere. It was not necessary to clean-up samples before samples were analyzed using GC/MS, and the overall performance of the method was tested by a variety of quality control and quality assurance schemes. It is generally known that the clean-up procedure can negatively affect the recovery of samples. Precision and accuracy was evaluated using SRM provided by US NIST, and the results were generally satisfactory and reliable. However, the GC/MS method appeared not to be adequate for 6-rings PAHs, such as coronene, due to its lower sensitivity. In addition, collection efficiencies for low molecular compounds, such as 2-rings PAHs, were poor because of the lower retention volume of the PUF adsorbent. As a result, it was concluded that the method based on high-volume sampling and GC/MS analysis can give very reliable data by simultaneous sampling of both particulate and vapor phases for 3-rings to 5-rings PAHs of environmental concern.

• 한국식품영양과학회지
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• 제44권3호
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• pp.418-424
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• 2015

본 연구는 식품성분표 개정을 위한 기초연구로서 농산식품인 조미료류 5개, 차류 2개, 채소류 2개, 곡류 3개, 견과류 및 종실류 6개, 유지류 2개, 과일류 20개에 함유되어 있는 기능성 영양성분 중 하나인 베타카로틴 함량을 분석하였다. 대표성과 신뢰성이 확보된 베타카로틴의 분석품질을 확보하기 위하여 참값을 알고 있는 표준인증물질인 slurried spinach(SRM 2385)의 베타카로틴 함량을 측정한 결과 RSD 1.73%였으며, 회수율은 102%로 아주 양호한 결과를 얻었다. 농산식품 분석 결과 채소류와 차류에서 비교적 높은 베타카로틴 함량이 검출되었다. 보리순가루 $17,293.95{\mu}g/100g$($2,882.33{\mu}gRE$), 보리순 생것 $2,755.15{\mu}g/100g$($459.19{\mu}gRE$), 녹차가루 $7,579.04{\mu}g/100g$($1,263.17{\mu}gRE$), 마른 녹차잎 $13,671.85{\mu}g/100g$($2,278.64{\mu}gRE$)으로 베타카로틴 함량이 비교적 높았다. 견과류 및 종실류의 베타카로틴 함량 분석 결과 검은 참깨 마른 것 $41.27{\mu}g/100g$($6.88{\mu}gRE$), 들깨 마른 것 $33.06{\mu}g/100g$($5.51{\mu}gRE$), 흰 참깨 마른 것 $25.36{\mu}g/100g$($4.23{\mu}gRE$) 순으로 베타카로틴 함량이 검출되었다. 유지류의 베타카로틴 함량 분석 결과 들기름 $58.56{\mu}g/100g$($9.76{\mu}gRE$)과 참기름 $11.41{\mu}g/100g$($1.90{\mu}gRE$)으로 측정되었다. 과일류 20개에서는 살구 생것 $2,280.35{\mu}g/100g$($380.06{\mu}gRE$)과 파파야완숙 생것 $242.57{\mu}g/100g$($40.43{\mu}gRE$), 파파야적숙 생것 $162.70{\mu}g/100g$($27.12{\mu}gRE$)으로 비교적 높은 베타카로틴 함량을 나타내었다. 거봉 생것, 청포도 생것, 켐벨얼리포도 생것의 경우 껍질을 포함하였을 때 베타카로틴 함량이 높게 측정되었다.

• 한국식품위생안전성학회지
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• 제32권2호
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• pp.89-95
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• 2017

에너지 음료는 카페인을 주성분으로 타우린, 비타민 같은 다른 energy-enhancing 성분을 함유하고 있다. 미국과 유럽에서는 글루쿠로노락톤이 에너지 음료에 첨가될수 있으나, 국내에서 의약품으로는 허가되어 있다. 따라서 식품 첨가물로는 그 사용이 금지 되어 있어, 지속적으로 수입 및 유통 음료에서 시험검사를 하여 규제하고 있다. 현재 분석법으로 사용하는 LC-PDA 법은 복잡한 유도체화 과정을 거치고, 음료 중에 당류들이 위양성 결과를 나타내기도 한다. 이런 기존 방법의 단점을 개선하기 위해 HILIC-ESI-MS/MS(hydrophilic interaction liquid chromatography coupled to electrospray ionization tandem mass spectrometry)를 이용한 분석법을 개발하고, 선택성, 직선성, 검출한계, 정량한계, 정밀도, 정확성, 재현성에 대하여 분석법 유효성 검증을 수행했고, AOAC, EURACHEM 가이드라인에 부합되는 결과를 얻었다.