• Title/Summary/Keyword: 2상 매질

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Elli-Situ 2000 (in situ, 실시간 표면 및 박막 모니터 장비)

  • 방현용;주한용
    • Proceedings of the Korean Vacuum Society Conference
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    • 2000.02a
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    • pp.46-46
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    • 2000
  • 과학기술 및 산업의 발달로 인하여 실험 중 또는 공정 상에서 in situ, 실시간으로 측정하고 분석하며 이를 되먹임하는 품질제어의 중요성이 대두되고 있다. 반도체 공정 또는 박막제조 공정 중에서 박막의 두께, 굴절율, 물질의 조성비 등을 알아내는 것이 긴요한 과제로 대두되고 있으며, 이를 위하여 공정중인 제품의 품질을 실시간으로 평가하는 장비가 요구되고 있는 것이다. 나아가 공정중의 예상하지 못한 시료의 특성변화를 그대로 감지하여 적절히 보정해 주는 되먹임 기법은 높은 수율을 보장하는 첨단기법이라 할 수 있다. 이러한요구에 부응할 수 있는 본 제품(Elli-situ 2000)은 박막의 두께 표면변화를 sub 의 정밀도를 가지고 in situ, 실시간으로 정밀 측정할 수 있는 첨단 계측장비로서 빛의 편광상태 변화를 측정하기 때문에 공정 중의 시료에 영향을 주지 않는 비간섭 특성과 비접촉 특성의 장점 뿐만 아니라 공기중에서는 물론 진공이나 액체 등의 매질에서도 사용될 수 있어서 매질에 대한 제약이 거의 없다는 장점도 가지고 있다. 편광상태의 제어 및 측정을 필요한 광학장비의 경우, 제작이 까다롭기 때문에 대부분 가격이 높은 편이고 사용방법이나 측정 데이터에 대한 해석이 어렵다는 단점이 있으나, Elli-situ 2000의 경우 상용화된 외국제품(국내제품은 없슴)과 비교하여 성능 및 가격경쟁력에 있어서도 우위에 있으며 간단, 명료한 장비조작 및 컴퓨터를 사용한 구동의 전자동화를 이룸으로써 초보자도 쉽게 측정하고 데이터를 처리할 수 있도록 하였다. 또한 취부대의 경우, 진공포트 플랜지의 표준규격(2-3" Del-Seal 플랜지 규격)에 맞춤으로써 기존의 진공챔버에 부착하여 진공에 전혀 영향을 주지 않는 상태에서 시료의 변화를 in situ, 실시간으로 정밀 측정할 수 있도록 하였다. 하였다.O 박막은 산소 가스압력과 기판온도, 인가 전류를 변화시켜가며 증착하였으며 이에 따른 박막의 결정성 변화를 알아보았다. 기판온도를 실온에서 점차 증가시켜나가면 $\Delta$$\theta$50은 급격히 감소하며 30$0^{\circ}C$에서는 결정성이 우수한 막을 얻을 수 있었다. 또한 산소 가스 압력이 0.5~1mTorr에서 $\Delta$$\theta$50은 양호한 값을 나타내었지만 그 이상에서는 c-축 배향성이 나빠짐을 확인하였다. 따라서 대향타겟식스퍼터 장치를 이용하여 ZnO 박막을 증착시 가스압력 0.5~1mTorr, 기판온도 20$0^{\circ}C$이상의 막 제작조건에서 결정성이 우수하게 나타나는 것을 확인할 수 있었다. gluten이 단단해졌음을 알수 있었다. 유화제 stearly 칼슘, 혹은 hemicellulase를 amarans 10% 대체한 밀가루에 첨가하면 확연히 비용적을 증대시킬 수 있다는 사실을 알 수 있었다. quinoa는 명아주과 Chenopodium에 속하고 페루, 볼리비아 등의 고산지에서 재배 되어지는 것을 시료로 사용하였다. quinoa 분말은 중량의 5-20%을 quinoa를 대체하고 더욱이 분말중량에 대하여 0-200ppm의 lipase를 lipid(밀가루의 2-3배)에 대하여 품질개량제로서 이용했다. 그 결과 quinoa 대량 7.5%에서 비용적, gas cell이 가장 긍정적 결과를 산출했고 반죽의 조직구조가 강화되었다. 또 quinoa 대체에 의해 전분-지질 복합제의 흡열량이 증대된 것으로부터 전분-지질복합제의 형성 촉진이 시사되었다.이것으로 인하여 호화억제에 의한 노화 방지효과가 기대되었지만 실제로 빵의 노화는 현저히 진행되었다. 이것은

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Determination of Hydraulic Conductivities in the Sandy Soil Layer through Cross Correlation Analysis between Rainfall and Groundwater Level (강우-지하수위 상관성 분석을 통한 사질토층의 수리전도도 산정)

  • Park, Seunghyuk;Son, Doo Gie;Jeong, Gyo-Cheol
    • The Journal of Engineering Geology
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    • v.29 no.3
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    • pp.303-314
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    • 2019
  • Surface permeability and shallow geological structures play significant roles in shaping the groundwater recharge of shallow aquifers. Surface permeability can be characterized by two concepts, intrinsic permeability and hydraulic conductivity, with the latter obtained from previous near-surface geological investigations. Here we propose a hydraulic equation via the cross-correlation analysis of the rainfall-groundwater levels using a regression equation that is based on the cross-correlation between the grain size distribution curve for unconsolidated sediments and the rainfall-groundwater levels measured in the Gyeongju area, Korea, and discuss its application by comparing these results to field-based aquifer test results. The maximum cross-correlation equation between the hydraulic conductivity derived from Zunker's observation equation in a sandy alluvial aquifer and the rainfall-groundwater levels increases as a natural logarithmic function with high correlation coefficients (0.95). A 2.83% difference between the field-based aquifer test and root mean square error is observed when this regression equation is applied to the other observation wells. Therefore, rainfall-groundwater level monitoring data as well as aquifer test are very useful in estimating hydraulic conductivity.

Assessment of Applicability of CNN Algorithm for Interpretation of Thermal Images Acquired in Superficial Defect Inspection Zones (포장층 이상구간에서 획득한 열화상 이미지 해석을 위한 CNN 알고리즘의 적용성 평가)

  • Jang, Byeong-Su;Kim, YoungSeok;Kim, Sewon ;Choi, Hyun-Jun;Yoon, Hyung-Koo
    • Journal of the Korean Geotechnical Society
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    • v.39 no.10
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    • pp.41-48
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    • 2023
  • The presence of abnormalities in the subgrade of roads poses safety risks to users and results in significant maintenance costs. In this study, we aimed to experimentally evaluate the temperature distributions in abnormal areas of subgrade materials using infrared cameras and analyze the data with machine learning techniques. The experimental site was configured as a cubic shape measuring 50 cm in width, length, and depth, with abnormal areas designated for water and air. Concrete blocks covered the upper part of the site to simulate the pavement layer. Temperature distribution was monitored over 23 h, from 4 PM to 3 PM the following day, resulting in image data and numerical temperature values extracted from the middle of the abnormal area. The temperature difference between the maximum and minimum values measured 34.8℃ for water, 34.2℃ for air, and 28.6℃ for the original subgrade. To classify conditions in the measured images, we employed the image analysis method of a convolutional neural network (CNN), utilizing ResNet-101 and SqueezeNet networks. The classification accuracies of ResNet-101 for water, air, and the original subgrade were 70%, 50%, and 80%, respectively. SqueezeNet achieved classification accuracies of 60% for water, 30% for air, and 70% for the original subgrade. This study highlights the effectiveness of CNN algorithms in analyzing subgrade properties and predicting subsurface conditions.

Determination of Copper Ion with 2-Mercaptobenzimidazol Immobilized on Surfactant-Coated Alumina (계면활성제를 코팅한 알루미나에 부동화한 2-Mercaptobenzimidazol을 이용한 구리이온의 정량)

  • Absalan, G.;Goudi, A.Aghaei
    • Journal of the Korean Chemical Society
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    • v.51 no.2
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    • pp.141-146
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    • 2007
  • The present paper describes a procedure for separation, preconcentration and determination of trace amount of copper in natural water samples by using 2-mercaptobenzimidazol as the complexing agent. The proposed method is based on the surfactant aggregation formed on γ-alumina by mixing sodium dodecyl sulfate and γ-alumina in water; 2-mercaptobenzimidazol was incorporated into inner hydrophobic part of produced ad-micelles in acidic media to produce an assemble suitable for preconcentration and determination of copper ion. Optimum experimental conditions for adsorption of μg/ml levels of copper ions from aqueous solution by the adsorbent have been reported. The copper ions were quantitively adsorbed by the sorbent over the pH range of 7.1-8.0 and were quantitatively desorbed afterward by using sulfosalycilic acid as the eluent. The determination of copper was not interfered in the presence of common metal ions. The procedure was applied for analysis of river water sample. Relative standard deviation was found to be 4.91%.

Cadmium Extraction from Solutions by Solid-Phase and its Trace Determination (고상에서 용액으로 부터 카드뮴 추출과 잔유물 측정)

  • Ashrafi, F.;Attaran, A.M.;Kermani, N. Memar
    • Journal of the Korean Chemical Society
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    • v.52 no.2
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    • pp.133-139
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    • 2008
  • A new sensitive and selective spectrophotometric method for determination of trace amounts of cadmium using a polyvinyl chloride membrane containing bis-(2-ethylhexyl)phthalate as a solid phase extraction medium was investigated. Bis-(2-ethylhexyl)phthalate has used as a plasticizer. Cd(II) in an aqueous solution was trapped on the membrane in the form of colorful Cd (II)-I- - MG complexes (which MG is malachite green) and the cadmium complex was concentrated in the membrane. The absorbance of the green membrane was measured at 629 nm using a spectrophotometer, and then, the concentration of the cadmium was calculated using a calibration curve, which expressed the relationship between the Cd(II) concentration and the membrane absorbance after coloring for 25 min. The calibration curve was linear in the range of 10-760 μgL-1 cadmium in the test solution. The detection limit based on the 3Sbl criterion was 1.8199 μgL-1 and the relative standard deviations (RSD) were less than 4 % (n=5). The proposed method has been successfully applied to the determination of trace amounts of cadmium in the Tadjan River water sample (Sari-Iran), and the mean value of 28.7 μgL-1 was obtained.

A Study on Flame Propagation Through a Mixture of H2/Air and Inert Particles with Radiation Effect (복사효과를 고려한 수소/공기/불활성입자 혼합물에서의 화염전파에 대한 연구)

  • Kim, Deok Yeon;Son, Jin Wook;Baek, Seung Wook
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.23 no.8
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    • pp.1040-1047
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    • 1999
  • The characteristics of flame propagation in inert particle-laden $H_2$/Air premixed gas are numerically investigated on this study. The 2nd order TVD scheme is applied to numerical analysis of governing equations and multi-step chemical reaction model and detailed transport properties are sued to solve chemical reaction terms. Radiation heat transfer is computed by applying the finite volume method to a radiative transfer equation. The burning velocities against the mole fractions of hydrogen agree well with results performed by different workers. The inert particles play significant roles in the flame propagation on account of momentum and heat transfer between gas and particles. Gas temperature, pressure and flame propagation speed are decreased as the loading ratio of particle is increased. Also the products behind flame zone contain lots of water vapor whose absorption coefficient is much larger than that of unburned gas. Thus, the radiation effect of gas and particles must be considered simultaneously for the flame propagation in a mixture of $H_2$/Air and inert particles. As a result, it is founded that because the water vapor emits much radiation and this emitted radiation is released at boundaries as radiant heat loss as well as reabsorbed by gas and particles, flame propagation speed and flame structure are altered with radiation effect.

A Study of Quality Control of Nuclear Medicine Counting System and Gamma Camera (핵의학 계측기기 및 감마카메라의 정도관리 연구)

  • 손혜경;김희중;정해조;정하규;이종두;유형식
    • Progress in Medical Physics
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    • v.12 no.2
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    • pp.103-112
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    • 2001
  • Purpose: The purpose of this study was to investigate the current status of performing nuclear medicine quality control in korea and to test selected protocols of quality control of nuclear medicine counting system and gamma camera. Materials and Methods: Fifty three hospitals were included to investigate the current status of nuclear medicine quality control in korea. The precision of dose calibrator and thyroid uptake system was measured with Tc-99m 35.52 MBq for 2 minuets and Tc-99m 5.14 MBq for 10 sec every one minute, respectively. The sensitivity of CeraSPECT$^{TM}$ with low energy high resolution parallel hole collimator was measured using two cylindrical phantoms with 15 cm in diameter and 12 cm and 30 cm in heights containing Tc-99m. The correction factor for sensitivity of CeraSPECT$^{TM}$ was calculated using phantom data. The system planar sensitivity, uniformity, count rate and spatial resolution were measured for Varicam gamma camera with low energy high resolution parallel hole collimator using 140 keV centered 20% energy window, 256$\times$256 or 512$\times$512 matrix sizes. Results: The quality control of dose calibrator and well counter were showed poor performance status. On the other hand, The quality control of gamma camera and other systems were showed relatively good performance status. The results of precision of dose calibrator and thyroid uptake system was $\pm$1.4%(<$\pm$5%) and chi^2=29.7(>16.92), respectively. It showed that the sensitivity of CeraSPECT$^{TM}$ was higher in center slices compared with the edge slices. After correction of nonuniform sensitivities for patient data, it showed better results compare with prior to correction. System planar sensitivity of Varicam gamma camera was 4.39 CPM/MBq. The observed count rate at 20% loss was 102,407 counts/sec (head 1), 113,427 counts/sec (head 2), when input count rate was 81,926 counts/sec (head 1), 90,741 counts/sec (head 2). The spatial resolution without scatter medium were 8.16 mm of FWHM and 14.85 mm of FWTM. The spatial resolution with scatter medium were 8.87 mm of FWHM and 18.87 mm of FWTM. Conclusion: It is necessary to understand the importance of quality control and to perform quality control of nuclear medicine devices.vices.

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Limitation of Natural Analogue Studies on Rock Matrix Diffusion (기질내에서의 확산작용에 관한 자연유사연구의 한계)

  • Kim, Chang-Lak;Chang, Ho-Wan
    • Journal of the Korean Society of Groundwater Environment
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    • v.1 no.2
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    • pp.100-104
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    • 1994
  • The rock matrix diffusion provides a retarding mechanism for sorbing and especially non-sorbing radionuclides. It has to be verified not only theoretically and experimentally but also from natural phenomena, before the mechanism can be incorporated fully into transport codes. The natural analogue studies, such as the concentration variation of radionuclides in profiles perpendicular to fluid-conducting fractures and to intrusive contact zones, have been believed to provide a validation. In thermal alteration zones of Naeduckri granite intruded by a pegmatite, large alkali and alkaline earth elements such as K, Rb, Sr, and Ba were moderately migrated during thermal alteration. Li, V. and Nb were also migrated about 9cm in width from the contact between the granite and the pegmatite. The concentration variation of these elements in thermally altered zones seems to be resulted from the local migration due to the re-equilibration among the elements released from the breakdown of primary minerals in the granite. Most of these natural analogue studies simply show only the concentration variation of elements without detailed informations on the diffusion time and other important data fir interpreting the behaviour of radionuclides, because of the absence of appropriate minerals for age data. Despite this problem, natural analogue studies will be needed for transport models of radionuclides in safety assessment.

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3D Numerical Study of Horizontal Falling Film Evaporator in Multi Effect Distillation (MED) Plant (MED 담수기내 수평관 강하막식 증발기의 3D 수치해석적 연구)

  • Kim, Soo Jae;Je, Junho;Kim, Moo Hwan
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.37 no.5
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    • pp.513-522
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    • 2013
  • In the present work, a numerical study of a horizontal falling film evaporator in a multi-effect distillation (MED) plant is performed. Tube bundles in the evaporator are described as porous media, and a volume-averaged method is applied. To calculate the fluid flow and phase change in the evaporator due to heat transfer in the system, FLUENT and user-defined functions (UDF) are used. To observe the performance of the evaporator under different operational conditions, tests are conducted for a steam mass flux ranging from 0.5 to 2.5 $kg/m^2s$ in the horizontal tube, for mass fraction of the noncondensable gas in the tube inlet ranging from 0% to 1%, and for film Reynolds numbers ranging from 100 to 1,000 for the falling film. The evaporation rate increases with the steam mass flux and Reynolds number. In contrast, the evaporation rate decreases by 0.87% with a 1% increase in the mass fraction of the noncondensable gas in the tube.

Simulation Anaysis on the Output Characteristics of XeF$(C\rightarrowA$ Excimer Laser Pumped by Electron-Beam (전자빔여기 XeF$(C\rightarrowA$ 엑시머 레이저의 출력특성에 대한 시뮬레이션 해석)

  • 류한용;이주희
    • Korean Journal of Optics and Photonics
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    • v.6 no.3
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    • pp.201-213
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    • 1995
  • By the use of computer simulation including collisional mixing kinetic processes of the B- and C-state in the upper laser level the output characteristics of electron-beam pumped XeF$(C\rightarrowA$ excimer laser are analyzed. We compared the results between experiments and simulations for the $XeF^*(C)$ formation that correlated the number of densities of the $XeF^*(B)$. We obtained good agreement$(28.5 mJ\pm5%)$ with comparisons between experiment and simulation and confirmed the optimal gas mixing ratio of $Xe/F_2/Ar=5.26/0.49/94.28%$ at atmospheric pressure laser medium under the condition of 70 ns [FWHM] electron-beam (800 kV, 21 kA). Also through the simulation we have investigated that the $XeF^*(C)$ formation channel, the $XeF^*(C)$ relaxation channel, and the absorption channel of bluegreen wavelength region as a function of F2 halogen donor and Xe partial pressure. ssure.

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