• Title/Summary/Keyword: 흡수법

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Development of Cellulose Strip for Dry Eye Inspection (건성안검사용 셀룰로즈 스트립 개발)

  • Lee, Myeonggu;Jeong, Myeong-jin
    • The Journal of the Convergence on Culture Technology
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    • v.5 no.4
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    • pp.355-359
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    • 2019
  • Schirmer test is one of the most used methods for the diagnosis of dry eye. We attempted to develop a tear level measurement tool to replace unreliable Schirmer test with inaccurate results. Absorbency tests for various absorbents were carried out. As a result, ${\alpha}$ cellulose pulp was selected as the absorbent. Prototypes were produced and evaluated twice. Finally a tear level measurement tool in the form of a strip of ${\alpha}$ cellulose pulp adhered to a polyurethane was prepared. Usability evaluation of prepared tear level measurement tool was performed. As a result, it was confirmed that it has a significant correlation with SM tube developed oversea recently. In addition, it was judged to be useful as an alternative to the Schirmer test in terms of measurement time and accuracy.

Implant-assisted removable partial denture for severely atrophied mandible (심한 하악 치조제 흡수를 가진 환자에서 임플란트를 이용한 가철성 국소의치로 수복한 증례)

  • Choi, Bada;Kim, Yeun Ju;Lee, Jae Hoon
    • The Journal of Korean Academy of Prosthodontics
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    • v.57 no.2
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    • pp.171-175
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    • 2019
  • Mandible with severe alveolar bone atrophy poses a significant challenge in terms of reproducing clinically acceptable anatomy for a removable prosthesis. To overcome this potential complication, altered cast impression technique is often recommended to capture accurate and functional gingiva tissues. It becomes possible to get proper anchors functional impression by placing 2 implants crowns which were impossible in previous implant overdenture impression technique. In this case, an 80-year old female patient with severe mandibular ridge atrophy was treated with an implant-assisted removable partial denture with two implant crowns on the canine area. An altered cast impression was taken with an individual tray on a metal framework of removable partial denture on both posterior edentulous areas. The patient was satisfied with the final prosthesis after failure of 2 previous prostheses. Clinician had a difficult time to manage disabled patient and patient were suffered with ill-fitting denture due to inaccurate impression in conventional overdenture condition. The oral rehabilitation was completed with placing 2 implants as proper anchor.

The Changes in Carbon Stocks and Emissions Assessment of Harvested Wood Products in Korea (우리나라의 수확된 목제품 탄소축적 변화량 및 배출량 평가)

  • Choi, Soo Im;Kang, Hag Mo
    • Journal of Korean Society of Forest Science
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    • v.96 no.6
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    • pp.644-651
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    • 2007
  • This study compared and estimated the changes in carbon stocks and emissions of harvested wood products (HWP) by applying FAO statistics and domestic statistics for Korean HWP production, import, and export volume, which is almost always supposed to be included in the carbon emissions and removals inventory by country in negotiations since the 2nd commitment period (2013~2017) of the Kyoto Protocol, for assessing the changes in carbon stocks and emissions of HWP. As a result, when applying FAO statistics to the changes in carbon stocks of HWP as of 2005, stock-change approach (SCA) was estimated at 1.434 Tg C, atmospheric-flow approach (AFA) -1.330 Tg C, and production approach (PA) 0.597 Tg C. When applying Korean statistics, SCA was estimated at 1.246 Tg C, AFA -11.520 Tg C, and PA 0.444 Tg C. When applying FAO statistics to $CO_2$ emissions and removals from HWP, SCA showed a decrease of $-5,258Gg\;CO_2$ (removals), AFA showed an increase of $4,877Gg\;CO_2$ (emissions), and PA showed a decrease of $-2,189Gg\;CO_2$ (removals). When applying Korean statistics, SCA showed a decrease of $-4,569Gg\;CO_2$ (removals), AFA showed an increase of $5,573Gg\;CO_2$ (emissions), and PA showed a decrease of $-1,628Gg\;CO_2$, (removals). Therefore, the application of FAO statistics was shown to be more beneficial for the estimation of both the changes in carbon stocks and emissions of HWP by all methods other than that of Korean statistics.

Method for Rapid Determination and Removal of Nitrogen Oxides in Flue Gases (Ⅰ). Rapid Determination on Nitrogen Oxides (배기가스중 질소산화물의 신속측정법과 그 제거에 관한 연구 (제1보). NO$_x$의 신속 정량법)

  • Yong Keun Lee;Tong Oh Seo;Kee Jung Paeng;Man Koo Kim;Kyu Ja Whang
    • Journal of the Korean Chemical Society
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    • v.29 no.1
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    • pp.52-60
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    • 1985
  • Oxides of nitrogen (NO$_x$) in exhaust gases was determined by absorbing the gas in alkaline peroxide solution containing 0.03${\%}$ H2O2 and 0.1N NaOH. About 100 ppm of NO$_x$ was rapidly oxidized to NO$_2$ or N$_2$O$_5$ by H$_2$O$_2$ and required a contact time of 2 minutes with the absorbing solution for complete absorption. With vigorous shaking including air or oxygen gas, high concentration of NO$_x$ (>200 ppm) can be absorbed within 30 minutes. The remaining H$_2$O$_2$ affect the absorbance of color solution strongly. However, the excess H$_2$O$_2$ was completely decomposed by zinc powder 0.5g and the sample solution should be adjusted to the pH range 6.1∼6.6 before the reduction so that conversion of nitrate to nitrite ion is possible. The absorbed NO$_x$ is determined colorimetrically by the diazotization-coupling method with sulfonilamide and NEDA as the coupling agent. The sensitivity of the new method was 4.48 ${\times}$ 10$^4$ as molar absorptivity which was high sensitive compared with that obtained for the usual zinc reduction NEDA method with O$_3$. This method was far more rapid, brief and accurate than previously published O$_3$-NEDA method in Korean industrial standard.

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The Magnetic Properties with the Variation of Sintering Temperature and Microwave Absorbing Characteristics of NiCoZn Ferrite Composite Prepared by Co-precipitation Method (공침법으로 제조한 NiCoZn Ferrite의 조성 및 소결온도에 따른 자기적 특성 및 전파흡수특성)

  • Kim, Moon-Suk;Min, Eui-Hong;Koh, Jae-Gui
    • Journal of the Korean Magnetics Society
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    • v.18 no.3
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    • pp.120-125
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    • 2008
  • In this study, NiCoZn ferrites with the variation of sintering temperature and chemical composition were prepared by the coprecipitation. Microstructures Crystal structure of NiCoZn ferrites were analyzed by XRD and their electric magnetic characteristics were analyzed by LCR meter and their morphology observed by SEM. We identified that these powders have a typical NiCoZn spinel structure and nanoparticles average size of 40 nm. The impurity, the initial permeability and the Q factor value are the lowest of sintered NiCoZn ferrite at $1250^{\circ}C$. Also, we measured S-parameter for $(Ni_{0.4}Co_{0.1}Zn_{0.5})Fe_2O_4$ which showed a maximum reflection loss of -3.1 dB at 6 GHz for the 2 mm thick sample. From this result, we found that the NiCoZn ferrite can be used in ferrite microwave-absorbing application at a higher frequency region (> 6 GHz).

Influence of Sustain Electrode Gap on Excited Xenon Atom in the Metastable State by Laser Absorption Spectroscopy in AC PDP (AC PDP에서 레이저 흡수법을 이용한 유지전극의 위치에 따른 제논 여기종 원자의 밀도 측정)

  • Lee, J.H.;Lim, J.E.;Lee, H.J.;Son, C.G.;Jeong, S.H.;Lee, S.B.;Yoo, N.L.;Han, Y.G.;Oh, P.Y.;Moon, M.W.;Ko, B.D.;Jeoung, J.M.;Moon, H.S.;Park, K.D.;Ahn, J.C.;Hong, J.W.;Cho, G.S.;Choi, E.H.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.05a
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    • pp.131-134
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    • 2005
  • PDP 방전 셀의 최적화 및 진공자외선 발광효율을 향상시키기 위한 목적으로 AC - PDP 미소방전에서 제논 여기종 원자의 밀도를 측정하는 레이저 흡수법을 개발하였다. 본 연구에서는 PDP 셀의 기체 압력을 350Torr, 제논 함량 10%로 고정하고, 전극 위에서의 여러 위치에서 준안정 준위 제논의 밀도를 흡수법으로 측정하였다. 실험 결과 제논 여기종의 밀도의 최대값은 전극의 위치(가장자리에서 안쪽으로의 거리)가 $50{\mu}m$, $120{\mu},\;150{\mu}m$ 일 때 $3.5{\times}10^{12}cm^{-3}$, $2.8{\times}10^{12}cm^{-3}$, $2.2{\times}10^{12}cm^{-3}$로 나타났다.

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Study on Absorption Characteristics of $CO_2$ in Aqueous Alkanolamine Solutions (알카놀아민 수용액을 이용한 이산화탄소 흡수특성 연구)

  • Oh, Sang-Kyo;Rhee, Young-Woo;Nam, Sung-Chan;Yoon, Yeo-Il;Kim, Young-Eun
    • Journal of Energy Engineering
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    • v.17 no.4
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    • pp.241-246
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    • 2008
  • Increase of $CO_2$ by using fossil fuels makes mainly global warming and the international efforts to reduce the $CO_2$ emission is being promoted. Absorption process using aqueous alkanolamine solution to remove acid components in the mixed gases has been used commercially. This method was used to remove $CO_2$ in the flue gas in recent years. $CO_2$ Absorption characteristics of several aqueous alkanolamine solutions such as MEA, DEA and AMP was studied by measuring vapor-liquid-equilibrium(VLE) and absorption velocity in this study. VLE measuring equipment, shell and reactor type, was used to acquire VLE data, equilibrium $CO_2$ pressure(${P_{CO_2}}^*$) and time at each pulse gas input. We also acquired the $CO_2$ absorption velocity by measuring the time to arrive the VLE at $40{\sim}80^{\circ}C$ and first gas input. The $CO_2$ absorption capacity of MEA 10wt% solution was higher than two alkanolamine solutions at $40^{\circ}C$ and the equilibrium $CO_2$ loading was 0.5. Absorption capacity was excellent as follows; AMP>DEA>MEA. But absorption velocity was fast as follows; MEA>AMP>DEA. Though good absorbent was considered by many variables, absorption velocity and capacity was more important factor.

Preconcentration of Copper(II) Using Mesoporous Organo-Silicas and Determination by Flame Atomic Absorption Spectrometry (메조다공성 유기-실리카를 이용한 구리(II)의 예비농축과 불꽃원자 흡수분광법으로의 정량)

  • Moghimi, Ali
    • Journal of the Korean Chemical Society
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    • v.52 no.2
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    • pp.155-163
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    • 2008
  • .A simple and reproducible method for the rapid extraction and determination of trace amounts of copper(II) ions using mesoporous organo-silicas mesoporous silica and atomic absorption spectrometry is presented. Common coexisting ions did not interfere with the separation and determination. The preconcentration factor was 100 (1 ml elution volume) for a 100 ml sample volume. The limit of detection of the proposed method is 1.0 ng ml-1. The maximum sorption capacity of sorbent under optimum conditions has been found to be 5mg of copper per gram of sorbent. The relative standard deviation under optimum conditions was 2.8% (n=10). Accuracy and application of the method was estimated by using test samples of natural and synthetic water spiked with different amounts of copper(II) ion.

투명전도막 변화에 따른 CIGS 박막태양전지 특성에 관한 연구

  • Son, Gyeong-Tae;Kim, Min-Yeong;Kim, Gi-Rim;Kim, Jong-Wan;Sin, Jun-Cheol;Jo, Seong-Hui;Im, Dong-Geon
    • Proceedings of the Korean Vacuum Society Conference
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    • 2014.02a
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    • pp.486-486
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    • 2014
  • CIGS 박막태양 전지는 I-III-VI2 Chalcopyrite 결정구조를 가진 화합물 반도체 태양전지로 인위적인 밴드갭 조작이 용이하여 효율 향상에 높은 가능성을 보이고 있다. 4원소 화합물인 CIGS 광흡수층의 대표적인 제조 방법으로는 co-evaporation 공정법이 있다. 동시 증발법은 CIGS 결정을 최적화하기 위하여 박막이 증착되는 동안 기판의 온도를 3단계로 변화시켜주는 3-stage 공정을 통하여 제작된다. 일반적으로 CIGS 박막태양전지는 전면전극으로 투명전도막이 사용되며 높은 광투과성과 전기전도성을 가져야 한다. 투명전도막의 광학적, 전기적 특성은 CIGS 박막태양전지의 효율에 영향을 미치기 때문에 최적화된 조건이 요구된다. 본 연구에서는 CIGS 광흡수층은 Ga/(In+Ga)=0.31, Cu/(In+Ga)=0.86으로 최적화 시켰으며, 투명전도막은 Al이 도핑된 ZnO 박막을 RF 마그네트론 스퍼터링법을 이용하여 증착하였다. ZnO:Al 박막의 두께를 가변하여 증착하였으며 박막의 특성을 평가하고, CIGS 광흡수층에 이를 적용함으로써 태양전지 변환효율 특성을 연구하였다. CIGS 박막 태양전지의 투명전극인 ZnO:Al 박막의 두께가 500 nm 일 때, Jsc=29.521 mA/cm2, Voc=564 mV, FF factor=71.116%, Efficiency=12.375%의 광 변환효율을 얻을 수 있었으며, 이에 따른 투명 전도막의 전기적, 광학적 특성을 통해 CIGS 박막태양전지에 미치는 영향에 대해 조사하였다.

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전구체 박막 증착법을 이용한 CuInSe2 박막 합성 및 결정화 메커니즘 분석

  • Lee, Dong-Uk;Choe, Yeong-U;Yong, Gi-Jung
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.08a
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    • pp.367-367
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    • 2011
  • 태양전지에서 광흡수층으로 널리 쓰이는 CuInSe2은 전기적, 광학적 특성이 우수하고 20%대의 고효율을 기록하며 큰 관심을 받고 있다. 하지만 증발법 및 스퍼터링 등의 기존 진공, 고온 기반 공정 기술은 원천적인 공정비용 절감이 어렵고, 고가의 희귀원소인 In 등의 원료 활용도가 떨어져 실험실 수준에 머무르고 있다. 최근 공정 비용을 최소화와 원료 활용을 극대화를 통해 고효율 CIGS 박막형 태양전지를 제조하기 위해 비진공 방식의 전구체 박막 코팅 및 열처리를 통한 광흡수층 제조에 관한 연구가 활발히 진행되고 있으며, 본 연구는 doctor-blade coating을 이용하여 전구체 박막을 기판 위에 형성하고 열처리 온도에 따른 박막 물성 변화를 관찰함으로써 박막 형성 메커니즘을 밝히는데 주력하였다. 또한 합성된 박막의 전기적, 광학적 특성을 분석하여 태양전지 응용 가능성을 살펴보았다. 본 연구에서는 SEM, XRD, TGA 분석을 통해 Cu, In, Se 전구체들이 각각 binary phase, 즉, Cu2-xSe 및 In2Se3의 metal chalcogenide을 형성하고, 고온에서 서로 결합하여 CuInSe2로 결정화 되는 현상을 관찰하였다. 또한 합성된 CIS 박막은 근적외선 및 가시광 영역에서 높은 광흡수도를 보였으며, 전기적으로 Mo 전극과 ohmic contact을 이룸으로써 CIGS계 태양전지의 광흡수층으로의 적합성을 나타내었다.

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