• Title/Summary/Keyword: 활성백토

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Pruification of Yellow Color from Gardenia(Gardenin jasminoides Ellis) for Development of Natural Food Color (천연식용색소 개발을 위한 치자 황색색소의 정제도)

  • 김희구;이상준
    • The Korean Journal of Food And Nutrition
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    • v.11 no.1
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    • pp.68-71
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    • 1998
  • In order make natural food color from gardenia(Gardenia jasminoides), we investigated optimal conditions of color extraction, in case of water extraction, optimal conditions for color extraction were 7$0^{\circ}C$, 48hrs, pH 7.0 and substrate 10%, respectively. And extracted crude color was purified by activated white clay, were isolated glycoside peak (238nm) and yellow color peak(40nm) from extracted crude color. The pruified color was increased by 27-fold and the yield was 96%.

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The Use of Activated Clay and Kieserguhr as a TLC Adsorbent(I) - Analysis of Tar Food Colorants - (박층(薄層) chromatography의 흡착제(吸着劑)로서 국내산(國內産) 활성백토(活性白土) 및 규조토(硅藻土)의 이용(利用)에 관(關)한 연구(硏究)(제일보)(第一報) - 식용(食用) tar색소(色素)의 분리분석(分離分析) -)

  • Kim, Byung-Soon;Chee, Bong-Ho
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.6 no.1
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    • pp.66-71
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    • 1977
  • An investigation of certain tar food colorants required a relatively inexpensive TLC adsorbent to be used in preparative thin-layer chromatography procedure. As will be shown activated clay and Kieselguhr has excellent physical characteristics for T LC applications, is easily applied, and is good for analytical work as well as showing good separator capabilities with selected groups of compounds. In addition to its usefulness its economical price suggested this article.

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A Study on the Relationship between the Pore Volume Distributions of Some Adsorbents Including Charcoal and the Rates of Adsorption of a Number of Cigarette Aerosol Ingredients such as Tar, Nicotine and etc. (활성탄을 포함하는 몇 가지 흡착제의 동공부피 분포와 이들의 흡착제에 대한 타르, 유기산 등 연초 에어로솔 성분의 흡착률과의 관련성)

  • Ick Kyun Kang;Sang Hyun Han;Yong Kwon Kim;Eun Hee Cha
    • Journal of the Korean Chemical Society
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    • v.33 no.4
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    • pp.350-356
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    • 1989
  • The analysis of adsortion behaviors of some cigarett aerosol ingredients such as tar, nicotine, carbon monoxide and a number of organic acids has shown that the rates of adsorption of the adsorbates of lower boiling point had increased in accordance with increasing cumulative pore volume, while that of higher doiling point decreased with increasing pore volume of smaller radius. The adsorbents used here were charcoal, silica gel, alumina, and activated clay. The common principle that the adsorbents of greater specific surface area adsorb the larger amount of adsorbates appeared to be disturbed in the adsortion of higher boiling point adsorbates. This confirmation was made mainly by analyzing the adsorption behaviors with regard to the pore volume distributions evaluated on the bases of desorption isotherms.

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Characteristics of Zeolites (Zeolite의 특성)

  • Im, Goeng
    • The Journal of Natural Sciences
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    • v.6 no.1
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    • pp.103-108
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    • 1993
  • Zeolites were discovered as a natural mineral more than two hundred ago. In the beginning, the mineral was used as ion-exchange material and adsorbent. After the end of World War II , however, a variety of zeolites have become available in large amounts because of the establishment of low temperature synthesis and the discobery of natural zeolite deposits of sedimentary origin. Various uses of xeolite were developed utilizing the unique crystal strucrure and function of these minerals. In connection with this development remakable progress has also been made in basic stuides on the related geology and mineralogy, crystallization from sols and gels, structure, ion exchange, adsorption and cataiysis. As a result, zeolites, which had been known only as mineral specimens displayed in museums. established a firm position among the high-technology masterials with excellent functional capabilities.

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Identification and Characterization of Homoharringtonine from Cephalotaxus koreana

  • Kim, Byung-Sik;Kim, Jin-Hyun
    • 한국생물공학회:학술대회논문집
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    • 2005.10a
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    • pp.566-569
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    • 2005
  • A novel purification method was developed for producing homoharringtonine from Cephalotaxus koreana, to guarantee high purity and yield. Our simple, efficient procedure for isolating and purifying homoharringtonine from C. koreanabiomass consisted of solvent extraction, synthetic adsorbent treatment, low-pressure chromatography, followed by high performance liquid chromatography (HPLC). The use of active clay treatment and silica gel low-pressure chromatography in the pre-purification process allowed for the rapid, efficient separation of homoharringtonine from interfering compounds and dramatically increased the yield and purity of crude homoharringtonine for high-performance liquid chromatography (HPLC) purification steps compared with alternative processes. Homoharringtonine could be obtained simply with high yield and purity from biomass using this purification method, while minimizing solvent use and the scale and complexity of HPLC operations for homoharringtonine purification. Purified homoharringtonine was identified and characterized.

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Refining of Squid Viscera Oil (오징어 내장유의 정제)

  • Ha, Jin-Hwan;Lee, Eung-Ho;Kim, Jin-Soo
    • Applied Biological Chemistry
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    • v.40 no.4
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    • pp.294-300
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    • 1997
  • As a part of basic investigation for utilizing by-products derived from marine food processing more effectively as a food source, refining of viscera oil of squid caught off Newzealand were investigated. In the process of refining, degumming with 3% of phosphoric acid at $60^{\circ}C$ for 30 min was effective in removing phosphatides, and optimal condition to neutralize was treating with 0.6% excess of 20% sodium hydroxide solution at $80^{\circ}C$ for 20 min. Bleaching was optimized by adding 10% activated clay and treating for $100^{\circ}C$ for 20 min under vacuum, and deodorizing was done by steam destillation at $180^{\circ}C$ for 60 min under 4 torr of vacuum. Acid value, peroxide value and chromaticity of refined squid viscera oil were 0.20, 0.8 meq/kg and 0.019, respectively. The ratio of polyenoic acid composition to saturated acid composition of refined squid viscera oil was 1.28 and its major fatty acids were 16 : 0, 18 : In-9, 20 : 5n-3 and 22 : 6n-3.

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Bleaching of Lipids Extracted from Single Cell Oil Produced by Mortierella sp. (모르티에렐라(Mortierella)속 유래 단세포유지로부터 추출한 지방질의 탈색)

  • Kim, Sun-Ki;Chung, Guk-Hoon;Han, Jeong-Jun;Cho, Sang Woo;Yoon, Suk Hoo
    • Korean Journal of Food Science and Technology
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    • v.47 no.3
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    • pp.405-408
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    • 2015
  • The deacidified oil obtained from the oleaginous fungus, Mortierella sp. (M-12) was bleached, after degumming, using activated clay under a 50-100 mmHg vacuum. The bleaching conditions were partially optimized as follows: activated clay, 1%, bleaching temperature $90^{\circ}C$, and treatment time 20 min. After bleaching, the color of bleached oil as determined by the Lovibond Tintometer, satisfied the specification for edible fats and oils. The bleaching process also decreased the contents of free fatty acids and phosphorus in the deacidified oil. The acid value of the bleached oil also satisfied the specification for edible fats and oils. It was early shown that the normal bleaching process can be used for the bleaching of heavily-colored microbial lipids for human consumption.

A Comparision Study of LDPE Pyrolysis over Resin Additives and Inorganic Compounds of Silica Alumina Type (수지첨가제와 실리카알루미나 계열 무기물이 LDPE 수지의 열분해에 미치는 영향 비교 연구)

  • Bak, Young-Cheol;Choi, Joo-Hong;Kim, Nam-Kyung
    • Journal of Korean Society of Environmental Engineers
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    • v.28 no.6
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    • pp.596-602
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    • 2006
  • The effects of resin additives and inorganic compounds addition on the thermal decomposition of low density polyethylene(LDPE) resin have been studied in a thermal analyzer(TGA, DSC) and a small batch reactor. The silica-alumina type compounds tested were kaolinite, bentonite, perlite, diatomaceous earth, activated clay and clay. The resin additives were antiforgging-agent and longevity-agent. As the results of TGA experiments, addition of antifogging-agent, longevity-agent and clay increased the temperature of the maximum reaction rate($T_{max}$). The silica-alumina type inorganic materials increased the pyrolysis reraction rate in the order of activated clay, diatomaceous earth, bentonite, perlites, and kaolinite. In the DSC experiments, addition of antifogging-agent and clay decreased the heat of fusion and the heat of pyrolysis reaction. Bentonite decreased 20% of the heat of fusion and 25% of the heat of pyrolysis reaction. In the batch system experiments, the mixing of clay retarded the initial producing rate of fuel oil, but increased the yield of fuel oil. Addition of bentonite increased the yield of fuel oil from LDPE resin. Mixing of antifogging-agent and longevity-agent produced the fuel oil having lower carbon number. The amounts of the carbon number below 12 in fuel oil decreased with adding the clay. That below 23 in fuel oil increased with mixing of bentonite, perlite, kaolinite, and activated clay. But the mixing of diatomaceous earth did not affect the carbon contents of fuel oil from pure LDPE resin. In the silica-alumina type inorganic material used in this experiments, bentonite was the most effective from the pyrolysis heat, yields, and the characteristics of fuel oil.

Effects of Process Conditions on Sardine Oil During Bleaching and Deodorization (정어리유에 대한 탈색 및 탈취조건의 영향)

  • Kim, Chul-Jin;Ahn, Byung-Hak;Hwang, Sung-Yeon;Shin, Hyun-Kyung
    • Korean Journal of Food Science and Technology
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    • v.19 no.5
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    • pp.420-425
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    • 1987
  • For use of sardine oil as an ingredient of food and feed, crude sardine oil obtained by rendering was processed to RBD sardine oil. Alkali deacidification was found to be most efficient with a concentration of 2.5N NaOH and 0.5% excess level at $75^{\circ}C$. Treatment with activated clay alone at $105^{\circ}C$ for 20 min without air admission was effective in reduction of the color intensity of the oil without any formation of the conjugated dienes and trienes of polyunsaturated fatty acids. In deodorization process, as the temperature was increased, color of the oil was to become lighter. The amount of conjugated compounds was, however, increased drastically at higher temperatures above $180^{\circ}C$ for 1hr. and content of polyunsaturated fatty acids was significantly decreased.

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Studies on the Isolation, Refining and Utilization of Lecithin from Skipjack Viscera Oil 1. The Isolation and Refining of Lecithin (참치 내장유 중에서 레시틴의 분리, 정제 및 이용에 관한 연구 1. 레시틴의 분리 및 정제)

  • KIM Kui-Shik;JEONG Bo-Young;BAE Tae-Jin;OH Won-Suk
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.31 no.6
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    • pp.895-900
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    • 1998
  • In order to the effective utility of marine by-product, crude lecithin was isolated from skipjack viscera oil and the lecithin was refined by bleaching and deodorization. Crude lecithin was separated from the skipjack viscera oil degummed with 0.4 ml of citric acid per 100 ml of the oil. Bleaching was effected by adding $5\%$ activated clay and treating for $40^{\circ}C$ for 90 min under vacuum, and deodorization was effectively conducted by steam distillation at $130^{\circ}C$ for 60 min under 4 ton of vacuum. The major fatty acids of the skipjack viscera oil. were 16:0. 18:1 (n-9), 22:6 (n-3), 18:0, and 16:1 (n-7). Crude and refined lecithins contained more aproximately $7\~18\%$ of 22:6 (n-3) than raw oil, the skipjack viscera oil.

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