• Title/Summary/Keyword: 합성 제어

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$In_2O_3$ Thin Film Ozone Sensor Prepared by Sol-Gel Method (졸-겔법을 이용한 $In_2O_3$ 박막의 오존 센서)

  • Lee, Yun-Su;Song, Kap-Duk;Choi, Nak-Jin;Joo, Byung-Su;Kang, Bong-Hwi;Lee, Duk-Dong
    • Journal of Sensor Science and Technology
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    • v.10 no.2
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    • pp.101-107
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    • 2001
  • A highly selective, sensitive and reliable ozone sensing $In_2O_3$ thin film was fabricated by a sol-gel method. The fabricated film is operated at a relatively lower temperature than ever developed thin films and saved operating power. $In_2O_3$ films deposited by sol-gel technique has been recently attracted because it is an economical and energy saving method and precisely controlled microstructure. Indium alkoxide precursor was synthesized from the reaction between indium hydroxide and butanol. PVA binder was used to improve adhesion of the films. The $In_2O_3$ thin films were obtained by spin coating from 1 to 5 times followed by drying at $100^{\circ}C$ and calcining at $600^{\circ}C$ for 1h. The film thickness was controlled by the number of coating time. The morphology and the thickness of the $In_2O_3$ films were examined by a SEM and XRD. The $In_2O_3$ thin films show a high sensitive to ozone gas at operating temperature of $250^{\circ}C$. The $In_2O_3$ sensor has very good selectivity to $CH_4$, CO, $C_4H_{10}$ and ethanol.

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Deterioration Diagnosis and Conservation Treatment of the Three-storied Stone Pagoda in the Cheongryongsa Temple, Anseong, Korea (안성 청룡사삼층석탑의 풍화훼손도 진단과 보존처리)

  • Lee, Sun-Myung;Lee, Myeong-Seong;Jo, Young-Hoon;Lee, Chan-Hee;Jeon, Seong-Won;Kim, Ju-Ok;Kim, Sun-Duk
    • Economic and Environmental Geology
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    • v.40 no.5
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    • pp.661-673
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    • 2007
  • Rock materials of the three-storied stone pagoda in the Cheongryongsa temple in Korea are mainly composed of gneissose two-mica granite and fine-grained granite. This stone pagoda shows structural instability due to cracks and breaking-out of the stones. The surface properties of the stone is highly degraded by various inorganic pollutants and epilithic biospecies. Therefore, this study carried out comprehensive deterioration diagnosis by non-destructive methods, and some conservation treatments base on the diagnosis were carried out to reduce weathering progress. As the treatments, the biospecies and lichen that covering on the stone surfaces were removed by dry and wet cleaning, and degraded concrete applied to the pagoda for restoration in the past was removed and repaired with epoxy resin. Oxidized iron plates inserted between the rock properties were also substituted titanium stainless steels. After all processes are completed, we sprayed consolidant on the rock surface. Finally, the ground of the stone pagoda was rearranged using small rock aggregates, and the fence was established for control of artificial deterioration by visitors and environmental maintenance.

RSM-based Practical Optimum Design of TMD for Control of Structural Response Considering Weighted Multiple Objectives (가중 다목적성을 고려한 구조물 응답 제어용 TMD의 RSM 기반 실용적 최적 설계)

  • Do, Jeongyun;Guk, Seongoh;Kim, Dookie
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.21 no.6
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    • pp.113-125
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    • 2017
  • In spite of bulk literature about the tuning of TMD, the effectiveness of TMD in reducing the seismic response of engineering structures is still in a row. This paper deals with the optimum tuning parameters of a passive TMD and simulated on MATLAB with a ten-story numerical shear building. A weighted multi-objective optimization method based on computer experiment consisting of coupled with central composite design(CCD) central composite design and response surface methodology(RSM) was applied to find out the optimum tuning parameters of TMD. After the optimization, the so-conceived TMD turns out to be optimal with respect to the specific seismic event, hence allowing for an optimum reduction in seismic response. The method was employed on above structure by assuming first the El Centro seismic input as a sort of benchmark excitation, and then additional recent strong-motion earthquakes. It is found that the RSM based weighted multi-objective optimized damper improves frequency responses and root mean square displacements of the structure without TMD by 31.6% and 82.3% under El Centro earthquake, respectively, and has an equal or higher performance than the conventionally designed dampers with respect to frequency responses and root mean square displacements and when applied to earthquakes.

Design of Multimode Block Cryptosystem for Network Security (네트워크 보안을 위한 다중모드 블록암호시스템의 설계)

  • 서영호;박성호;최성수;정용진;김동욱
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.28 no.11C
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    • pp.1077-1087
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    • 2003
  • In this paper, we proposed an architecture of a cryptosystem with various operating modes for the network security and implemented in hardware using the ASIC library. For configuring a cryptosystem, the standard block ciphers such as AES, SEED and 3DES were included. And the implemented cryptosystem can encrypt and decrypt the data in real time through the wired/wireless network with the minimum latency time (minimum 64 clocks, maximum 256 clocks). It can support CTR mode which is widely used recently as well as the conventional block cipher modes such as ECB, CBC and OFB, and operates in the multi-bit mode (64, 128, 192, and 256 bits). The implemented hardware has the expansion possibility for the other algorithms according to the network security protocol such as IPsec and the included ciphering blocks can be operated simultaneously. The self-ciphering mode and various ciphering mode can be supported by the hardware sharing and the programmable data-path. The global operation is programmed by the serial communication port and the operation is decided by the control signals decoded from the instruction by the host. The designed hardware using VHDL was synthesized with Hynix 0.25$\mu\textrm{m}$ CMOS technology and it used the about 100,000 gates. Also we could assure the stable operation in the timing simulation over 100㎒ using NC-verilog.

Fabrication and Characterization of $La_{0.6}Sr_{0.4}Co_{0.2}Fe_{0.8}O_{3-\delta}$ Oxygen Permeation Membranes Prepared with Different Powders ($La_{0.6}Sr_{0.4}Co_{0.2}Fe_{0.8}O_{3-\delta}$ 산소 투과 분리막의 제조 및 특성)

  • Lim, Kyoung-Tae;Lee, Kee-Sung;Han, In-Sub;Seo, Doo-Won;Hong, Kee-Seog;Bai, Kang;Woo, Sang-Kuk;Cho, Tong-Lae
    • Journal of the Korean Ceramic Society
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    • v.38 no.10
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    • pp.886-893
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    • 2001
  • We synthesized $La_{0.6}Sr_{0.4}Co_{0.2}Fe_{0.8}O_{3-\delta}$ powders by coprecipitation, citration and solid-state reactions. The oxygen permeation membranes were fabricated by cold isostatic pressing of the synthesized powders, followed by sintering in air. All powders and membranes consist of perovskite phases. The coprecipitated powders showed the highest surface area ($7.5m^2/g$) but strontium deficiency was found during washing and filtering in the process. The membrane with lower relative density was fabricated by citration method. On the other hand, solid state reacted powders had high relative density (95%), and mechanical properties showed superior properties. Especially, the composition of the solid-state reacted powders was relatively well-controlled.

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A Study on Combustion Experiments of Multi Type Air-Conditioner Outdoor Units by Large Scale Calorimeter (라지스케일 칼로리미터에 의한 멀티시스템형 에어컨실외기의 연소실험에 관한 연구)

  • Min, Se-Hong;Bae, Yeon-Jun
    • Fire Science and Engineering
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    • v.25 no.6
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    • pp.168-177
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    • 2011
  • The combustion test for real box of AC outdoor unit has been performed in this study in order to estimate the fire hazard in multi-system type of AC outdoor unit which is currently used for commercial use. The result showed that in test, there was explosion inside of AC outdoor unit, and flame erupted and fire spread through upper side grill. And then this fire burnt the combustibles such as wires, electronic control board, heat exchange copper plate and plastics etc inside the unit, refrigerant gas pipe was burst due to fire, and accelerated the explosion and flame eruption to outside while the refrigerant was erupting. It is found in this test that the maximum heat release rate of AC outdoor unit is 5,830 kW, the maximum internal temperature measured with infrared camera and thermocouple is $1,201^{\circ}C$, maximum ambient temperature is $881^{\circ}C$, and flame rose higher than about 5 m. It is concluded that the fire in AC outdoor unit cause fire to combustibles around the unit, and may give big damage by generating the secondary fire. It is expected that the result obtained from the test on the real object may be applied to fire realization of AC outdoor unit and estimation of fire spreading to the combustibles around in the future computer simulation.

Antimicrobial Activity of Lysimachia clethroides Duby Extracts on Food-borne Microorganisms (식중독 미생물에 대한 큰까치수영(Lysimachia clethroides Duby)의 항균활성)

  • Han, Ji-Sook;Shin, Dong-Hwa
    • Korean Journal of Food Science and Technology
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    • v.33 no.6
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    • pp.774-783
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    • 2001
  • The ethanol extract of 77 species of edible and medicinal plants were examined antimicrobial activity against 5 strains of Listeria monocytogenes ATCC 19111, ATCC 19112, ATCC 19113, ATCC 19114 and ATCC 15313 by optical density using Bioscreen C. The ethanol extract of Siegesbeckia glabrescens Makino, Jeffersonia dubia Benth, Aquilaria agallocha Roxburgh, Lysimachia clethroides Duby and Nardostachys chinensis Batal. exhibited comparatively strong growth inhibition effect on 5 strains of L. monocytogenes at 1000 ppm level in broth. The minimum inhibitory concentration (MIC) of ethanol extract of Lysimachia clethroides Duby was $100{\sim}500\;ppm$ on 5 strains of L. monocytogenes. The MIC of the n-hexane and chloroform fraction of the extract were same concentration as $50{\sim}100\;ppm$. The n-hexane fraction of Lysimachia clethroides Duby showed strong growth inhibition at 25 ppm on Vibrio parahaemolyticus for 72 hr at $30^{\circ}C$ and at 50 ppm on Bacillus cereus and at 500 ppm on Staphylococcus aureus and Escherichia coli.

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An Analysis of PMF and Critical Duration for Design of Hydraulic Structure (수공구조물 설계를 위한 PMF 및 임계지속시간 분석)

  • Lee, Sang-Jin;Choi, Hyun;Shin, Hee-beom;Park, Sang-Kil
    • Journal of Korea Water Resources Association
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    • v.37 no.9
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    • pp.707-718
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    • 2004
  • This study is to analyze the Probable Maximum Flood(PMF) as a part of counterplan for the disaster prevention of hydraulic structures such as dams, according to recent unfavorable weather conditions. During the period of typhoon RUSA in August 2002, the rainfall recorded in Gang-loeng Province was 880mm a day and exceeded the scale of PMP made in 2001. Accordingly, the reconsideration of hydrologic criteria for dam design was inevitable. In the design of dams for flood controls, the design flood must be determined by introducing the concept of maximum values. When the duration of design rainfall is determined, it needs to use the critical duration which causes the maximum flood by the maximum runoff. In this study, we Investigate the variation of critical duration with hydrologic parameters used in three different synthetic unit hydrographs(Clark, Nakayasu and SCS methods). As a result, the total runoff calculated from 24-hour duration is larger than that calculated from the critical duration. We calculate also the hydrographs with three different time distribution models(Huff's 4-quartile, IDF curve and Mononobe) and compare those with measured hydrograph data. From this comparison, we propose that the Huff's 4-quartile model must be used to obtain the desirable data in the hydrologic design of dams.

Surface Modification of Li Metal Electrode with PDMS/GO Composite Thin Film: Controlled Growth of Li Layer and Improved Performance of Lithium Metal Battery (LMB) (PDMS/GO 복합체 박막의 리튬 금속 표면 개질: 리튬전극의 성장 제어 및 리튬금속전지(LMB) 성능 향상)

  • Lee, Sanghyun;Seok, Dohyeong;Jeong, Yohan;Sohn, Hiesang
    • Membrane Journal
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    • v.30 no.1
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    • pp.38-45
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    • 2020
  • Although Lithium metal battery (LMB) has a very large theoretical capacity, it has a critical problem such as formation of dendrite which causes short circuit and short cycle life of the LMB. In this study, PDMS/GO composite with evenly dispersed graphene oxide (GO) nanosheets in poly (dimethylsiloxane) (PDMS) was synthesized and coated into a thin film, resulting in the effect that can physically suppress the formation of dendrite. However, PDMS has low ion conductivity, so that we attained improved ion conductivity of PDMS/GO thin film by etching technic using 5wt% hydrofluoric acid (HF), to facilitate the movement of lithium (Li) ions by forming the channel of Li ions. The morphology of the PDMS/GO thin film was observed to confirm using SEM. When the PDMS/GO thin film was utilized to lithium metal battery system, the columbic efficiency was maintained at 87.4% on average until the 100th cycles. In addition, voltage profiles indicated reduced overpotential in comparison to the electrode without thin film.

Determination Method of Hydrocarbon Compounds in DME-LPG Blending Fuels by Gas Chromatography with Deans Switching (Deans Switching을 이용한 가스크로마토그래피에서 DME-LPG 혼합연료의 탄화수소 화합물 분석방법)

  • Youn, Ju Min;Park, Cheon Kyu;Yim, Eui Soon;Jung, Choong Sub
    • Korean Chemical Engineering Research
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    • v.50 no.2
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    • pp.353-357
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    • 2012
  • The new qualitative and quantitative analytical method for hydrocarbon compounds in DME-LPG blending fuel, mixing dimethyl ether (DME) with liquefied petroleum gas (LPG), by using gas chromatography (GC) was investigated. It is difficult to analyze all components of DME-LPG blending fuel by using single column in GC due to consisting of the non-polar LPG and the polar DME which is oxygen-containing compound. Therefore, it has been introduced the Deans switching system, which are useful for analyzing mixtures of a very different nature and/or target analytes in very complex matrix. This technique is to control the pressure between two columns and to selectively change the path of effluent flows to either one of two columns. As a result, we found that DME and LPG can be completely separated at the different columns and the determination of all hydrocarbon compounds in DME-LPG blending fuel can be achieved to this method qualitatively and quantitatively during the operation of one injection. In addition, this method can be applied to the determination of trace components of by-product, such as methanol, methyl formate and ethyl methyl ether, which will be derived from DME synthesis process.