• Title/Summary/Keyword: 표준가스

Search Result 436, Processing Time 0.024 seconds

Development of dimethyl disulfide gas CRM and stability test (다이메틸다이설파이드 가스 인증표준물질 개발 및 안정성 평가)

  • Kim, Young-Doo;Woo, Jin-Chun;Bae, Hyun-Kil
    • Analytical Science and Technology
    • /
    • v.19 no.6
    • /
    • pp.498-503
    • /
    • 2006
  • A type of dimethyl disulfide gas CRM in the ppb level was developed for the analysis of tracelevel odorous gas in environmental atmosphere. The concentration of dimethyl disulfide($(CH_3)_2S_2$) was $10{\mu}mol/mol$ level in the cylinder filled with nitrogen, 1500 psi. And the variability of the concentration for 2 years was about 0.14% due to the adsorption or instability of $(CH_3)_2S_2$. The gas standards produced simultaneously in 4 bottles and examined by GC-FID were shown with 0.4%, reproducibility of preparation and 0.25%, standard uncertainty due to weighing and purity. The relative expended uncertainty of 1.1%(95% of confidence level, k=2) was assigned to the certified value of $10{\mu}mol/mol$ level of $(CH_3)_2S_2$ after quantitative evaluation on the purity, mixing, weighing, analysis, adsorption and stability of dimethyl sulfide gas.

A Study for Pathological Observations on the HBr Combustion Toxity (병리학적 관찰을 통한 HBr의 연소 독성에 관한 연구)

  • Jo, Nam-Wook;Lee, In-Ku;Choi, Jae-Bum;Lee, Bong-Jae;Shin, Hyun-Jun
    • Proceedings of the Korea Institute of Fire Science and Engineering Conference
    • /
    • 2012.04a
    • /
    • pp.373-376
    • /
    • 2012
  • 건축 재료가 다변화됨에 따라 화재 시 발생되는 연소가스 또한 다양해지고 있다. 그중 HBr은 NES 713과 BS 6853에서 연소 가스의 독성 평가를 위해 측정되는 독성가스이다. 특히 산업안전물질보건자료(MSDS)에서는 HBr가스를 흡입할 경우 화상을 일으키며 호흡부전, 두통 등을 유발시킬 수 있고 50ppm의 HBr가스에 노출된 사람은 생명과 건강에 즉시 영향을 받을 수 있는 매우 유독한 연소가스이다. 본 논문에서는 HBr 표준가스를 사용하여 건축법에서 규정한 가스유해성 시험결과와 HBr가스에 노출된 mouse의 병리학적 관찰 결과를 비교 분석하여 HBr의 연소 독성에 관하여 연구를 진행하였다.

  • PDF

Prediction of Explosion Risk for Natural Gas Facilities using Computational Fluid Dynamics (CFD) (전산유체역학시뮬레이션을 이용한 도시가스 설비의 폭발위험성 예측)

  • Han, Sangil;Lee, Dongwook;Hwang, Kyu-Suk
    • Journal of the Korean Applied Science and Technology
    • /
    • v.35 no.3
    • /
    • pp.606-611
    • /
    • 2018
  • City natural gas is classified flammable hazardous gas and should be secured according to explosion risk assessment determined by Industrial Standard KS C IEC. In this study, leak size, ventilation grade and effectiveness were adopted to the KS C IEC for risk assessment in natural gas supply system. To evaluate the applicability of the computational fluid dynamics (CFD), the risk assessment was studied for four different conditions using hypothetical volume($V_z$) valuesfrom gas leak experiments, KS C IEC calculation, and CFD simulation.

Stability Study for B.T.X Gas in the Aluminum Cylinder (알루미늄용기에서 BTX 가스에 대한 안정성 연구)

  • 김용두;배현길;김병문;김광섭;허귀석;김진석;우진춘
    • Proceedings of the Korea Air Pollution Research Association Conference
    • /
    • 2003.11a
    • /
    • pp.356-357
    • /
    • 2003
  • 대기오염을 유발하는 가스 중 휘발성 유기오염물(VOC)의 가스성분에 대한 관심은 점점 높아지고 있다. 휘발성 유기오염물(VOC)가스 중 가장 대표적인 성분은 벤젠, 톨루엔, 자일렌으로서 주 발생원은 유해한 작업환경의 대기나 공장의 배기 가스, 또는 주변 주거 지역의 대기 등이다. 본 연구는 벤젠, 톨루엔, 자일렌을 측정하는데 있어서 표준가스로 사용하는 벤젠, 톨루엔 및 자일렌 교정용 혼합가스의 인증 값의 정확성 및 신뢰성을 유지하기 위하여 이들 성분을 조성으로 하는 혼합가스를 제조하고 단기 흡착성 정도 및 유효기간 설정을 위하여 안정도 조사를 수행하였다. (중략)

  • PDF

Results of a Round-Robin Test for the Draft International Standard on FT-IR Gas Analysis of Fire Effluents from a Cone Calorimeter (콘칼로리미터 연소가스 FT-IR 분석을 위한 국제표준 초안의 비교시험 결과분석)

  • Choi, Jung-Min;Park, Kye-Won;Jeong, Jae-Gun
    • Fire Science and Engineering
    • /
    • v.33 no.3
    • /
    • pp.1-8
    • /
    • 2019
  • The international standard for FT-IR gas analysis of fire effluents in ISO 5660-1 cone calorimeter has been being developed in ISO TC 92. A comparison of the round-robin test of WD 21397 was conducted with six participating laboratories in 2018. The test specimens were PMMA, rigid PU foam board, and PVC flooring. The measurement quantities were the time-to-ignition, peak heat release rate, total heat release, and effective heat of combustion for a cone calorimeter test and peak gas concentration, gas generation, and gas yield for FT-IR gas analysis. No outliers were identified. For the cone calorimeter quantities, the repeatability and reproducibility were 1.5% and 9.8%, respectively. For FT-IR gas analysis, the repeatability and reproducibility was 12.9% and 27.9%, respectively.

The Use of Gas Chromatograph for the Measurement of Engine Exhaust Gas Composition (엔진 배기가스 성분 측정 을 위한 Gas Chromatograph 의 이용)

  • 김승수;정영교
    • Transactions of the Korean Society of Mechanical Engineers
    • /
    • v.9 no.6
    • /
    • pp.743-749
    • /
    • 1985
  • In this study the usefulness of Gas Chromatograph for the measurement of engine exhaust gas composition was confirmed. It was found that the composition of standard gas which was used for the calibration of Gas Chromatograph should not be greatly different from that of exhaust gas. Although self-evident, it cannot be overemphasized that utmost attention should be paid to prevent even a minute amount of air being mixed into the gas throughout the sampling process.