• Korean Chemical Engineering Research
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• v.60 no.2
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• pp.300-307
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• 2022

Time-resolved serial femtosecond crystallography (TR-SFX) is a powerful technique for determining temporal variations in the structural properties of biomacromolecules on ultra-short time scales without causing structure damage by employing femtosecond X-ray laser pulses generated by an X-ray free electron laser (XFEL). The mixing rate of reactants and biomolecule samples, as well as the hit rate between crystal samples and x-ray pulses, are critical factors determining TR-SFX performance, such as accurate image acquisition and efficient sample consumption. We here develop two distinct sample delivery systems that enable ultra-fast mixing and on-demand droplet injecting via pneumatic application with a square pulse signal. The first strategy relies on inertial mixing, which is caused by the high-speed collision and subsequent coalescence of droplets ejected through a double nozzle, while the second relies on on-demand pneumatic jetting embedded with a 3D-printed micromixer. First, the colliding behaviors of the droplets ejected through the double nozzle, as well as the inertial mixing within the coalesced droplets, are investigated experimentally and numerically. The mixing performance of the pneumatic jetting system with an integrated micromixer is then evaluated by using similar approaches. The sample delivery system devised in this work is very valuable for three-dimensional biomolecular structure analysis, which is critical for elucidating the mechanisms by which certain proteins cause disease, as well as searching for antibody drugs and new drug candidates.

• Particle and aerosol research
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• v.13 no.4
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• pp.151-158
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• 2017

Electrostatic precipitator is widely used to remove particulate matters in indoor air and industrial flue gas due to low pressure drop and high collection efficiency. However, it has a low collection efficiency for the submicrometer sized particles. Electrospraying is a potential method to increase the particle charging efficiency, which results in increased collection efficiency. Although particle charging efficiency is highly dependent upon droplet size, the effective measuring method of the droplets is still uncertain. Tap water was electrosprayed in this study, and the images of electrosprayed droplets were taken with a high speed camera coupled with several visualization methods in order to measure the droplets size. The droplet size distribution was determined by an image processing with an image-J program. As a result, a droplet measured by a laser visualization, had a half size of that by a Xenon light visualization. In addition, the experimentally measured droplet sizes were a good agreement with the predicted values suggested by $Fern{\acute{a}}ndez$ de la Mora and Loscertales(1994).

• Transactions of the Korean Society of Mechanical Engineers B
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• v.28 no.9
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• pp.1093-1100
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• 2004

Numerical analysis of the heat transfer associated with droplet impact on a hot solid surface is performed by solving the equations governing conservation of mass, momentum and energy in the liquid and gas phases. The deformed droplet shape is tracked by a level set method which is modified to achieve volume conservation and to include the effect of contact angle at the wall. The numerical method is validated through the calculations for the cases reported in the literature. Based on the numerical results, the heat transfer rate is found to depend strongly on the droplet spread radius. Decreased advancing/receding contact angles enlarge the splat radius and in turn enhance the wall heat flux. The effect of impact velocity on the droplet spread is reduced as the droplet size decreases. Also, droplet atomization is observed to significantly enhance the heat transfer rate and the effect is pronounced for a smaller size of droplet. An existing model equation to predict the maximum spread radius is improved for application to a micro droplet.

• Journal of ILASS-Korea
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• v.16 no.2
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• pp.104-109
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• 2011

The present study investigated experimentally the spreading characteristics of a single liquid impinging on the inclined micro-textured aluminum (Al 6061) surfaces manufactured by using a micro computerized numerical control (${\mu}$-CNC) milling machine. The textured surfaces were composed of patterned micro-holes (diameter of $125\;{\mu}m$ and depth of $125\;{\mu}m$). In our experiment, the de-ionized (DI) water droplet of $4.3\;{\mu}l$ was impinged normally on the non-textured and textured surfaces at two different Weber numbers, and the droplet impinged on the inclined surfaces with different angles. A high speed camera was used to capture sequential digital images for measurement of the maximum spreading distance. It was found that for the textured surface, the measured apparent equilibrium contact angle (ECA) increased up to $105.8^{\circ}$, higher than the measured ECA of $87.6^{\circ}$ for the non-textured (bare) surface. In addition, it is conjectured that the spreading distance decreased because of a liquid penetration during droplet spreading through the holes, the increase in hydrophobicity, and viscous dissipation during impact process.

• Journal of ILASS-Korea
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• v.18 no.1
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• pp.9-15
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• 2013

Wall thinning of pipeline in power plants occurs mainly by flow acceleration corrosion (FAC), cavitation erosion (C/E), liquid droplet impingement erosion (LDIE). Wall thinning by FAC and C/E has been well investigated; however, LDIE in plant industries has rarely been studied due to the experimental difficulty of setting up a long injection of highly-pressurized air. In this study, we designed a long-term experimental system for LDIE and investigate the behavior of LDIE for three kinds of materials (A106B, SS400, A6061). The main control parameter was the air-water ratio (${\alpha}$), which was defined as the volumetric ratio of water to air (0.79, 1.00, 1.72). In order to clearly understand LDIE, the spraying velocity (${\nu}$) of liquid droplets was controled larger then 160 m/s and the experiments were performed for 15 days. Therefore, this research focuses relation between erosion rate and air-water ratio on the various pipe-flow materials. NPP(nuclear power plant)'s LDIE prediction theory and management technique were drawn from the obtained data.

• Journal of ILASS-Korea
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• v.17 no.1
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• pp.14-19
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• 2012

The present study conducts experimental investigation on spreading and deposition characteristics of a $4.3{\mu}l$ de-ionized (DI) water droplet impacting upon aluminum (Al 6061) flat and textured surfaces. The micro-textured surface consisted the micro-hole arrays (hole diameter: $125{\mu}m$, hole depth: $125{\mu}m$) fabricated by the conventional micro-computer numerical control (${\mu}$-CNC) milling machine process. We examined the surface effect of texture area fraction ${\varphi}_s$ ranging from 0 to 0.57 and impact velocity of droplet ranging from 0.40 m/s to 1.45 m/s on spreading and deposition characteristics from captured images. We used a high-speed camera to capture sequential images for investigate spreading characteristics and the image sensor to capture image of final equilibrium deposition droplet for analyze spreading diameter and contact angle. We found that the deposition droplet on textured surfaces have different wetting states. When the impact velocity is low, the non-wetting state partially exists, whereas over 0.64 m/s of impact velocity, totally wetting state is more prominent due to the increase kinetic energy of impinging droplet.

• Journal of the Korean Society of Visualization
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• v.18 no.1
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• pp.18-25
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• 2020

The droplet impact behavior is dominated by some parameters such as surface temperature, We number, surface and fluid property. Especially, Leidenfrost effect which prevents the contact between surface and droplet is very powerful phenomenon for determining droplet impact behavior. Due to this effect, the impact regime is divided into contact boiling regime and film boiling regime whether the droplet contact with the surface. Many studies have found that surface micro-structures which processed by surface processing are effective to overcome the Leidenfrost effect. In this study, droplet impact behaviors were compared using ethanol both on flat and laser-ablated Al surface. On the flat surface, impact regime was mainly divided by surface temperature. And there is key dominant parameter for each regime. On the laser-ablated surface, we could see changed impact regime and different impact behavior such as jetting and ejection of tiny droplets despite of same impact conditions.

• Journal of the Korean Society for Precision Engineering
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• v.29 no.9
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• pp.1020-1025
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• 2012

In this study, we fabricated the superhydrophobic and super-water-repellent surface with the micro/nano scale structures using simple conventional silicon wet-etching technique and the black silicon method by deep reactive ion etching. These fabrication methods are simple but very effective. Also we reported the droplet impact experimental results on the micro/nano-scaled surface. There are two representative impact behaviors as "rebound" and "fragmentation". We found the transition Weber number between "rebound" and "fragmentation" statements, experimentally. Additionally, we concerned about the dimensionless spreading diameters for our super-water-repellent surface. The novel characterization method was introduced for analysis including the "fragmentation" region. As a result, our super-water-repellent surface with the micro/nano-scaled structures shows the different impact behaviors compared with a reference smooth surface, by some meaningful experiments.

• Journal of ILASS-Korea
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• v.27 no.4
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• pp.188-194
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• 2022

In this study, the behavior of water droplet impacting on a thin horizontal orifice was investigated. The impact behavior modes, transition velocities and diameters of daughter droplets were analyzed by changing the droplet velocity, orifice diameter and orifice thickness. Four typical modes of impacting droplet on an orifice were observed. The single-droplet and double-droplet transition velocities increased with increasing the orifice thickness and decreased with increasing the orifice diameter. On the other hand, the multi-droplet transition velocity decreased and then increased as the orifice diameter increased. At thin orifice thickness, the single droplet diameter approximated the orifice diameter, and increasing the orifice thickness produced a droplet larger than the orifice diameter. In the case of double droplet mode, the diameter of the first droplet showed a similar tendency like the single droplet mode, but the diameter of the second droplet was smaller than that of the first droplet, and the difference between them was affected more by the orifice thickness.

• Journal of the Korean Society of Visualization
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• v.20 no.3
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• pp.10-18
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• 2022

We present an experimental investigation on emulsions created during the impact process between a surfactant-laden droplet and an oil layer on water. By varying the surfactant concentration and the viscosity of oil layer, we created emulsions and visualized them using multi-dimensional high-speed imaging. Our analysis shows that the emulsions are more likely to be unstable and decay within a minute if the impacting droplet contains more surfactant. We also found that there are three mechanisms of generation of emulsions depending on the concentration of surfactant and the viscosity of oil layer; the jet pinch-off, cavity pinch-off, and tearing of oil layer. Jet and cavity pinch-off turned out to be dominant mechanisms for high oil viscosities, while tearing of oil layer is dominant for low oil viscosities. Our result is potentially useful in designing optimal dispersant properties for offshore oil contamination.