• Journal of Welding and Joining
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• v.12 no.1
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• pp.38-43
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• 1994

고강도 알루미늄합금은 중량이 가벼우면서 인장강도와 항복강도가 높고 가공성, 성형성이 좋아 항공기, 자동차, 선박 등 수송용 재료로 각광을 받고 있으며, 이 중 Al-Zn-Mg계(7000계) 알루미늄 합금은 용접 구조물용 경량소재로 활용범위가 높다. Al-Zn-Mg계 알루미늄 합금은 고온에서 용체화 처리후 저온으로 급냉시킨 재료를 자연시효 또는 인공시효처리를 하여 이 때 석출되는 시효 석출물에 의해 강도를 증가시킨 석출 경화형 합금이다. 그런데, 7000계열 알루미늄합금은 적절한 열처리 작업을 통해 최적의 기계적 성질이 얻어지도록 합금설계가 되어있기 때문에 구조물 제작시 용접에 의한 ARC 열을 받게 되면 열이력(thermal cycle)에 의해 모재의 미세조직이 변화하고 용접 결함이 발생하며 강도의 약화와 함께 내식성 등이 저하한다. 따라서 고강도 알루미늄합금의 용접성을 향상시키기 위해서는 용접부의 미세조직거동과 용접부에 발생하는 용접결함의 현상을 조사하여 용접용 고강도 합금에 필수적으로 요구되는 용접성에 대한 검토가 충분히 이루어져야 한다. 따라서 본 고에서는 알루미늄합금, 특히 7000계열 알루미늄합금에 주목하여, 용접방법, 각종 결함과 대책, 용접부의 시효경화와 응력부식균열 및 기계적 성질 등을 지금까지 보고된 각종 자료를 기초로 하여 3회에 걸쳐 기술하고자 한다.

• Proceedings of the Korean Vacuum Society Conference
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• 2012.02a
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• pp.238-238
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• 2012

현재 국내 주얼리(gold alloy) 제품을 생산함에 있어 주조 방법은 크게 대기 중 주조(흡입주조) 방법과 진공주조 방법으로 나누어진다. 국내 주얼리 제조업체의 약 90%이상이 대기 중에서 주조하는 흡입주조방법을 통해 제품을 제작하고 있고, 국외의 경우, 대다수 진공주조방법을 통해 제품을 제작하고 있다. 본 연구에서는 주얼리 제품을 생산할 때 사용되는 합금재료(master alloy)가 동일한 조건에서 주조방법을 달리하여 각각 24개씩 총 48개의 14K yellow gold alloy 제품을 제작한 후 열처리를 통해 각각의 기계적, 물리적 특성분석을 비교 분석하였다. EPMA (Electron Probe Micro Analysis)분석을 통해 합금재료 및 제품의 구성성분을 조사하였고, ICP-MS (Inductively Coupled Plasma Mass Spectroscopy)를 사용하여 성분에 대한 정량분석을 실시하였다. 용체화처리(solid solution treatment)는 $700^{\circ}C$, 30분의 조건으로 실시하였고, 시효경화처리(age-hardening)는 $200{\sim}300^{\circ}C$의 온도범위에서 $50^{\circ}C$ 간격으로 실시하였다. 열처리 전과 후 시료의 grain 들의 배열 및 size 변화를 관찰하기 위해 식각 후 OM (optical microscope) 및 SEM (Scanning Electron Microscope)를 통해 분석하였다. 열처리 전 제품의 경도측정결과 대기 중 흡입주조방법 및 진공 주조방법을 통해 제작된 제품이 각각 119 Hv, 126 Hv로 나타났고, 용체화 처리 후 98 Hv, 92 Hv로 감소하였다. 시효경화 처리 후의 경도변화는 대기 중 흡입주조 및 진공주조방법을 통해 제작된 제품 모두 $270^{\circ}C$에서 각각 154 HV, 166 HV로 가장 높은 경도 값을 나타내었고, $270^{\circ}C$ 이상에서는 과시효(over aging)현상으로 인해 경도 값이 다시 감소하는 경향을 나타내었다. EPMA mapping 분석을 통해 주조방법에 따라 각각 제품의 구성성분분포도를 확인하였다. 이를 통해 열처리 전 다소 불균일하게 분포되었던 성분들이 열처리 후 균일해짐을 확인할 수 있었다.

• Analytical Science and Technology
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• v.18 no.5
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• pp.444-451
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• 2005

The accurate and simple extraction method for sterols and fatty acids in sesame oil was developed. The new method improved the extraction efficiency of sesamin in sesame oil and the ratio of sesamin over campesterol. It will be applied to judgement of adulteration of plant edible oils. The minor components of sterols were also confirmed. The simultaneous determination of sterols and fatty acids with derivatization were processed, but it was not enough to confirm adulteration, thus need more experiments.

• Magazine of the Korea Concrete Institute
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• v.6 no.3
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• pp.152-161
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• 1994

Most widened bridges have been constructed by the joining-construction method that makes new and existing bridges structurally a single structure. Since the joining-construction method has several problems in design and construction viewpoint, this study is conducted in order to investigate the structural behaviors of RC slabs, which are widened and influenced by traffic-induced vibration of existing bridge during placing and curing of new concrete, with the prototype flexural strength test and FEM analysis. It was found that cracks are generated in construction joint at low applied load and that stress concentration at the joints and slips between steel bar and concrete are occured. But, the decreasing of load carrying capacity is negligible according to the traffic-induced vibration as well as the difference of construction method.

• Korean Journal of Cognitive Science
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• v.15 no.4
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• pp.61-66
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• 2004

I think constructivism can be considered as the new count proposal for understanding human to Cartesian rationalism. Constructivism has the common area not only with recent results of evolutionary biology, evolutionary psychology. brain science, system theory, and complex adaptive system but also with recent trends of humanities, and social science. In artificial intelligence, the studies which can be considered as constructivistic methods is going on. In this paper, from a constructivistic pint of view, to broaden the concept of intelligence in artificial intelligenve, I will examine constructivistic methodologies to intelligent machine and look about the artificial intelligence techniques which are constructivistic. Throughout such a discussion I want to promote the integral understanding of various kinds of mind theories and techniques, and pave the way of general intelligence in artificial intelligence.

• Journal of Food Hygiene and Safety
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• v.8 no.1
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• pp.9-15
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• 1993

In an attempt to quantitate and qualitate residual antibiotics and antibacterial agents in meat simultaneously, we studied a gas chromatography-mass spectrometry(GC/M8) analysis. For a simultaneous analysis of penicillin G, chloramphenicol and thiamphenicol in meat, a simple and rapid clean-up procedure including extraction with 0.01 M EDTA-2Na Mcilvaine buffer (pH 4.0), defatting with n-hexane, and elution with 0.01M-methanolic oxalic acid from Bond Elute $C_{18}$ cartridge, and quantitation by selected ion monitoring (SIM) mode after derivatization was performed. The recoveries (%) of penicillin G, chloramphenicol and thiamphenicol (CV, %) at 1 ppm fortification level were 63.5 (7.6), 76.3 (8.1) and 84.7 (2.0), and the detection limits of those were 0.6, 0.085 and $0.084\;\mu\textrm{g}$ beef, respectively. This method using 81M mode allows excellent detection and quantitation of residual antibiotics and antibacterial agents in meat. Moreover, confirmation by a full scan electron impact mass spectrum is possible if residual level in the sample in above 1 ppm.

• Journal of Korea Technology Innovation Society
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• v.10 no.4
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• pp.687-705
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• 2007

Nowadays it is more important to measure the technological impact of a concerned R&D technology on others, when deciding or selecting strategically, under the environment such as more complex, more uncertain and more costly. But there was very few of proper methods to measure quantitatively. So we studied on measuring the technological impact of one group of technologies on others, which means the flow of disembodied knowledge, using patent citation analysis. We reviewed the prior art of the measurement of technological impact, and designs the effective citation analysis method using patent information, analyzing the prior art of patent citation analysis method and ie index. Finally, we developed the disembodied knowledge flow matrix between technology groups, counting citation frequencies between them, using KISTI's US patent database(USPA) and the index to represent the technological impact to others using the developed matrix as well as the intrinsic nature of the technological groups clustering by network analysis. The results of this study is to present the insight of a technological impact on the others quantitatively and this study aims at using them to refer to R&D budgeting and decision making in case of R&D planning or to the basic information to understand technology conversion or fusion.

• Korean Journal of Construction Engineering and Management
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• v.6 no.1 s.23
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• pp.65-72
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• 2005

The 3D objects far representing artificial element in building project can be easily organized in 4D system. However, the civil engineering projects need a composing technology of irregular triangulate network because the projects generally include earthwork of large scale that consists of cutting, filling, and excavating work. It Is very difficult to represent earthwork status as 3D object type because the earthwork in highway or railway projects is being progressed on the natural geographical features. That is, a composing technology of irregular triangulate networks necessary function to simulate natural site condition as 3D object in 4D system. This study suggests a new composing technology of irregular triangulate network that 3D objects can be automatically generated by attribute in each layer.

• Applied Biological Chemistry
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• v.40 no.5
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• pp.442-446
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• 1997

A new analytical method was developed by HPLC after supercritical fluid extraction and fluorogenic derivatization for the determination of quinclorac (3,7-dichloro-8-quinoline carboxylic acid) in soil. The graminicide quinclorac was extracted from soil by supercritical fluid extraction. Supercritical carbon dioxide at 7000 psi $(80^{\circ}C)$ modified with 30% of methanol extracted quinclorac from soil samples at the level of $0.1ng\;g^{-1}$ with 96% recovery. Extracted quinclorac was determined by HPLC as a fluorescent derivative. Derivatization was made with 4-bromomethyl-7-methoxycoumarin (4-Br-Mmc) using 18-crown-6-ether as a catalyst. The conversion was completed within 30 min and the limit of detection was 0.5 ppb to prove that the procedure could be used in the residue analysis of the pesticides containing carboxylic acid group.

• Journal of Welding and Joining
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• v.11 no.2
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• pp.53-61
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• 1993

One of the most interesting and promising steel groups considered for the rocket motor case, aircraft and aerospace component is the maraging(martensitic plus aging) nickel steel, developed by International Nickel Company in 1960. This material attains a very high strength with good fracture toughness by simple heat treatments which do not involve a quenching. Full strength can be obtained by "maraging" at 480.deg. for 3 hours for the 18% Ni maraging steel. The effect of heat treatments was considered on the residual stress field of 18% Ni maraging steel weldments. In experiments, various heat treatments such as stress relieve heat treatment, aging and solution heat treatment were carried out of the GTA weldments and the residual stresses were measured by using the hole drilling method. Whereas the conventional pattern of residual stress shows the stresses to be maximum along the weld centerline with tensile stress extending into the heat affected zone, the pattern in maraging steels shows the centerline stress to be compressive. After welding, a series of aging, solution heat treatment and solution heat treatment plus aging treatment were carried out and the residual stresses were measured to reveal that these heat treatments almost completely remove the welding residual stresses.