• 한국의상디자인학회지
• /
• 제11권3호
• /
• pp.135-141
• /
• 2009

In this paper, Tagetes extracts were extracted from leave, root, stem and flower at $100^{\circ}C$ for 20 minutes. Silk fabrics were dyed with Tatetes Patula L. to investigate the dyeing properties in accordance with dye concentration, pH, temperature, time of pre-, simul- and post-treatment of mordants using the three types of mordants. As a result, the surface color of the silk fabrics was yellowish regardless of the types of mordants. However, the a values were decreased and b values were increased in the order of the dyeing using Al>Cu>Fe: Al mordanted silk fabrics were appeared in greenish yellow and Fe mordanted silk fabrics were done in redish yellow. K/S values of the silk fabrics treated with Fe mordant were 3 times higher than those of Al and Cu mordants according to the increase in dye concentration. This behaviour was shown even in the increase of mordant concentration due to the interaction of mordant and pigments of Tatetes Patula L. But, the types of mordants did not affect because the equilibrium was obtained in 20 minutes in a similar way. And it showed that the highest K/S value of the silk fabrics studied was pH 4 and $80^{\circ}C$ regardless of the types of mordants.

• 한국의류학회지
• /
• 제39권4호
• /
• pp.601-612
• /
• 2015

This research investigated the dyeing behavior of palmatine (a major coloring compound of Phellodendron bark in addition to berberine) using mercerization (M), tannic acid (T), mercerization-tannic acid (MT), and tannic acid -mercerization (TM) pretreatments. Mercerization was conducted using $20^{\circ}C$ of 20% NaOH for 5 minutes. Tannic acid treatment was conducted using 15% o.w.f. solution of tannic acid at $60^{\circ}C$ for 30 minutes and fixed with potassium antimonyl tartrate trihydrate. Dyeing was conducted using 1% o.w.f. palmatine chloride hydrate with 1:100 liquor ratio at $10-95^{\circ}C$ for 10-60 minutes in a dyebath of pH 3-9. MT method resulted in the highest dye uptake and was two times higher than the average dye uptake of T method. MT method provided the best result when the dyeing temperature was $80^{\circ}C$ or $95^{\circ}C$ and the dyeing time was 60 minutes. The pH of the dyebath had less effect on the dye uptake but a pH higher than 5 provided better results. The study confirmed that palmatine is a major coloring compound of Phellodendron bark and that the MT method can be used as a successful cotton dyeing method.

• 한국의류산업학회지
• /
• 제13권5호
• /
• pp.778-789
• /
• 2011

The natural dyeing of silk fabrics with guava leaf extract was investigated. Mixed components of flavonoid and tannin seem to be the components of guava leaf extract. The temperature and time for dyeing of silk fabrics with guava leaf extract were $40^{\circ}C$ and $90^{\circ}C$ for eighty minutes, respectively. The dyeing equilibrium was shown at the fourth time of repeated dyeing. The highest K/S value was recorded at pH 3. Fe-mordanted fabrics showed the highest K/S value. High K/S values were shown in the post-mordanting of dyed fabrics at $40^{\circ}C$ and the pre-mordanting of dyed fabrics at $90^{\circ}C$. After repeated dyeing and mordanting, various color change occurred with mordant treatment. Surface colors were changed to YR color in alkaline water extract and to Y color in acidic water and ethanol extract, respectively. The washing fastness was level 3-4 for Sn-mordanted fabrics and level 4 for Fe-mordanted fabrics, and the dry cleaning fastness also showed very excellent result with level 4-5. The rubbing fastness was satisfactory with level 3-4. The light fastness was above level 4 only when Fe-mordanting was conducted, and the rest of dyed fabrics was not fast enough. In the antibacterial activity, the powder of guva leaf extract showed 99.9% of high antibacterial activity and Staphylococcus aureus showed 99.6% in dyed fabric. All dyed fabrics showed higher deodorization and UV protection rate than control fabric.

• 한국생활과학회지
• /
• 제18권6호
• /
• pp.1315-1321
• /
• 2009

The chemical composition of natural powder dye $Pinux^{TM}$ manufactured from Pinus radiata bark and dyeability of dyed silk fabrics with $Pinux^{TM}$ were examined. It is made up of the optimum dyeing condition of silk fabric according to the dyeing concentration, dyeing time, and dyeing temperature. Also, we examined the colorfastness and antibiosis of dyed silk fabrics to washing, rubbing, perspiration and light. For the analysis of the chemical composition of $Pinux^{TM}$, the total contents of phenolic compound, proanthocyanidin(PA) and anti-oxidative activities of the dye were analyzed. As a result, it was found that the main components of the $Pinux^{TM}$ manufactured from Pinus radiata bark is proanthocyanidin, mostly a flavonoid containing a procyanidin structure, and it consists of approximately 63% phenol. As a result of examining the dyeability of silk fabrics with $Pinux^{TM}$, it showed that the dyeability was best under the conditions of the concentration of dye $1{\sim}1.5%$(wt/v%), dyeing time of 90 minutes, and dyeing temperature at $90^{\circ}C$. It was found that the colorfastness of dyed silk fabrics, colorfastness to washing, perspiration for acidic and rubbing were as good as grade 4 or 4-5. However, the colorfastness to light was low at grade 1, the same as the results of other natural dyed fabrics. As a result of the antibiosis measurement for the $Pinux^{TM}$-dyed silk fabrics, it showed high antibacterial properties to Staphylococcus sureus at 99.6%.

• 한국지역사회생활과학회지
• /
• 제17권1호
• /
• pp.79-86
• /
• 2006

This study purposes to find the best one for dyeing with artemisia in order to develop a more efficient method of dyeing with artemisia and investigates the antibiotic activities of artemisia. After dyeing cotton, rayon, silk, wool and nylon fabrics with dyebath extracted from artemisia, observation on dyeability by temperature, concentration and time has been carried out. And I took an observation on color change, color fastness to washing and color fastness to light after mordanting treatment. Also observation on the antibiotic properties of non-dyed fabrics, artemisia-dyed fabrics and artemisia-dyed fabrics with post-mordant has been performed to investigate the antibiotic activities of artemisia. And the following results have been obtained. 1. The dyeability of artemisia was better for protein fabrics such as silk or woo and amide-based synthetic fabrics like nylon than for cellulose fabrics such as cotton and rayon. 2. For all tested fabrics, the dyeability was increased as the concentration of artemisia dyebath, dyeing time and dyeing temperature was increased. Especially the dye ability for protein fabrics was most affected by the temperature, and high dyeability was obtained at high temperatures. 3. For the color fastness of artemisia-dyed fabrics with mordanting treatment, the color fastness to washing was good with grade of 4-5 while the color fastness to light ranged from grade 2 to grade 3, which requires improvement for practical use. 4. The artemisia-dyed fabrics were shown to have much higher antibiosis than the non-dyed fabrics, and the artemisia-dyed fabrics with mortanting treatment showed the following result; Cu 99.9%, Al 64% and bittern 64.7%.

• 복식문화연구
• /
• 제18권2호
• /
• pp.371-381
• /
• 2010

The pine needles can be used for four seasons in normal living and it can be taken friendly everywhere as it is distributed over 50% in Korea. The pine needles consist of vitamins, protein, minerals, essential oil and enzyme related to antimicrobial activity. It has effect like high blood pressure, neuralgia and hanged over by terpene, glucokinin, rutin, apigenic acid and tannin. Also the extract of them can be used for dyeing of fabrics. However, the extract components and effects of them are not well known yet. Therefore, the purpose of this study was to investigate the volatile components of the pine needles extract and functionality. The pine needles extract was dyed into various fabrics(nylon, silk, wool and soybean) and mordanted with Al, Cu, Cr, Fe and Sn. The extracted aroma compounds were compared by gas chromatography-mass spectrometry. The major volatile compounds of pine needles verified by using SPME were alpha-pinene, beta-pinene, beta-phellandrene, caryophyllene, ethanon, benzen. A total of 15 compounds were identified by using the SPME fibers. In the UV-visible spectra, the maximum absorption of wavelength of the pine needles ethanol extract appeared at 460, 630nm for chlorophyll component and at 237, 281nm for tannin component with the pine needles distilled water extract. Most of sample showed high antibacterial effect in none mordant but wool fabric showed high antibacterial effect in mordants. The result of UV block test showed a superior ability of blocking ultraviolet ray infiltration in all sample.

• 한국의상디자인학회지
• /
• 제14권4호
• /
• pp.151-162
• /
• 2012

Regarding experimental study on the dyeing properties of natural dye, I have dyed silk fabric with Styphnolobium japonicum, sappan wood, and indigo. The results of the experiment have been analysed by wavelength of maximum absorption, K/S and CIE Lab chromaticity co-ordinated. The results are as follows: In case of complex dyeing using Styphnolobium japonicum and sappan wood, dyeing with sappan wood, which is red related color, after dyeing with Styphnolobium japonicum, which is yellow related color, is more efficient. When dyeing was maden by complex of Styphnolobium japonicum and sappan wood, Dyeing method by the order of "Styphnolobium japonicum${\rightarrow}$sappan wood${\rightarrow}$mordanting" made the best result of complex dyeing. In case of complex dyeing using Styphnolobium japonicum and Indigo, dyeing with Styphnolobium japonicum after the indigo made the best result. When dyeing with indigo first, and then Styphnolobium japonicum, yellow color was not well dyed, and low level of saturation caused lusterless color. Ordering of Styphnolobium japonicum${\rightarrow}$sappan wood${\rightarrow}$indigo made the best result of complex dyeing in case of complex dying with Styphnolobium japonicum and indigo. Dyeing order, sappan wood first and then indigo last method shown 560~640 nm wavelength of maximum absorption which most color was blue related. In contrast, Indigo first and then sappan wood method shown 460~560nm wavelength of maximum absorption which color was red related. Complex dyeing with sappan wood and indigo was showing lusterless color. In case of dyeing with red and blue, dyeing with sappan wood and indigo was not appropriate.

• 한국의류산업학회지
• /
• 제21권1호
• /
• pp.112-119
• /
• 2019

This study had a purpose of further investigating and developing the usage of the eco-friendly functional dye that has physiological and pharmacological functions. This study was implemented complex dyeing method which used both natural dyes such as Gardenia jasminoides J.Ellis colorant, which are the yellow dyes that have high brightness and low chroma, and Xanthium strumarium L. extract. The silk fabrics were used to dye in various methods. They were also used to investigate functionalities dyed fabrics by various treating method, such as their color fastness, antibacterial activities and deodorization, the following were obtained. The fabrics that were dyed with herbs had decreasing brightness as the herbs extract concentrations were increased and had subtly changing chroma. But, because their K/S values were under 0.5, they were not properly dyed. Color fastness differed according to the natural dyes and herbs' complex dyeing order. The Color fastness was good when the fabrics were dyed with the colorant first, and then with the herb. When the fabrics were dyed with mixture dyeing solution, the natural dye and the herb extract, the herb didn't affect the dyeabilities of fabrics as much. When the fabrics were dyed with the mixture of the colorant and the herb extract, the dyeabilities didn't have much changes. However, their color fastnesses were improved a little bit due to the complex dyeing condition. When the fabrics were dyed with the mixture of the colorant and the herbs extract, their antibacterial activities and deodorization were increased.

• 멤브레인
• /
• 제32권2호
• /
• pp.100-108
• /
• 2022

다양한 산업 중에서 섬유 산업은 섬유 염색을 위해 가장 많은 양의 물을 사용하는데, 이는 여러 종류의 염료를 포함한 폐수의 방대한 배출로 이어진다. 염료의 제거를 위한 방법에는 오존 처리, 흡착 등의 다양한 처리 방법이 존재한다. 하지만 이러한 처리 방법은 폐수 재사용의 문제로 인해 처리 가격이 상승하기 때문에 성공적이지 못하다. 이에 대한 대안으로 막분리 공정이 폐수의 염료 처리를 위한 가장 적절한 기술로 보고되고 있다. 이때 사용되는 분리막은 고분자 분리막과 세라믹 분리막으로 나눌 수 있다. 세라믹 분리막의 장점에는 세척의 용이함, 긴 수명, 내열성, 내화학성, 그리고 기계적 안정성이 있다. 세라믹 분리막은 다양한 원료로 만들 수 있으며, 점토, 제올라이트, 플라이 애시와 같은 천연 재료는 저렴하고 구하기 용이하다. 본 리뷰에서 폐수처리는 크게 한외여과(ultrafiltration), 정밀여과(microfiltration), 그리고 나노여과(nanofiltration) 세가지 공정으로 나누어져 있다.

• 한국염색가공학회지
• /
• 제33권4호
• /
• pp.202-209
• /
• 2021

Natural dyes are more expensive than synthetic dyes and the dyeing process, which is mainly immersion of dye, is complicated. For this reason, relatively small-scale production methods were predominant. However, awareness and interest in environmental sustainability is rising globally, and the use of synthetic dyes causes various environmental problems such as wastewater and CO₂ emission, so the consumption of natural dyes is increasing. In addition, interest in digital textile printing, an eco-friendly dyeing method that can produce products of various designs and uses less water, is growing. In this study, natural indigo dye (Indigofera tinctoria) was used as a raw material for Digital Textile Printing ink, and ¹⁴C (Biocarbon) present in it was measured to confirm whether it was derived from natural ingredients. The performance was confirmed by testing the pH, viscosity, electrical conductivity, surface tension, and particle size analysis of natural indigo ink. In addition, the performance of natural indigo DTP ink and printing fabric was evaluated by inspecting the change in color fastness and corresponding index substances before and after digital printing with natural indigo DTP ink on textiles. Through this, the possibility of commercialization of DTP ink and printing fabric using natural indigo was confirmed.