• Conservation Science in Museum
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• v.10
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• pp.43-61
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• 2009

The Buyeo National Museum was requested conservation treatment for wooden objects excavated from three Baekje archeological sites: Neungsan-ri, Ssangbuk-ri, and Gungnamji Pond. Prior to conservation treatment, analysis was conducted to identify the species used. The results of the analysis revealed wood from diverse species of trees including Hard pine, Cryptomeria japonica D. Don, Zelkova serrata Makino, Quercus spp., Platycarya strobilaceae S. et Z., Castanea spp., Torreya nucifera S. et Z., Taxus cuspidata S. et Z., and Salix spp. A high percentage of the objects were made of Cryptomeria japonica D. Don., a species native to Japan, which indicates that exchange with Japan was active at that time. Among the wooden objects, we analyzed lacquer fragments from six pieces of lacquerware, and the characteristics of the lacquer fragments were peculiar to specific artifacts. Most of the fragments were thicker than 100 ㎛. Pure lacquer and mixed black pigment were used. Infrared spectroscopy of the lacquered wooden fragments revealed that they had a very similar absorption band as refined lacquer, confirming that they were painted with lacquer. For their conservation, we immersed the objects in a high molecular weight aqueous solution of PEG#3,350 (10% → 50%) to strengthen them before vacuum freeze-drying.

• Membrane Journal
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• v.17 no.3
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• pp.174-183
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• 2007

The manufacturing process of metal membrane made of only metal mesh and both metal mesh and powder with using rolling process have been studied. In the rolling of metal mesh, selected metal meshes were rolled with the reduction ratio of 10%, 20%, and 30%, respectively. Such rolling process resulted in the decrease of mesh pore size through reduction the cross sectional area of mesh and changing the diameter of mesh wires. Also, it enhanced the filtration ratio of rolled mesh which is almost same as the filtration ratio of upper grade unrolled mesh and the reliability of membrane by making pore size distribution become more uniform. In fabricating metal powder layer onto metal mesh, using PVA(polyvinyl alcohol) as a binder of powder, drying the metal powder layer at $100^{\circ}C$ for 1 hr, and sintering it at $1,000^{\circ}C$ for 3 hr in vacuum were to be optimum conditions for obtaining good quality of metal powder layer on metal mesh with high pore density but no crack. With additional rolling of metal powder layer on metal mesh with 30% reduction before sintering, metal membrane which filtration ratio is about $0.7{\mu}m$ has been successfully manufactured.

• Journal of the Korean Society of Food Science and Nutrition
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• v.39 no.1
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• pp.8-13
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• 2010

The angiotensin converting enzyme (ACE) inhibition effect of soybean protein isolate hydrolysate was studied using protease. Soybean protein isolate was hydrolysed by seven enzymes (Alcalase 2.4 L, Flavourzyme 500 MG, GC 106, Multifect Neutral, Neutrase 0.8 L, Papain 30,000 and Protamex), enzyme concentrations (0, 0.5, 1.0 and 1.5%), at various hydrolysis times (0, 1, 2, 3, 4, 5 and 6 hr) and suspension concentrations (1, 5, 7, 10 and 15%). Absorbance at 280 nm, brix and ACE inhibitory activity of soybean protein isolate hydrolysates were investigated. Absorbance at 280 nm and brix of Alcalase 2.4 L treatment were higher than other enzyme treatments. The optimum condition of hydrolysis was Alcalase 2.4 L, 1% enzyme concentration, 5% suspension concentration for 4 hr. $IC_{50}$ value of ACE inhibitory activity of soybean protein isolate hydrolysate was $79.94 {\mu}g/mL$. These results suggest that soybean isolate protein hydrolysate from Alcalase 2.4 L may be of benefit for developing antihypertensive therapeutics.

• Korean Journal of Fisheries and Aquatic Sciences
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• v.15 no.1
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• pp.99-106
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• 1982

Vacuum-packed and seasoned-dried products of filefish, Navodon modestus, caught in large quantities in the coasts of Japan and Korea, were prepared tentatively and stored at $35^{\circ}C$ for $3\sim4$ months to test their keeping quality. Headed, eviscerated, ana skinned filefish were purchased from Tokyo central wholesale market and filleted. The fillets were seasoned with the seasoning powder prepared from sugar, sorbitol, salt, glutamate, 5'-ribonucleotide, and either beef flavor (Flava-Beef, Kyowa Hakko Kogyo Co. Ltd.), red pepper, or smoke flavor (Smok-EZ, Alpha Foods Co. Ltd.). After seasoning, the fillets were dried at $39\sim41^{\circ}C$ for several hours, vacuum-packed in the bag of plastic film, and cooked in water of $80^{\circ}C$ for 40 min. Two kinds of products different in moisture level were prepared : one containing moisture of $26\sim29\%$ and the other $40\sim46\%$. The moisture level, water activity, color value (L,a, and b values), texture, and viable counts of bacteria of these products were determined during storage at $35^{\circ}C$. From the results obtained, it became clear that the products could be preserved in good condition for $3\sim4$ months at $35^{\circ}C$, though they slightly decreased in the softness with decrease of moisture content and developed a pale brown during storage. Judging from organoleptic evaluation on the flavor, the products containing beef flavor as a seasoning was most desirable.

• Analytical Science and Technology
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• v.27 no.4
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• pp.187-195
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• 2014

It is very important to minimize the damage of latent fingerprints at enhancing the contrast. This study proves the enhancement effects of cyanoacrylate-fumed latent fingerprints using p-dimethylaminobenzealdehyde (DMAB) on semi-porous surfaces and the influence factors. The latent fingerprints in experiment were developed for cyanoacrylate treatment in a vacuum chamber and used after drying at room temperature for 24 hours. For fluorescence staining, the cyanoacrylate-developed marks using DMAB were sublimated during 48 hours under the different conditions of surface area, temperature, atmospheric pressure. First experiment showed how surface area effects on the sublimation rate and fluorescence intensity by DMAB of particle size and container size. In addition, the fluorescence staining using DMAB with solvent-free contact method had the greatest fluorescence intensity after 36 hours and a low fluorescence intensity over a certain size of surface area. Second experiment showed that the evaporation of DMAB solid crystals got a satisfying result in a temperature of $20^{\circ}C$ and reduced time to get the greatest fluorescence intensity. It took a long time to get a optimum level of fluorescence intensity at $30^{\circ}C$ or more and it was less effective in fluorescence intensity. Third experiment on the pressure indicated that the fluorescence intensity of vacuum was weaker than nonvacuum but it was inapplicable to very high variations in pressure.

• Korean Journal of Fisheries and Aquatic Sciences
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• v.16 no.4
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• pp.355-362
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• 1983

A vacuum-packed seasoned-dried product of sea mussel, Mytilus edulis, caught in the southern coasts of Korea, was prepared and stored at $35^{\circ}C$ for 70 days to test quality stability. Sea mussel, purchased from Jagalchi fish market in Busan, was steamed, shucked and eliminated byssus. The sea mussel meat was seasoned with the seasoning solution prepared with sugar, salt, sorbitol, glycerol, monosodium glutamate, 5'-ribonucleotide and smoke flavor (Smoke-EZ, Alpha Foods Co., Ltd.). After seasoning, the meat was dried at $52-58^{\circ}C$ for three hours, vacuum-packed in the laminated plastic film bag($14{\times}15cm$), and finally sterilized at $120^{\circ}C$ for 26 minutes in hot water circulating retort. The moisture, water activity, color value(L, a and b value), texture, TBA value and viable bacterial count of the products were determined during the period of storage at $35^{\circ}C$. From the results obtained, it became clear that the product could be preserved in a good quality for 70 days at $35^{\circ}C$, though a slight decrease in moisture content and development of a pale brown color was resulted. Judging from the sensory evaluation on flavor, the products containing smoke flavor were most desirable.

• Food Science and Preservation
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• v.18 no.1
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• pp.1-6
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• 2011

Kochujang-gulbi, a Korean traditional food, was prepared with kochujang and freeze-dried gulbi slices. Kochujang-gulbi was treated with high hydrostatic pressure (200, 400 and 600 MPa) and gamma-irradiation (7, 10, 20 and 30 KGy) to improve its quality and shelf-life. The pH of high hydrostatic pressure and gamma-irradiation treated kochujang-gulbi samples did not significantly different compared to that of control. However, Hunter L value slightly increased, and Hunter a and b values decreased by high hydrostatic pressure and gamma-irradiation treatment. During storage, the pH and color of high hydrostatic pressure and gamma-irradiation treated kochujang-gulbi samples did not significantly changed. The VBN and TBA level decreased by the increase treatment of high hydrostatic pressure and then slowely increased during storage. The VBN and TBA level of kochujang-gulbi samples treated by the strong gamma ray emission slowely increased during storage. In particular, gamma-irradiation treatment was very effective to sterilize microorganisms when compared to that of high hydrostatic pressure in kochujang-gulbi products. In addition, the high hydrostatic pressure and gamma-irradiation treated kochujang-gulbi samples shown significantly lower total viable cell number than control for the 20 days of storage at room temperature with retort pouch packaging.

• Journal of the Korean Society of Food Science and Nutrition
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• v.26 no.1
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• pp.54-59
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• 1997

After extracting Caridina denticulata denticulata, the raw material of salt-fermented Toha, with the use of water, ether, acetone and methanol in order, we had the antimicrobial activity test for nine strains of bacteria which are harmful to the human body and food. It is as follows; solvent extract yield of the powder of vacuum freeze dried Caridina denticulata denticulata was 52% of water fraction, 7.4% of ether fraction, 1.0% of acetone fraction and 0.8% of methanol fraction. The result of solvent extract antimicrobial search of Caridina denticulata denticulata said that with the sample of 20$\mu\textrm{g}$/disk, ether fraction resulted in clear one of 8~12mm, acetone fraction 8~12mm, methanol fraction 7~9mm and water fraction didn't have antimicrobial effect. The minimal inhibitory concentration of solvent extract of Caridina denticulata denticulata per area was that ether fraction was 250~500$\mu\textrm{g}$/$m\ell$, acetone fraction 125~500$\mu\textrm{g}$/$m\ell$ and methanol fraction 250~500$\mu\textrm{g}$/$m\ell$. The minimal bactericidal concentration of solvent extract per area of Caridina denticulata denticulata showed that ether fraction was 2, 500~10, 000$\mu\textrm{g}$/$m\ell$, acetone fraction 1, 250~10, 000$\mu\textrm{g}$/$m\ell$ and methanol fraction 5, 000~10, 000$\mu\textrm{g}$/$m\ell$.

• Proceedings of the Korea Water Resources Association Conference
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• 2007.05a
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• pp.296-300
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• 2007

우리나라에 내리는 대부분의 강수량은 6월${\sim}$8월의 장마기간 혹은 태풍의 영향으로 인해 발생한다. 특히 국지적으로 발생하는 집중호우로 인해 많은 인명, 재산 피해 등이 발생한다. 우리나라에서 집중호우로 인한 피해는 거의 매년 발생하고 있으며, 집중호우의 발생 지역은 특정 지역에 국한되어 있지 않다. 따라서 집중호우 발생으로 인한 피해 방지를 위해 사전에 충분한 준비를 해야 한다. 2006년 7월 8일부터 10일까지 3일 동안 진주지역 306.5mm, 합천지역 259.5mm, 산청지역 366.0mm의 집중호우가 발생하였으며, 이 기간 동안 이들 지역 외에도 전국적으로 태풍 에위니아(EWINIAR)의 영향으로 많은 호우가 발생하였다. 본 연구에서는 2006년 7월 진주지역 집중호우 특성 연구를 위해 진주지역 시강우 자료를 이용하여 자료를 분석하였다. 시강우 자료를 이용하여 진주지역 재현기간별 확률강우량을 산정하였고 2006년 7월 8일부터 10일까지의 강우분포형태를 설계강우분포형과 비교하였다. 또한 2006년 7월 발생했던 진주지역 집중호우의 무차원 누가곡선을 작성하여 분석을 실시하였다. 분석 결과 일최대 강우량의 경우 그 크기가 50년 혹은 80년 이내였으며, 강우분포형의 경우 하천정비기본계획의 경우 Mononobe 중앙집중형이였지만, 지난 호우의 경우 후방위의 강우가 연속적으로 발생한 형태였다. 또한 대부분의 강우가 6시간 이내에 내려 첨두홍수 발생에 많은 영향을 미쳤을 것으로 판단된다. 앞으로 이상기후와 같은 자연 현상에 대비하기 위해서는 단시간 호우에 대한 정확한 분석과 강우분포에 대한 연구가 더욱 필요할 것으로 생각된다.적자색의 미려한 결정이 석출되므로 이 결정을 여과하여 ethanol로 세척하고 진공 desiccator중에서 건조시켰다. 수득량 1.2~1.3g.)와의 조환가는 11.9565의 상인연소현상을 보였다. 삭과색(Y) 경색(R) 유전자간에는 어느것이나 연소현상이 보이지 않았다. 4. 단일반응성의 변이는 연소적이며 우성은 거의 인정되지 않았고 인자간의 상호작용도 인정되지 않았으며 상가적 유전을 보였다. 광의와 협의의 유전력은 각각 89.50%로서 실용적으로 대단히 높은 것으로 생각되었으며 단일반응성에 관여하는 유전자수는 2대의 인자로 추정하였고 다시 양친의 유전자형을 aabb AABB라고 측정하여 각인자의 작용가는 11.136일로 산출되었고 분해법에 의한 유전분석결과 유전자형의 관찰빈도분포와 이론빈도분포는 서로 잘 적합되었다. 단일반응성에 있어서 유전력이 대단히 높았으므로 비교적 초기세대에서 본 형질의 선발이 가능할 것 같았다. 5. 단일반응성과 엽형 및 엽병색 유전자와의 사이에 $F_2$, $BC_1$ 및 $BC_2$에서 각각 유의적인 상관관계를 볼 수 있었으므로 이들 형질간에 연소가 있는 것으로 인정되었다. 더욱 엽형과 엽병색과의 연소가 있는 것으로 인정되는 이상단일반응성 유전자와의 사이에 연소군이 인정된다. 6. 섬유중 유전자와 엽병색 및 엽형유전자와의 사이에 $F_2$$BC_1$ 및 $BC_2$에서 각각 유의적 상관관계를 볼 수 있었으므로 이를 형질간에 연소가 있는 것으로 인정되었다. 더욱 엽형과 엽병색과의 연소가 있는 것으로 인정되는 이상 섬유중 유전

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2002.11a
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• pp.29-29
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• 2002

공구강 등 산업용 재료로 널리 사용되는 카바이드 계 재료는 입자 크기 및 분포에 따라 기계적 성질이 변화하므로, 이를 제어하고 조절하는 기술에 관하여 많은 연구가 진행되어 왔다. 본 연구에서는 TiCN-WC-Co 복합초경계 에서 소결 공정 및 조성변화에 따른 입자 모양을 관찰하고 이에 따른 업자 성장 거동을 고찰하였다. 일반적으로 입자 조대화 양상과 고상 입자의 모양과는 밀접한 관계가 있다. 각진 입자의 경우에 는 계면이 원자적으로 singular 하여 원자의 홉착이 어렵기 때문에 임계값 이상의 성장 구동력을 받 는 몇몇 입자만 성장하는 비정상 입자 성장이 일어날 수 있다. 반면에 계면이 rough한 퉁큰 엽자의 경우에는 원자 홉착에 필요한 구동력이 존재하지 않아 성장 구동력을 받는 모든 입자들이 성장하기 때문에 정상 입자 성장을 하게 된다. 이와 같이 입자 모양에 따른 입자 성장 거동은 전체 미세구조를 결정하게 되며, 이에 따른 물리 화학적 물성을 변화시킨다. 이러한 입자 성장 원리를 적용하 면 복합초경계 (TiCN-WC-Co)에서도 입자성장이 억제되고 치밀한 소결체를 제조할 수 있을 것이다. 본 실험에서는 평균입도가 각각 0.1, 1.33, 2$\mu\textrm{m}$인 TiCN, WC, Co 분말을 사용하여 $((I00_{-x)}TiCN+_xWC)-30Co$ (wt%) 조성에서 TiCN/WC 비를 변화시키면서 업자 모양과 입자성장 거동을 관찰하였다. 청량된 분말은 WC 초경 볼로 밀렁하고, 건조한 후, 100 mesh 체로 조립화 하였다. 이 분말을 100 MPa의 압력으로 냉간정수압성형 하고 $10^{-2}$ torr의 진공분위기의 graphite f furnace에서 carbon black으로 packing 하여 액상형성 온도 이상에서 소결하였다. 소결된 시편은 경면 연마하여 주사전자현미경으로 미세 조직을 관찰하였다. TiCN-30Co 조성 시편은 corner-round 모양의 입자 모양으로 소결 시간 증가에 따라 빠른 입자 성장을 나타내었다 .(7STiCN+2SWC)-30Co 조성 시변의 경우 일반적으로 보고된 바와 같이 core/shell 구조를 나타내었으며, core는 TiC-rich 상이었고, shell은 (Ti,W)(C,N) 복합 탄화물 상이었다. WC 함량이 중가함에 따라 입자의 corner-round 영역이 증가하였으며 (SOTiCN-SOWC)-30Co 조성 근처에서는 거의 둥근 형태의 입자 모양을 나타내었다. 또한 TiCN - 30Co 조성 시편에 비하여 WC가 첨가된 시펀들은 작은 평균입자크기를 나타내었다. 본 연구의 결과는 shell 영역 조성 변화는 계면에너지 이방성과 기지상 내의 펑형 입자 모양을 변화시키고 나아가 입자 성장 속도 에도 영향을 미친다는 것을 보여준다.