• Korean Journal of Materials Research
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• v.22 no.3
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• pp.130-135
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• 2012

We present a method of graphene synthesis with high thickness uniformity using the thermal chemical vapor deposition (TCVD) technique; we demonstrate its application to a grid supporting membrane using transmission electron microscope (TEM) observation, particularly for nanomaterials that have smaller dimensions than the pitch of commercial grid mesh. Graphene was synthesized on electron-beam-evaporated Ni catalytic thin films. Methane and hydrogen gases were used as carbon feedstock and dilution gas, respectively. The effects of synthesis temperature and flow rate of feedstock on graphene structures have been investigated. The most effective condition for large area growth synthesis and high thickness uniformity was found to be $1000^{\circ}C$ and 5 sccm of methane. Among the various applications of the synthesized graphenes, their use as a supporting membrane of a TEM grid has been demonstrated; such a grid is useful for high resolution TEM imaging of nanoscale materials because it preserves the same focal plane over the whole grid mesh. After the graphene synthesis, we were able successfully to transfer the graphenes from the Ni substrates to the TEM grid without a polymeric mediator, so that we were able to preserve the clean surface of the as-synthesized graphene. Then, a drop of carbon nanotube (CNT) suspension was deposited onto the graphene-covered TEM grid. Finally, we performed high resolution TEM observation and obtained clear image of the carbon nanotubes, which were deposited on the graphene supporting membrane.

• Proceedings of the Materials Research Society of Korea Conference
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• 2003.03a
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• pp.82-82
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• 2003

p-CdI $n_2$T $e_4$ 단결정을 Bridgeman법으로 3단 수직 전기로에서 성장하였다. 성장된 결정의 결정성은 X선 회절과 광발광 측정으로 조사하였다 막 성장된(as-grown) 결정과 여러 열처리 CdI $n_2$T $e_4$ 결정들의 광발광 스펙트럼 측정으로부터 CdI $n_2$T $e_4$:Cd 광발광에서는 중성 주개 bound 엑시톤 ( $D^{\circ}$,X)가 우세함을 발견하였고 반면에 CdI $n_2$T $e_4$:Cd 광발광에서는 중성 받개 bound 엑시톤 ( $A^{\circ}$,X)가 완전히 사라졌다. 더우기, CdI $n_2$T $e_4$:Te의 광발광 스펙트럼에서 중성 받개 bound 엑시톤 ( $A^{\circ}$,X) 발광은 막 성장된 CdI $n_2$T $e_4$결정에서처럼 우세하였다. 이러한 결과들은 ( $D^{\circ}$,X)가 주개로써 작용하는 $V_{Te}$ ,와 관련이 있고, ( $A^{\circ}$,X)는 받개로 작용하는 $V_{cd}$와 관련이 있음을 가리킨다. p-CdI $n_2$T $e_4$ 결정은 Cd 증기 분위기에서 열처리한 후에는 n형으로 type conversion이 된다는 것을 알았다. 중성 주개-받개 bound 엑시톤 ( $D^{\circ}$, $A^{\circ}$)과 이들의 TO 포논 복제의 발광은 $V_{Te}$ 나 C $d_{int}$와 같은 주개들과 $V_{cd}$ 또는 T $e_{int}$와 같은 받개들 사이의 상호 작용과 관련이 있다. 또한, CdI $n_2$T $e_4$에서 In은 안정된 결합의 형태로 있기 때문에 자연 결함의 형성에는 관련이 없음을 알았다 알았다았다았다

• Journal of the Korean Vacuum Society
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• v.7 no.3
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• pp.187-194
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• 1998

InGaAsP epitaxial layers lattice matched to InP were grown at 600 and $620^{\circ}C$ by low pressure metalorganic chemical vapor deposition. Solid phase composition of group III was controlled by the diffusion flux gas phase to the reachion surface. For the case of group V, the difference of As and P vapor pressure and pyrolysis efficiency of $PH_3$and $AsH_3$ mainly determined their in corporation into solid. An abnormal behavior of peak energy shift was observed below 75K in temperature variant photoluminescence study. This abnormal behavior was explained by the difference in order of ordering which makes spatial variation of energy gap in InGaAsP layer and this explanation was supported by the analyses of transmission electron microscopy and transmission spectroscopy.

• Journal of the Korean Vacuum Society
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• v.15 no.5
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• pp.485-492
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• 2006

Two new copper(I) complexes with organic ligands, $[Cu^I(hfac)]_2(DVTMSO)$ and $[Cu^I(hfac)]_2(HD)$ (hfac=hexafluoroacetylacetonate, DVTMSO=1,2-divinylte-tramethyl-disiloxane, HD=1,5-hexadiene) were synthesized and used for copper metal-organic chemical vapor deposition. In these compounds, two Cu(hfac) fragments are bonded by one neutral ligand forming unusual structure with respect to other Cu(I) complexes. The compounds exhibited relatively high volatility and stability when compared to other copper(I) precursors. By using the reported compounds as precursors, a continuous Cu layer was not formed but the Cu islands were only observed. And the shape and size of Cu islands are significantly changed as a function of the substrate temperature.

• Journal of the Microelectronics and Packaging Society
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• v.16 no.4
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• pp.23-28
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• 2009

We investigated the wafer-level MEMS capping process for which cavity formation in Si wafer was not required. Ni caps were formed by electrodeposition on 4" Si wafer and Ni rims of the Ni caps were bonded to the Cu rims of bottom Si wafer by using epoxy. Then, top Si wafer was debonded from the Ni cap structures by using SnBi layer of low melting temperature. As-evaporated SnBi layer was composed of double layers of Bi and Sn due to the large difference in vapor pressures of Bi and Sn. With keeping the as-evaporated SnBi layer at $150^{\circ}C$ for more than 15 sec, SnBi alloy composed of eutectic phase and Bi-rich $\beta$ phase was formed by interdiffusion of Sn and Bi. Debonding between top Si wafer and Ni cap structures was accomplished by melting of the SnBi layer at $150^{\circ}C$.

• Journal of the Korean Society for Nondestructive Testing
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• v.29 no.1
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• pp.27-35
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• 2009

In this paper, we study the classification of steam generator tube defects using an improved feature extraction. We consider 4 axisymmetric defect patterns of tube: I-In type, I-Out type, V-In type, and V-Out type. Through numerical analysis program based on finite element modeling, 400 ECT signals are generated by varying width and depth of each defect type. From those generated ECT signals, we propose new feature vectors that include an angle between the two points where the Maximum impedance and half the Maximum impedance, and angles between Maximum impedance point and 10%, 20%, 30%, 40% of Maximum impedance points. Also, multi-layer perceptron with one hidden layer is used to classify the defect patterns. Through the computer simulation study, it is shown that the proposed method achieves an improved defect classification performance in terms of Maximum Error and mean square Error.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 1990.10a
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• pp.173-178
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• 1990

로터-베어링축계는 증기및 가스터빈, 터보 발전기, 압축기등 거의 모든 산업 기계류에서 동력 전달의 기본 도구로써 사용되고 있다. 즉 회전에 의한 동력 의전달은 비교적 간단히 대용량의 동력을 효율적으로 전달할 수 있다. 이에 따라 회전기계류에 대한 연구는 산업 혁명 이후 꾸준히 발전되어 온바, 특히 근래에 들어와 산업기계류의 경쟁이 치열하여짐에 따라 산업기계류의 고정 밀화, 고속화, 고신뢰화 요구가 증대하고 있는 현실을 비추어 볼때, 산업 기 계류의 근간을 이루고 있는 로터-베어링 축계의 안정성을 포함한 진동에 관 한 문제는 회전기계류 설계의 주요 기술로써 연구.개발의 필요성이 매우 높 다 하겠다. 회전축계 진동 관련 연구는 두 분야로 대별될 수 있는데 언밸런 스(Unbalance)에 의한 Synchronous진동과 여러가지 원인에 의해 계의 불안 정성을 유발시키는 Nonsynchronous진동으로 나눌 수 있다. 본 연구에서는 이들 연구의 기본이 되는 회전축-베어링계 동특성 해석 프로그램을 개발하 였다. 여러가지 방법이 있으나 여기서는 Holzer가 비틀림 진동에 적용하고, Mykiestad(2)와 Prohl(3)에 의하여 회전축의 횡 진동에 적용된 이후 Lund(4) 등에 의하여 베어링의 영향등이 첨가된 전달 매트릭스 (Transfer Matrix) 방 법을 이용하여 임계속도(Critical Speed), 모우드 형태(Mode shapes)를 예측 하고 불안정 판정(Instability Criteria)등을 할 수 있는 프로그램을 개발하였 다. 특히 Murphy(1)의 다항식 방법(Polynomial Method)에 기본을 두어 기존 의 전달 매트릭스가 가지고 있던 반복, 수렴 시간 문제와 빠뜨리는 임계속도 예측에 대한 개선을 이루었으며 기존 논문과 실험 결과와의 비교 검토를 통 하여 개발된 프로그램의 신뢰성을 검토하였다. 특히, 각종 회전 기계의 소형 화, 경량화 추세에 따라 지반이나 케이싱이 경량이거나 유연하여 회전축과 동적으로 연성된 경우 회전축-베어링-지반으로 이루어진 2중구조의 회전축 계 동특성을 해석할 수 있는 프로그램을 개발하므로서 회전 기계류의 진동 전반에 걸친 문제점에 대한 그 원인과 현상을 명확히 분석하여 국내의 전기 계류의 보다 신뢰성있는 설계 및 제작자료를 확보하는데 기여할 수 있게 하 였다.

• Korean journal of food and cookery science
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• v.30 no.2
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• pp.183-192
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• 2014

This study was conducted to investigate the effect of superheated steam (SHS) on the improvement of quality during the manufacturing process of Samgyetang products. SHS cooking showed the increase in moisture content and the decrease in protein. In terms of chromaticity, the value of L was significantly higher in the $2^{nd}$ SHS cooking compared to conventional cooking. As for texture, the hardness decreased in Samgyetang with SHS cooking than conventional cooking. According to the results of the safety experiment with a 14-day refrigerations storage the total number of bacteria was lower in the SHS cooking compared to conventional cooking. The TBA value increased to 0.59-5.70 mg MD/kg after 15 days; VBN values were also 0.70-4.54 mg% in SHS cooking indicating a slight decomposition. Overall, it was found that SHS cooking and HHP were more preferred and also had an effect of reducing microorganisms, which were improvements in product quality and sanitation.

• Journal of Korean society of Dental Hygiene
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• v.15 no.4
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• pp.713-718
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• 2015

Objectives: The purpose of the study was to investigate the bacterial morphology attached on ultrasonic scaler tips using no cleansing solution, alcohol cotton, liquid chemical disinfecting agent, and autoclave method. Methods: Scaling tip was applied to the mouth and the ultrasonic scaler tips were assigned to four groups. Group 1 was control group with no cleansing solution. Group 2 was treated with alcohol cotton. Group 3 was treated with 2% green Y-Na solution in liquid chemical disinfecting agent, and Group 4 was sterilized by autoclave method. Live bacteria were observed by phase contrast microscopy. The scanning electron microscopy(SEM) revealed the morphological characteristics of scaler surface. The type of attached bacteria were analyzed using SPSS 21.0 program. The data were analyzed by one-way analysis of variance(ANOVA) and Tukey's post-hoc test. Results: The types of sterilization methods had influences on the bacterial viability. The numbers of cocci, bacilli, spiral form bacteria, and filamentous bacteria was observed in $89.00{\pm}3.60%$, $29.67{\pm}3.51%$, $3.33{\pm}0.57%$ and $1.67{\pm}0.57%$ in control group, $31.67{\pm}3.51%$, $63.33{\pm}4.04%$, $2.00{\pm}1.00%$ and $1.67{\pm}0.57%$ in alcohol cotton group, $69.67{\pm}4.50%$, $12.33{\pm}2.51%$, 0% and 0% in liquid chemical disinfecting agent group, and 0.0%, 0.0%, 0.0% and 0.0% in autoclave method group. The clean surface of ultrasonic scaler tip was shown on SEM by autoclave method. Conclusions: The most effective sterilization method of ultrasonic scaler tip was the autoclave method. Autoclave method is the most effective sterilization method and can reduce the cross-infection in the dental clinic.

• Journal of Korean Society of Occupational and Environmental Hygiene
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• v.1 no.2
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• pp.136-143
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• 1991

Inorganic mercury in urine and airborne was determined by cold vapor atomic absorption spectrophotometry. Detailed sampling methods and analylical results are as follows : 1. 100~200ml of urine for each person was taken in 250 ml borosilicate bottle and $K_2S_2O_8$ (0.1g/100ml urine) was added to prevent bacterial contamination. About 1001 air of workingplace was absorbed in l0ml of absorbing solution. Urine samples and absorbing solution tubes were stored at $4^{\circ}C$. Dillution solution to prepare standard solution used deionized water (D.W) for urine and absorbing solution (A.S) for air. 2. 1n this procedure deteclion limit was 1ng/ml and mercury contents of blank reagent solution was 1~2ng/ml. 3. Calibration range was $0.02{\sim}0.1{\mu}g/ml$ and in this range r.s.d for each calibration curve in D.W and A.S and ${\pm}7.9%$ and ${\pm}3.7%$, respectively. 4. Repeatability (n=5 times, conc. $0.05{\mu}g/ml$) was ${\pm}5.8%$, in D.W. and ${\pm}4.4%$ in A.S, respectively. 5. Recovery for urine adding spiked concentration ($0.05{\mu}g/ml$) was about 90%. 6. Analytical result of samples was $1{\sim}139{\mu}g/l$ in urine and ${\sim}0.127mg/m^3$ in airborne.