• Title/Summary/Keyword: 접착레진

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Statistical Verification of Acoustic Emissions Detected during Polymerization Shrinkage of Resin Restoration in Dental Ring (치아/복합레진 수복부의 중합 수축시 검출된 음향방출의 통계적 검증)

  • Gu, Ja-Uk;Choi, Nak-Sam;Arakawa, Kazuo
    • Composites Research
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    • v.23 no.6
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    • pp.39-46
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    • 2010
  • Acoustic emission (AE) signals are detected during the polymerization shrinkage of composite resin restoration in artificial dental ring according to various interfacial treatment conditions. AE amplitudes and the number of AE hit events were compared through the non-parametric statistics of Mann-Whitney method and Kruskal-Wallis method. The AE amplitudes detected from the PMMA and human tooth ring specimens were not significantly different according to adhesive conditions. The stainless steel ring specimen, meanwhile, had a difference in AE amplitude (p<0.05). The quantity of hit events for the human molar dentin specimens of the good bonding state was much less than that for the steel ring specimen but more than that for the PMMA ring specimen. For the same substrate, the better the bonding state, the less the AE hit events (p<0.05). The degree of marginal disintegration measured by SEM was proportional to the amount of AE hit events detected.

The effect of surface treatment conditioning on shear bond strength between zirconia and dental resin cements (지르코니아 세라믹의 표면처리에 따른 치과용 접착제의 전단결합강도)

  • Kim, Ji-Hye;Seo, Jae-Min;Ahn, Seung-Geun;Park, Ju-Mi;Song, Kwang-Yeob
    • The Journal of Korean Academy of Prosthodontics
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    • v.51 no.2
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    • pp.73-81
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    • 2013
  • Purpose: The purpose of this study was to evaluate the effect of surface treatment on the shear bond strength of zirconia ceramic to 3 resin cements. Materials and methods: A total of 143 disk-shaped Zirconia blocks (HASS Co., Gangneung, Korea) were randomly divided into three treatment groups: (1) only 50 ${\mu}m$ $Al_2O_3$ sandblasting, (2) 50 ${\mu}m$ $Al_2O_3$ sandblast and zircona liner, (3) 50 ${\mu}m$ $Al_2O_3$ sandblasting and Rocatec (3M ESPE, Seefeld, Germany). Bistite II (Tokuyama Dental Co., Japan), Panavia F (Kuraray Medical, Japan), and Superbond C&B (Sun Medical, Japan) were used to cement onto the zirconia. After 24h of storage in distilled water, shear bond strength was evaluated. High value group was re-tested after thermocycling at 5,000 cycles(5-$55^{\circ}C$). Shear bond strength data were analyzed with one-way ANOVA, two-way ANOVA test and Post Hoc Test (${\alpha}$=.05). Shear bond strength data before and after thermocycling were analyzed with Independent sample T test (${\alpha}$=.05). Results: Super-bond C&B treated with Rocatec showed the most high shear bond strength. Super-bond C&B groups resulted in significantly higher than other cement groups (P<.05). Rocatec groups resulted in significantly higher than other surface treatment groups (P<.05). Shear bond strength has increased in Panavia F treated with Zirconia liner (P<.05). After thermocycling, shear bond strength was increased in Super-bond C&B treated with Rocatec but decreased in other groups (P<.05). Conclusion: Super-bond C&B cement resulted the highest shear bond strength and Rocatec system enhanced the shear bond strength. After thermocycling, shear bond strength has decreased in most resin cements except Super-bond C&B treated with Rocatec.

THE EFFECTS OF CRYSTAL GROWTH ON SHEAR BOND STRENGTH OF ORTHODONTIC BRACKET ADHESIVES TO ENAMEL SURFACE (Crystal growth에 의한 법랑질 표면처리가 교정용 브라켓 접착제의 전단결합강도에 미치는 영향)

  • Lee, Young-Jun;Park, Young-Guk
    • The korean journal of orthodontics
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    • v.27 no.5 s.64
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    • pp.839-852
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    • 1997
  • It has been submitted that different ion solutions containing sulfate induce crystal growth and might substitute conventional acid etching for pretreatment of enamel in orthodontic bonding(${\AA}rtun$ et al., Am. J. Orthod. 85, 333, 1984). This investigation was designed to evaluate the relevance of crystal growth on the enamel surface as an alternative to conventional acid etching in direct bonding of orthodontic brackets. Annexing Li2SO4, MgSO4, K2SO4 respectively in the solution with $25\%$ polyacrylic md 0.3M sulfuric acids were employed to enhance the crystal growth. Human bicuspids were treated with various parameters as combinations of crystal growth and glass ionomer cement, crystal growth and orthodontic resin, acid etching and orthodontic resin for an investigative purpose. Crystal growth solution containing MgSO4 showed the highest shear bond strength(15.6MPa) within the groups of bonding brackets with glass ionomer cement(p<0.01). Bonding with glass ionomer cement on the surface of crystal growth demonstrated higher shear bond strength than with orthodontic resin(p<0.001). Bonding with glass ionomer cement on the surface treated with crystal growth solution containing MgSO4 or K2SO4 was not different shear bond strength statistically from bonding with orthodontic resin on the acid-etched surface. It suggests that bonding brackets with glass ionomer cement on the surface treated with crystal growth solution containing MgSO4 or K2SO4 is a potential alternative to bonding with resin on the acid etched sufrace.

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Evaluation of mechanical properties of several dual-cure resin cements by curing modes (중합방법에 따른 여러 이중중합 레진 시멘트의 기계적 성질 평가)

  • Kim, Soo-Yeon;Park, Se-Hee;Kim, Jin-Woo;Cho, Kyung-Mo
    • Journal of Dental Rehabilitation and Applied Science
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    • v.31 no.1
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    • pp.1-9
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    • 2015
  • Purpose: The purpose of this study was to evaluate the mechanical properties of several dual-cure cements by different curing modes. Materials and Methods: One resin-modified glass ionomer cement (FujiCEM 2), two conventional dual-cure resin cements (RelyX ARC, Multilink N), and two dual-cure self-adhesive resin cements (RelyX U200, G-CEM LinkAce) were used. To evaluate the influence of the curing methods, each cements divided into four conditions (n = 20); Condition 1: self-curing for 10 minutes, Condition 2: immediate after 20 seconds light-curing, Condition 3: 24 hours after self-curing, Condition 4: 24 hours after light-curing. The compressive strength and diametral tensile strength were measured with a universal testing machine. All data were statistically analyzed using t-test, one-way ANOVA and Scheffe's test. Results: The results showed the compressive strength and diametral tensile strength after 24 hours in all curing modes were higher than immediate except RelyX ARC light-cured and Multilink N light-cured. The FujiCEM 2 showed lowest values (P < 0.05). Conclusion: The outcome was cement-depend, but there is no significant difference about compressive strength and diametral tensile strength between dual-cure self-adhesive resin cements and conventional resin cements. And this result will be used as a base line data selecting resin cement for favorable long-term prognosis.

A comparison study of the effects of handpiece speed on teeth in debonding procedure (탈접착 후처치시 핸드피스(handpiece) 속도가 치아에 미치는 영향에 대한 비교 연구)

  • Park, Soo-Byung;Kim, Gu-Ho;Ha, Man-Hee
    • The korean journal of orthodontics
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    • v.34 no.1 s.102
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    • pp.83-91
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    • 2004
  • This study was performed to examine treatment efficiency and patient discomfort rate according to used handpiece speed in clean-up technique. Brackets were bonded to extracted human premolar(50 teeth). After debonding, 50 extracted human premolar were divided Into each two groups(low speed handpiece group with tungsten carbide bur and high speed handpiece group with ultra-fine diamond finishing bur) of 25 according to used handpiece speed in clean-up technique. In clean-up procedure, teeth vibration and pulp thermal changes were measured. After clean-up procedure, the enamel surfaces of randomly selected 10 teeth from each two groups were taken by SEM and evaluated. The findings of this study were as follows ; 1. During resin removal, tooth vibrations of various amplitude in low speed handpiece group were more than those of high speed handpiece. 2. The pulpal thermal changes of high speed handpiece group were significantly higher than those of low speed handpiece group, also the resin removal time in high speed handpiece group was almost as twice as in low speed handpiece group. 3. The figures of SEM to enamel surfaces after resin removal showed that notches and resin remnants in high speed handpiece group were more than those in low speed handpiece group.