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한지의 처리공정에 따른 섬유와 한지의 물성 비교

  • Choi, Chan-Ho;Seo, Yeong-Beom;Jeon, Yang
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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    • 2001.04a
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    • pp.193-197
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    • 2001
  • 본 연구에서는 국산닥, 태국닥, 중국닥의 원료를 사용하여 펄핑, 표백, 고해, 초지, 건조의 방식을 변화시켜 총 3500 여장에 이르는 한지를 한지제조 전문가가 일정한 방법에 따라 제 조하였고 그 특정들을 조직적으로 검토하였다. 이러한 연구는 한지의 물성이 닥섬유의 처 리공정에 의해 어떻게 영향을 받는지 연구를 통계적으로 가능하게 하였다. 본 연구에서는 육재펄핑과 일광표백의 효과, 외발뜨기와 쌍발뜨기의 효과, 고해방식의 차이, 먹퍼집성에 대 해 결과들을 보이 고 있다. 육재 펄핑과 일광표백이 한지의 물성에 어떠한 영향을 미치는지 알아보기로 하였다. 현 재는 많은 한지 업자들이 육재펄핑보다는 가성소다 펄핑 (그림에서는 약품펄핑으로 표기), 일광표백보다는 차아염소산 나트륨 (그림에서는 약품표백으로 표기)을 사용하는 것이 보통 이다. 육재펄핑과 일광표백을 실시한 한지는 열단장, 인열강도, 내절도를 약품펄핑이나 약 품표백보다 높이는 효과가 있음을 알 수 있었다. 하지만 약품을 사용하는 경우 리그닌의 용출이 더 수윌하므로 백색도는 약품을 사용하는 경우가 더 유리하였다. 국산닥의 경우 육 재펄핑과 일광표백을 한 경우 먹퍼짐성이 약품사용 한지보다 크지 않음을 볼 수 있었다. 한국의 전통적인 외발뜨기 초지방식은 일본의 쌍발뜨기 방식에 비해 많은 물리적 우수성 을 보이고 있다. 외발뜨기가 쌍발뜨기에 비해 열단장, 신장율, 인열지수 및 내절도 모두가 우수함을 잘 보이고 있다. 섬유의 성질과 관련하여 전체적으로 조명해 보면, 열단장, 인열 지수는 국산닥이 가장 높으며, 내절도는 태국닥이 우수하였고, 중국닥의 경우 모두 매우 불 량함을 알 수 있다. 이것은 아마도 처리중에 과도한 표백을 실시하지 아니하였는가 하는 의구심을 들게한다. 열단장과 신장율 역시 국산닥이 우수하였다. 글씨를 쓸 때, 붓이 나가 는 정도를 마찰게수로 짐작해 보았다. 동 마찰계수와 정 마찰계수는 국산닥이 낮은 편이였 다. 마찰계수가 낮다는 사실은 한지의 표면이 더 매끄럽다고 표현될 수 있는데, 역시 국산닥 으로 제조한 한지가 붓이 나가는데 유리하지 않을까 하는 추측을 할 수 있다. 본 실험결과 는 한지 사용자들의 느낌과 상관관계를 얻어내어서 확인해야 할 것이다. 닥방망이로의 고해나 칼비터에 의한 고해나 큰 물성적으로 큰 차이를 보이지는 않고 있 었다. 단지 섬유의 차이가 고해방식의 차이보다 월등히 크다는 사실을 보이고 있다 이러한 점은 섬유장의 길이에서도 볼 수 있다. 칼비터가 섬유를 절단하기만 하고 닥방망이 고해가 섬유장의 변화를 일으키지 않는다면 틀림없이 평균 섬유장의 차이가 생길것이다.

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FRACTURE STRENGTH OF THE IPS EMPRESS CROWN : THE EFFECTS OF INCISAL REDUCTION AND AXIAL INCLINATION ON UPPER CANINE (IPS Empress 도재관의 파절강도 : 상악 견치에서 절단연 삭제량과 축면 경사도에 따른 영향)

  • Shin Dong-Kuk;Kang Han-Joong;Park Yong-Suck;Park Kwang-Soo;Dong Jin-Keun
    • The Journal of Korean Academy of Prosthodontics
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    • v.43 no.1
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    • pp.30-40
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    • 2005
  • Purpose. The purpose of this study was to compare the fracture strength of the IPS Empress ceramic crown according to the incisal reduction (2.0mm, 2.5mm, 3.0mm) and axial inclination ($4^{\circ}$, $8^{\circ}$, $12^{\circ}$) of the upper canine. Material and methods. After 10 metal dies were made for each group, the IPS Empress ceramic crowns were fabricated and each crown was cemented on each metal die with resin cement. The cemented crowns mounted on the testing jig were inclined 30 degrees and the universal testing machine was used to measure the fracture strength. Results. 1. The fracture strength of the ceramic crown with 3.0mm depth and $12^{\circ}$ inclination was the highest (839N) Crowns of 2.0mm depth and $12^{\circ}$ inclination had the lowest strength (559N). 2. There was no significant difference in the fracture strength by axial inclination in the same incisal reduction group. 3. The fracture mode of the crowns was similar. Most of fracture lines began at the loading area and extended through proximal surface perpendicular to the margin irrespective of incisal reduction.

An Image Watermarking Method for Embedding Copyrighter's Audio Signal (저작권자의 음성 삽입을 위한 영상 워터마킹 방법)

  • Choi Jae-Seung;Kim Chung-Hwa;Koh Sung-Shik
    • The Journal of the Acoustical Society of Korea
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    • v.24 no.4
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    • pp.202-209
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    • 2005
  • The rapid development of digital media and communication network urgently brings about the need of data certification technology to protect IPR (Intellectual property right). This paper proposed a new watermarking method for embedding owner's audio signal. Because this method uses an audio signal as a watermark to be embedded, it is very useful to claim the ownership aurally. And it has the advantage of restoring audio signal modified and especially removed by image removing attacks by applying our LBX(Linear Bit-expansion) interleaving. Three basic stages of our watermarking include: 1) Encode . analogue owner's audio signal by PCM and create new digital audio watermark, 2) Interleave an audio watermark by our LBX; and 3) Embed the interleaved audio watermark in the low frequency band on DTn (Discrete Haar Wavelet Transform) of image. The experimental results prove that this method is resistant to lossy JPEG compression as standard image compression and especially to cropping and rotation which remove a part of Image.

CLEANLINESS AND WALL MOPHOLOGY OF ULTRASONIC ROOT-END RETROGRADE CAVITY (초음파로 형성된 치근단 역충전와동의 정화도 및 와벽형태)

  • Kim, Sung-Kyo;Lee, Jae-Whan;Baek, Seung-Moo
    • Restorative Dentistry and Endodontics
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    • v.22 no.2
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    • pp.536-545
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    • 1997
  • The purposes of this study were to evaluate the degree of cavity cleanliness and to observe cavity wall morphology when root-end retrograde cavity preparation was done with ultrasonics. Root resections were done on 20 extracted human maxillary central incisors after canal filling with gutta-percha, and retrocavities were prepared using a slow-speed round bur as a control, and stainless steel ultrasonic tips of power settings of 2 and 6 ($Miniendo^{TM}$, EIE, SA, USA) as experimentals. The degree of the remaining cavity debris and smear layer, and wall morphology were evaluated under the scanning electron microscope. The results were as follows : Cavity prepared with ultrasonics of either power setting showed significantly less smear layer than did slow-speed preparations (p<0.01). However, there was no significant difference in canal debris (p<0.05). Cavity prepared with ultrasonics showed hatcheted appearance of wall, while slow-speed preparation showed relatively plain one.

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The Improvement of Wet Strength Properties of Sheet by N-Chlorocarbamoylethylation (N-chlorocarbamoylethyl화에 의한 sheet의 습윤강도 향상효과)

  • Jeong, Myung-Joon;Jo, Byoung-Muk;Oh, Jung-Soo
    • Journal of the Korean Wood Science and Technology
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    • v.27 no.3
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    • pp.63-72
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    • 1999
  • For the purpose of improving the wet strength properties of paper, cellulosic fibers were modified by the processes of carbarmoylethylation and N-chlorocarbamoylethylation. Carbamoylethylated cellulose was prepared by the reaction of acrylamide with cellulosic fibers under the alkali catalyst, and N-chlorocarbamoylethylated cellulose was prepared by the addition of sodium hypochlorite into the carbamoylethylated cellulose. In carbamoylethylation reaction, the conditions of NaOH concentration, temperature and acrylamide addition rate were considered to be important factors. An initial reactivity and degree of substitution(DS) in carbamoylethylation of cellulosic fibers were effective according to increasing the addition rates of alkali, acrylamide and the temperature condition of $40^{\circ}C$. The effective wet strength properties by N-chlorocarbamoylethylation of cellulosic fibers were indicated under the conditions of DS 0.06. The wet strength of sheet was improved to 85% at the 100% basis of dry strength. From the photograph of scanning electron microscopy, fiber cuttings on the edge of sheet sample used in tensile strength testing were found in the N-chlorocarbamoylethylated sheet, due to the improvement of fiber bonding strength. The hypochlorite treatment was effective in the recycling of N-chlorocarbamoylethylated sheet, and was reduced the wet strength of sheet to be able to reslush.

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Effect of Mechanical Peeling Time on Yield and Quality of Paeonia lactiflora Pallas Root (작약근(芍藥根)의 기계박피(機械剝皮) 시간(時間)에 따른 품질(品質) 차이(差異))

  • Kim, Ki-Jae;Park, Chun-Hong;Shin, Jong-Hee;Kim, Se-Jong;Park, So-Deuk;Choe, Boo-Sull
    • Korean Journal of Medicinal Crop Science
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    • v.7 no.1
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    • pp.27-30
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    • 1999
  • This experiment was carried out to determine the adequate machine peeling and retting time of peony roots, which are used as medicinal resources in Korea. When the roots were peeled for $10{\sim}30$ minitues in the peeling machine, the epidermis of root was removed, and higher yield was obtained and paeoniflorin content as compared with roots which were peeled for longer time. The paeoniflorin content of root varied with the different parts of root. The highest content was recorded in the upper part and the lowest in the middle part. The loss of paeoniflorin increased in the roots processed for expanded peeling and retting time. Lightness of peeled root was higher and ${\Delta}\;E$ was lower in the roots which were peeled by machine for longer time.

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The effect of cavity configuration on the mechanical properties of resin composites (중합환경에 따른 복합레진의 물리적 성질에 관한 연구)

  • Ryu, Gil-Joo;Park, Sang-Jin;Choi, Kyoung-Kyu
    • Restorative Dentistry and Endodontics
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    • v.27 no.3
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    • pp.239-248
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    • 2002
  • 이 연구의 목적은 와동의 형태가 굴곡강도와 탄성계수 등 복합레진의 물리적 성질에 미치는 영향을 평가하는 것이다. 복합레진은 Clearfil$^{TM}$ AP-X(Kuraray, Japan)와 Esthet-X$^{TM}$(Dentsply, USA)가 이용되었으며, 상아질 접착제는 Clearfil$^{TM}$ SE Bond(Kuraray, Japan)와 Prime & Bond NT$^{TM}$(Dentsply, USA)를 사용하였다. 대조군의 시편은 split steel mold(25mm$\times$2mm$\times$2mm) 내에 상기 2종류의 복합레진을 충전하여 2개의 대조군 시편을 제작하였으며, 2.4 및 3.4의 C-factor를 부여하기 위한 유리 모형와동을 제작하고, 와동 내에 상기 2종류의 복합레진을 충전하기 전 유리와동의 내면은 sandblasting 처리하고 각각의 복합레진과 동일회사 제품의 상기 상아질 접착제로 처리한 후, 복합 레진을 각각 충전하여 4개의 실험군을 제작하였다. 제작된 실험군 시편은 저속 diamond saw로 충전된 복합레진 부위의 중심부를 통과하도록 절단하여 레진기둥(25mm$\times$2mm$\times$2mm)이 되도록 제작하였다. 제작된 시편을 37$^{\circ}C$의 증류수에 24시간 동안 보관 후, 만능시험기(EZ Test, Shimadzu, Japan)를 이용하여 분당 1mm의 crosshead speed로 3점 굴곡강도를 측정하였다. 또 Linometer(R&B, Korea)를 이용하여 복합레진의 중합수축량을 측정하였으며 굴곡강도측정 후 시편의 파단면은 주사전자현미경(S-2300, Hitachi, Japan)을 이용하여 관찰하였다. 실험결과의 통계분석은 95% 수준의 one-way ANOVA/Tukey's test를 이용하여 결과를 얻었다. 실험에 이용된 2종류 복합레진의 굴곡강도와 탄성계수는 C-factor치 증가에 따라 감소하였으며, 파단면 또한 C-factor의 증가에 따라 더 불규칙해지는 양상을 나타내었다. 본 실험의 결과 hybrid형 복합레진이 micro-hybrid형 복합레진에 비해 C-factor의 영향을 더 많이 받는 것으로 나타났으며, 와동의 C-factor증가가 굴곡강도나 탄성계수와 같은 복합레진의 물리적 성질을 저하시킨다는 것을 의미하였다.

3D Mesh Watermarking Using Projection onto Convex Sets (볼록 집합 투영 기법을 이용한 3D 메쉬 워터마킹)

  • Lee Suk-Hwan;Kwon Seong-Geun;Kwon Ki-Ryong
    • Journal of the Institute of Electronics Engineers of Korea CI
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    • v.43 no.2 s.308
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    • pp.81-92
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    • 2006
  • This paper proposes a robustness watermarking for 3D mesh model based on projection onto convex sets (POCS). After designing the convex sets for robustness and invisibility among some requirements for watermarking system, a 3D-mesh model is projected alternatively onto two constraints convex sets until the convergence condition is satisfied. The robustness convex set are designed for embedding the watermark into the distance distribution of the vertices to robust against the attacks, such as mesh simplification, cropping, rotation, translation, scaling, and vertex randomization. The invisibility convex set are designed for the embedded watermark to be invisible. The decision values and index that the watermark was embedded with are used to extract the watermark without the original model. Experimental results verify that the watermarked mesh model has invisibility and robustness against the attacks, such as translation, scaling, mesh simplification, cropping, and vertex randomization.

Evaluation of the Lip during Smile in Normal Occlusion Adults (정상교합자의 미소시 구순 형태에 관한 연구)

  • Chi, Kuk-Sop;Kim, Kwang-Won
    • The korean journal of orthodontics
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    • v.26 no.2 s.55
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    • pp.197-204
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    • 1996
  • This study was performed to mark the criteria of the eathetic smile that was necessary to improve the esthetic problem in oral maxillo-facial region. The facial straight photographs of 62 adults(30 males, 32 females : 19-24 years old) in resting position and during smile were taken. The measurements and proportion of lip-teeth relationship during smile were statistically analyzed with photogrammetry. The following results wow obtained : 1. In the evaluation of the change of lips, smile line ratio was 0.93, buccal corridor ratio was 0.63, and smile symmetry ratio was 0.96. 2. The width of mouth during smile was 1.31 times of the width inthe resting position and 0.48 times of face width. 3. The upper lip height during smile was 0.69 times of the height in the resting position and the lower lip height during smile was 0.93 times of the height in the resting position. 4. The mean exposed lenght of upper central incisor was 9.96mm. Maxillary incisor exposure was significantly correlated with the upper lip change ratio, mouth width change ratio, and buccal corridor ratio.

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The Structural Characterization of Recombinant Bovine Somatotropin Expressed in Escherichia coli (재조합 소성장호르몬의 구조적 특성)

  • 김정호;김훈주박은숙김준
    • KSBB Journal
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    • v.9 no.2
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    • pp.165-173
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    • 1994
  • In this paper we have described the structural characterization of recombinant bovine somatotropin produced in Escherichia coli. Recombinant bovine somatotropin consists of 191 amino acid residues with a calculated molecular weight of 21,802 Da. For fragmentation of recombinant bovine somatotropin, we have used trypsin, Staphylococcus aureus V8 pretease, CNBr, and mild acid hydrolysis method. Digestion and cleavage with these proteases and chemicals yielded peptides of various size for amino acid sequence determination. The N-terminal sequence analysis was carried out up to thirty residues. Because the design of the recombinant bovine somatotropin gene for expression was such that the coding sequence begins with an initiation codon, AUG, before Ala, the first amino acid of bovine somatotropin, we could expect the initial amino acid as N-formyl Met. But the first amino acid of this protein, expressed in E. coli cells as inclusion bodies, was Ala. And the amino acid composition of RP-HPLC purified recombinant bovine somatotropin was determined and no essencial difference was observed. The amino acid sequence of the recombinant bovine somatotropin was identical to that predicted from its recombinant gene. There was no processing or replacement of amino acid residues in recombinant bovine somatotropin expressed in E. coli. The hydropathy plot of recombinant bovine somatotropin revealed a hydrophobic region at the NH2-terminus and hydrophilic region at the COOH-terminus. The E. coli expression system is thought to be valuable for the expression of recombinant bovine somatotropin because protein was processed to remove the N-terminal Met residue by methionyl-aminopeptidase autonomously.

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