• 제목/요약/키워드: 저항 분포도

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Synthesis of Nanoscale Sn-Pb Alloy Powders by Electrical Explosion of Wire (전기선폭발법을 이용한 Sn-Pb 나노분말의 합성)

  • ;;;;A. P. Ilyin;D. V. Tichonov
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2003.04a
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    • pp.35-35
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    • 2003
  • )를 금속와이어에 인가하면 저항발열에 의해 와이어가 미세한 입자나 금속증기상태로 폭발하는 현상을 이용한 것으로 기상합성법에 속한다고 할 수 있다. 선폭법은 다른 제조법에 비해 공정이 간단하여 생산비용이 저렴하며, 원재료의 조성을 갖는 분말의 합성과 금속간화합물, 융점차이가 나는 재료의 합금화 등이 가능하다. 인가에너지의 크기와 폭발 시 분위기를 제어함으로써 분말의 평균크기와 분포 제어 또한 가능하다. 본 연구는 러시아의 우수한 기초기술을 바탕으로 Pb-Sn계 합금은 전기폭발법으로 극미세분말을 제조하였으며, 분말의 형상, 상 화학조성의 변화를 조사하였다. 본 실험에 사용된 Sn-Pb계(All-Union State Standard 1499-70, 0.53mm)합금와이어는 자동시스템(1-0.6Hz)에 의해 챔버안으로 공급되었다. 이 때 임계폭발 와이어 길이는 50-80nm으로 실험을 행하였다. 챔버 압력은 1.4~2.0atm으로 유지하였다. 제조된 분말의 특성은 XRD, XRPES, SEM등을 이용하여 분말의 형상과 상, 화학조성, 표면분석을 행하였으며 DSC, TGA, BET분석을 통하여 온도변화에 따른 금속분말의 열량변화, 질량변화, 비표면적을 측정하였다. 제조된 Sn-Pb계 분말은 모두 평균 입도 117nm~220nm의 구형형상이었다. 이때 합금분말의 조성은 51.17~63.21 at%Sn, 35.47~46.37 at%Pb로 나타났다. 와이어에 인가되는 비에너지(W/Wc)가 감소된에 EK라 표면층의 Pb함량이 증가함을 보였다. 이는 와이어 내부 저항의 감소로 인한 공정시간의 지연과 Sn, Pb의 확산계수 차이에 의한 것으로 사료된다. 열분석 결과, Sn~Pb계 화합물의 융점은 167~$169^{\circ}C$로 관찰되었으며, $10^{\circ}C$/min로 $920^{\circ}C$까지 승은 하였을 때 17.1~18 wt%의 질량증가를 보였다.TEX>계 나노복합분말이 얻어짐을 알 수 있었다. 이 때 X션 회절피크의 line broadening으로부터 복합분말의 Fe 명균 결정립 크기는 24nm로 초미세 결정럽의 분말합금이었다. 포화자화값은 볼밀처리에 따라 점점 증가하여 MA 30시간에는 20.3emu/g로 포화됨을 알 수 있었다. 또한 보자력 Hc는 MA초기단계에 350e로 매우 낮으나 30시간 후에는 Hc값이 2600e로 매우 큰 값을 나타내었다. 이것은 환원반응결과 초기에 생성된 Fe의 결정립이 비교적 크고 결정결함이 적으나 볼밀처리를 30시간까지 행하면 Fe 결정렵의 미세화 빛 strain 증가로 magnetic hardening이 일어나기 때문인 것으로 사료된다.길이가 50, 30cm인 압출재를 제조하였다. 열간압출한 후의 미세조직을 광학현미경으로 압출방향에 평행한 방향과 수직방향으로 관찰하였고, 열간 압출재 이방성을 검토하기 위하여 X선 회절분석을 실실하여 결정방위를 확인하였다. 전기 비저항 및 Seebeck 계수 측정을 위하여 각각 2$\times$2$\times$10$mm^3$ 그리고 5$\times$5$\times$10TEX>$mm^3$ 크기의 시편을 준비하였다.준비하였다.전류를 구성하는 주요 입자의 에너지 영역(75~l13keV)에서 가장 높은(0.80) 상관계수를 기록했다. 넷째, 회복기 중에 일어나는 입자들의 유입은 자기폭풍의 지속시간을 연장시키는 경향을 보이며 큰 자기폭풍일수록 현저했다. 주상에서 관측된 이러한 특성은 서브스톰 확장기 활동이 자기폭풍의 발달과 밀접한 관계가 있음을 시사한다.se that were all low in two aspects, named "the Nonsignificant group". And the issues were high risk perception in general setting and lo

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Effect of Ground Boundary Condition on Evaluation of Blast Resistance Performance of Precast Arch Structures (지반경계조건이 프리캐스트 아치구조물의 폭발저항성능 평가에 미치는 영향)

  • Lee, Jungwhee;Choi, Keunki;Kim, Dongseok
    • Journal of the Computational Structural Engineering Institute of Korea
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    • v.32 no.5
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    • pp.287-296
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    • 2019
  • In this study, the effect of ground boundary conditions on the evaluation of blast resistance performance of precast arch structures was evaluated by a numerical analysis method. Two types of boundary conditions, namely, fixed boundary conditions and a perfectly matched layer (PML) were applied to numerical models. Blast loads that were much higher than the design load of the target structure were applied to compare the effects of the boundary conditions. The distribution and path of the ground explosion pressure, structural displacement, fracture of concrete, stress of concrete, and reinforcing bars were compared according to the ground boundary condition settings. As a result, the reflecting pressure shock wave at the ground boundaries could be effectively eliminated using PML elements; furthermore, the displacement of the foundation was reduced. However, no distinct difference could be observed in the overall structural behavior including the fracture and stress of the concrete and rebar. Therefore, when blast simulations are performed in the design of protective structures, it is rational to apply the fixed boundary condition on the ground boundaries as conservative design results can be achieved with relatively short computation times.

Colossal Magnetoresistance and Mossbauer Studies of La-Ca-Mn-O Compound Doped with $^{57}Fe$ ($^{57}Fe$를 미량 치환한 La-Ca-Mn-O의 초거대자기저항과 Mossbauer분광학연구)

  • 박승일;김성철
    • Journal of the Korean Magnetics Society
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    • v.8 no.6
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    • pp.335-340
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    • 1998
  • Colossal magnetoresistance $La_{0.67}Ca_{0.33}Mn_{0.99}^{57}Fe_{0.01}O_3$ material has been produced by a metal-salt routed sol-gel process method. Magnetic properties of $La_{0.67}Ca_{0.33}Mn_{0.99}^{57}Fe_{0.01}O_3$ have been studied with x-ray diffraction, Rutherford back-scattering spectroscopy(RBS), vibrating sample magnetometer, and Mossbauer spectroscopy. Crystalline $La_{0.67}Ca_{0.33}Mn_{0.99}^{57}Fe_{0.01}O_3$ was perovskite cubic structure with a lattice parameter $a_0=3.868$\AA$$. And there was no appreciable change in the value of the lattice parameter when a small amount (x=0.01) of iron was added. However, Mossbauer and VSM data indicate the Curie temperature of the $La_{0.67}Ca_{0.33}Mn_{0.99}^{57}Fe_{0.01}O_3$ decreased from 282 to 270 k and also the saturation magnetization from 84 to 81 emu/g at 77 K. Mossbauer spectra of $La_{0.67}Ca_{0.33}Mn_{0.99}^{57}Fe_{0.01}O_3$ have been taken at various temperatures ranging form 4.2 K to room temperature. Analysis of $^{57}Fe$ Mossbauer data in terms of the local configurations of Mn atoms has permitted the influence of the magnetic hyperfine interactions to be monitored. The isomer shifts show that the charge state of all Fe ions are ferric. The magnetoresistance of $La_{0.67}Ca_{0.33}Mn_{0.99}^{57}Fe_{0.01}O_3$ was about 33 % at semiconductor-metal transition temperature $T_{SC-M}=250K$.

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Temperature Compensation on the Cone Tip Resistance by Using FBG Temperature Transducer (FBG센서를 이용한 콘 선단저항력의 온도영향 보상)

  • Kim, Rae-Hyun;Lee, Jong-Sub;An, Shin-Whan;Lee, Woo-Jin
    • Journal of the Korean Geotechnical Society
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    • v.25 no.10
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    • pp.31-40
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    • 2009
  • As the measurement of strain-gage type cone penetrometer is influenced by the temperature change during penetration, the temperature is a factor producing an error of the cone tip resistance. In this study, the 0.5 mm diameter temperature transducer and 7 mm diameter micro cone penetrometer are manufactured by using FBG sensors to evaluate the effect of temperature on the cone tip resistance. Design concepts include the cone configuration, sensor installation and the temperature compensation process. The test shows that the tip resistance measured by strain gauge is affected by the temperature change. The error of the tip resistance increases with an increase in temperature change, while the temperature effect on the tip resistance of FBG cone is effectively compensated by using FBG temperature transducer. Temperature compensated tip resistance of the strain gauge cone shows the good matched profile with FBG cone which performs real-time temperature compensation during penetration. This study demonstrates that the temperature compensation by using FBG sensor is an effective method to produce the more reliable cone tip resistance.

Capacitively Loaded Loop Antenna Fed with Metamaterial Balun (Metamaterial 발룬으로 급전된 Capacitively Loaded 루프 안테나)

  • Jung, Youn-Kwon;Lee, Bom-Son
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.20 no.10
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    • pp.1084-1090
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    • 2009
  • This paper presents a balun consisting of a T-junction, a Right/Left Handed Transmission line(RLH-TL), and a conventional Right Handed(RH) line. It is assumed that the RLH-TL consists of N unit-cells. We provide closed-form solutions and design a very compact wideband(80 %) balun using CPW lines based on the obtained solutions. Then, we propose a capacitively loaded loop antenna designed for a uniform current distribution. The antenna resistance of the proposed antenna at resonance is about 204 ohms. The length of the unit cell is about $\lambda/12$(total length: $1\;\lambda$). The magnetic field generated from the proposed antenna is stronger than that of the conventional one by as much as 20 dB. We used a coplanar strip line(CPS) to combine the loop antenna and balun. The proposed antenna may be used as a near field UHF RFID reader antenna.

Characteristics of Neutral Point Loci on Line Voltages to Hull When Insulation Resistance Collapses by Earthing Faults at 3 Phase Power Distribution Systems Onboard Vessels (선박 3상배전선로의 지락고장에 따른 대지전압 중성점의 이동경로 특성)

  • Choi, Soon-Man
    • Journal of Advanced Marine Engineering and Technology
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    • v.35 no.8
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    • pp.1117-1123
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    • 2011
  • Ungrounded power systems are adopted onboard vessels which enable more stabilized power supply even in case of electric leakage to hull. If earthing faults happen at these systems, they make grounding impedances of power lines unbalanced each other on the three phases, resulting in high voltages to hull which can bring more possibilities of electric shocks and electric fires. This study focuses on how to configure a calculation module for transferring a grounded condition by lowered insulation resistance into a vector diagram of the voltages to hull. By using the module, the loci of neutral points were acquired to analyze how voltages to hull are affected by earthing faults and the distributed capacitances between power lines and hull. The suggested module was simulated and compared to the measured values from a test power system in good results.

Pathotypes of Xanthomonas campestris pv. oryzae in Honam District, Korea (호남지역에 분포하는 벼흰빛잎마름병균의 균형)

  • Lee D. K.;Seo J. H.;Choi J. E.;Park K. H.;Bae S. H.
    • Korean Journal Plant Pathology
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    • v.2 no.2
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    • pp.102-106
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    • 1986
  • The 719 isolates of Xanthomonas campestris pv. oryzae collected in Honam district during 1980-1984 were classified with new differential cultivars: 466($64-.8\%$) were pathotype K1, 116$(16.1\%)$ pathotype K2, 130$(18.1\%)$ pathotyps K3, and 7$(1.0\%)$ pathotype K4. No isolate for pathotype K5 was found. The isolates of pathotypes K1, K2 and K3 were distributed in the geographic regions, Haenam, Gwangyang, Gangjin, Wando, Igsan, and Buan. The isolates of all pathotypes were obtained from Milyang 23, Nagdong, and Dongjin which were susceptible to all the pathotypestested, while most of the isolates belonging to pathotype K3 and K4 were obtained from pungsan, Baegyang, Samgwang and Milyang 30.

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A Numerical Study on the Rock Fragmentation by TBM Cutter Penetration (TBM 커터 관입에 의한 암석 파쇄의 수치해석적 연구)

  • 백승한;문현구
    • Tunnel and Underground Space
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    • v.13 no.6
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    • pp.444-454
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    • 2003
  • Rock fragmentation technique by cutter penetration has widely been used in the mechanical tunnel excavation. Microcracks propagate and interact because of locally concentrated high stress induced by cutter penetration. which is caused by heterogeneity of rocks. In this study Weibull distribution function and degradation index are used to consider the strength heterogeneity of a rock and the degradation of rock properties after failure. Through the numerical analyses, it is shown that the lateral pressure has an important influence on the rock fragmentation. In the single cutter penetration, large chips are formed as lateral pressure increase. The cutter spacing is also an important factor that affects the rock fragmentation in the double cutter penetration. The fragmentation efficiency of the double cutter penetration is better when cutter spacing is 70 mm than 40 mm and 100 mm. From the results, it is expected that this study can be applied to a TBM tunnel design by understanding of chipping process and mechanism of rock due to cutter penetration.

Mathematical Model for the Removal of SO2 by the γ-Alumina Impregnated with CuO (γ-Alumina에 담지된 산화구리에 의한 SO2의 제거에 관한 수치모사)

  • Jeon, Bup Ju;Hong, In Kwon;Park, Kyung Ai;Jung, Il Hyun
    • Applied Chemistry for Engineering
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    • v.5 no.3
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    • pp.385-394
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    • 1994
  • Numerical solutions were obtained to the model equations for various of the parameters characterizing the pore structure, effective internal diffusion, and the chemical reaction constant. The conversion was decreased with the cause of pore closure at the surface of reacting particles, reduction of porosity, surface area of reaction and effective diffusion coefficient in the solid with the progress of reaction. Total conversion was strongly dependent on the local conversion at surface. According to the decreasing of impregnated concentration of the copper oxide and the increase of the flue gases concentration, total conversion was increased. The conversion was affected by gas flow rate and pore size distribution in the reacting solid.

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Occurrence and Distribution of Monosporascus Root Rot and Pathogenicity of Monosporascus cannonballus on Cucurbitaceae Plants (박과류 검은점뿌리썩음병의 발생분포 및 분리병원균의 병원성)

  • 허노열;류경열;현익화;권진혁
    • Research in Plant Disease
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    • v.7 no.1
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    • pp.11-15
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    • 2001
  • Root rot of Cucurbitaceae plants, caused by Monosporascus cannonballus, is one of the recently described diseases in Korea. The distribution and pathogenicity of M. cannonballus were examined by field and in vitro experiments. Root rot caused by M. cannonballus occurred on melon, oriental melon, watermelon and cucumber plants. In two years of disease survey, the disease occurred at 10 and 32 fields in 1997 and 1998, respectively, which were located at Kimhae, Chinju, and Namhae in Kyeongnam province, at Kwangyang in Chonnam province, at Kwangju city, and at Yeoju and Inchon in Kyeonggi province. The disease progress in a melon field at Namhae was not observed until the middle stage of plant growth, but rapidly increased at the fruit maturing stage, resulting in more than 50% yield loss. Isolation rate of M. cannonballus was 36.7% from wilted hosts. Fusarium oxysporum and Rhizoctonia solani were also frequently isolated. In vitro test, seedlings wilted after 7∼14 days of inoculation, and perithecia were formed in infected roots 21 days later. Two cucumber cultivars, Baekbong and Eunhwa, were resistant to the disease.

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