• Title/Summary/Keyword: 재료측정학

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Design of High-precision CTE measurement System for the Structural Materials in Space Applications (우주용 구조 재료의 초정밀 열팽창계수 측정시스템 설계)

  • Kim, Hong-Il;Han, Jae-Hung;Yang, Ho-Soon;Cho, Chang-Rae;Cho, Hyok-Jin;Kim, Hong-Bae
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.36 no.9
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    • pp.916-922
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    • 2008
  • Structures being used in space environment, should be designed to have minimum CTE(coefficient of thermal expansion) for the dimensional stability. Accurate CTE data of the materials are required to design the space structures consisting of various materials. There are uncertainties in the characteristics of materials even though the same manufacturing processes are applied. Therefore, it is needed to measure the thermal deformation of not only the material specimen but also substructures in simulated space environment, such as high vacuum condition. In this research, therefore, precise CTE measurement system using displacement measuring interferometer and vacuum chamber has been designed with uncertainty analysis of the measurements. This system can be used to measure the CTE of the specimen or thermal expansion of the substructure with varying size up to 50cm in length. To measure the low CTE material, overall uncertainty of this system is expected under 0.01ppm/K.

The electrical and rheological properties of zeolite based electrorheological (ER) Fluids (제올라이트 분말을 기본 재료로한 전기유변유체의 전기 및 유변학적 특성)

  • Jeong, Dong-Un;Choe, Yun-Dae;Kim, Sang-Guk
    • Korean Journal of Materials Research
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    • v.4 no.2
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    • pp.213-218
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    • 1994
  • 제올라이트 분말을 기본재료로 하는 전기유변유체의 전기 및 유변학적 특성이 연구되었다. 전기장 인가시 높은 한계응력을 얻기 위하여 비교적 유전상슈가 큰 5종류의 유전유체를 선택하여 제올라이트 분말과 혼합하여 전기유변유체를 준비하였다. Couette형 rheometer를 이용하여 유변유체의 한계응력을 인가된 전기장 및 온도의 함수로서 측정하였다. 이중 chlorinate hydrocabon oil과 제올라이트 분말을 혼합한 전기유변유체의 한계응력은 6KPa(E=4KV/mm, T=$25^{\circ}C$)로서 최대치를 기록하였다. 측정된 한계응력은 온도가 상승하면 점차 감소하는 반면 전류밀도는 온도에 따라 증가하였다. 전류밀도에 대한 Arrhenius 그라프에서 전기전도에 대한 활성화 에너지는 약 0.7eV였으며 이는 제올라이트 분말에 포함된 $Na^{+}$ 이온의 확산에 기인하는 것으로 분석되었다.

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A Fundamental Research on Determining Segregation Boundary using Rheological Parameters for 21 and 24MPa grade of Normal Strength Concrete (레올로지 정수를 이용하여 21, 24MPa급 일반강도 콘크리트의 재료분리 경계를 판단하기 위한 기초연구)

  • Lee, You-Jung;Lee, Young-Jun;Han, Dongyeop
    • Journal of the Korea Institute of Building Construction
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    • v.20 no.5
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    • pp.399-407
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    • 2020
  • The aim of the research is to provide the boundary conditions for segregation of normal strength grade and high fluidity concrete mixture (so called mid-fluidity concrete) with rheology parameters. Since the normal strength grade concrete mixture has a relatively high water-to-cement ratio and no SCMs, it is easy to be segregated when superplasticizer is added. Hence, to achieve the mid-fluidity concrete of normal strength grade and high fluidity, preventing segregation of the mixture is inevitable. In this research, using two superplasticizers with different solid concentrations, the flow behaviors and rheological behaviors were assessed by increasing fluidity until the segregation happened. According to the experiment in this research, an unusual behavior in rheology parameters was observed when the concrete mixture started to be segregated. From this results and report, it is expected to contribute on the definition of segregation with rheological test methods.

Heat-treatment Effects of CdS Thin Films Fabricated by Thermal Evaporation Method (진공증착법으로 제작한 CdS 박막의 열처리효과)

  • Park, Tae-Seong;Jin, Gyo-Won;Kim, Yeong-Ho;Han, Eun-Ju;Kim, Geun-Muk
    • Korean Journal of Materials Research
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    • v.7 no.11
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    • pp.981-985
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    • 1997
  • 열증착법에 의해서 온도 85$^{\circ}C$인 glass기판 위에 CdS 박막을 제작하였다. 두께가 200nm정도로 측정된 CdS박막은 공기 중에서 온도 25$0^{\circ}C$-55$0^{\circ}C$범위에서 각각 30분간 열처리 되었으며 이들 시료에 대하여 4-point probe, XRD, SEM, UV-Spectrophotometer 및 광발광 측정으로 전기적 광학적 특성을 조사하였다. 이들의 일련의 실험값은 열처리 온도 37$0^{\circ}C$ 근처에서 구조의 변화를 보여주었는데, 열처리 온도에 대한 비저항아니 XRD, SEM 의 측정은 cubic로부터 hexagonal구조로의 변환을 나타내었다. 특히 상온에서 측정한 광발광에서 green edge emission(GEE)피이크가 2.42eV를 나타내었는데 이 때의 발광 중심은 열처리할 때 생긴 S-vacancy에 보상된 산소로 이루어진 'CdO'의 악셉터준위에 기인하는 것으로 해석되며 그 이온화 에너지는 약 0.16eV이었다.

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A Study on the Measurement Technique of the Characteristics of Electromagnetic Wave Absorber Using $20 mm\phi$ Coaxial Tube ($20 mm\phi$ 동축관을 이용한 전파흡수체의 특성측정법에 관한 연구)

  • 김동일;정중식;백명숙;안영섭;정세모
    • The Proceeding of the Korean Institute of Electromagnetic Engineering and Science
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    • v.4 no.2
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    • pp.17-23
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    • 1993
  • This study aims to measure the reflection loss and the material constants of the fabricated samples for electromagnectic wave absorber by using $20 mm\phi$ coaxial tube with the endshort-type. The authors have established the extraction algorithm of material constants by one port method, and proved that the results of the experiments were in agreement with the calculated ones. On the basis of the above results, the validity of the proposed measuring method is confirmed. This measurement method could be used effectively for the design of microwave absorber and for its evalustion.

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An Improved Method for the Measurement of Fungal Degradability of Synthetic Polymers (진균에 의한 합성고분자재료 분해도 측정법의 개선)

  • 이영하;이정애;맹필재;전창림
    • Korean Journal of Microbiology
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    • v.28 no.2
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    • pp.158-161
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    • 1990
  • An improved fungal test method, soft agar overlay method, has been developed for the measurement of biodegradability of synthetic polymers. Advantages of this technique over conventionally used test method of ASTM include better visualization of fungal growth on polymeric materials, shortening of incubaiton period, and engnaced sensitivity especially to polymeric materials containing highly recalcitrant molecules.

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Development of Coercivity Measuring System for Ferromagnetic Materials in Open Magnetic Circuit (개방자기회로에서 강자성재료의 보자력 측정장치 개발)

  • 유권상;박진습
    • Journal of the Korean Magnetics Society
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    • v.10 no.6
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    • pp.297-301
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    • 2000
  • Coercivity is defined as the magnetic field strength required to reduce the magnetic polarization to zero of magnetic specimen which has been previously magnetized to saturation. This quantity is a reference for classifying soft and hard magnetic materials. We have constructed the measuring system for measurement of coercivity of ferromagnetic materials in open magnetic circuit. The measurement range of the constructed system is from tens A/m to tens kA/m, the combined uncertainty is ${\pm}$0.22 kA/m as coercivity is 14.63 kA/m.

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