• Korean Journal of Materials Research
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• v.4 no.2
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• pp.241-249
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• 1994

We studied on the effects of hot-worm rolling on recrystalized structures and tensile strength in over-aged 7075 A1 alloy, to develop the process for improving properties. It showed more clear effect of the grain refinement with over-aging before plastic deformation. That means, the coarse precipitates from over-aging play a roll as nucleation sites in the course of recrystallization. And on this study, the relations between yield strength and grain size was not satisfied with Hall-Petch equation because of the elongated structure, but the yield strength is proportional to aspect ratio of grains. In TMT process for improving strength and toughness, the worm working is available for increase of those properties than cold working.

• Korean Journal of Materials Research
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• v.2 no.5
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• pp.343-352
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• 1992

The high temperature deformation behavior of microalloyed hot forging steels has been examined as a function of the temperature, the strain rate, and the alloying element by using high temperature compression test. The high temperature deformation mechanism, which was obtained by analyzing the flow stress-strain curve and microstructure, could be considered to dynamic recrystallization. The peak stress of Nb-V-Mo steel was more increased and the dynamic recrystallization of Nb-V-Mo steel was faster than those of Nb-V steel. The peak stress of 1.2Mn-0.09Nb steel was more increased and the dynamic recrystallization of 1.2Mn-0.09Nb was delayed a little bit than those of 1.0Mn-0.05Nb. The peak stress of C-Nb-V steel was more increased and the dynamic recrystallization of C-Nb-V steel was delayed than those of C-steel. The constitutive equation of high temperature deformation had a power law type. The grain size of dynamic recrystallization was refined as the Zener-Hollomon parameter was increased. The relation of the dynamic recrystallization grain size and Zener-Hollomon parameter could be quantified to power law.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.2 no.2
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• pp.53-62
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• 1992

In Zone Melting Recrystallization(ZMR) of SOl structure, thin silicon films have been recrystallized by artificial control of beam intensity profile which was obtained by tilting of upper elliptical reflector. Temperature profiles and gradients near solidification interface were calculated by numerical simulation for analysis of asymmetric line heating effect. The larger the tilting angle of the upper reflector, the larger the degree of supercooling at liquid and the interdefect spacing in thin silicon films. Major defects were continuous subgrainboundaries. Isolated threading dislocations were observed in the case of the film having low defect density. We have found that the thin silicon films were recrystallized into (100) textured single crystals by cross-sectional TEM and thin film X-ray diffraction analysis.

• Proceedings of the Materials Research Society of Korea Conference
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• 2009.05a
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• pp.43.2-43.2
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• 2009

니켈기 초내열합금 Inconel 617은 Cr, Mo 등의 첨가물이 함유된 고용 강화된 합금으로써, 우수한 고온 강도, 크립 저항성, 내부식성 및 내산화성을 가지고 있는 것으로 알려져 있다. 또한 Inconel 617의 주된 carbide은 $M_{23}C_6$와 미량의 $M_6C$ carbide로 형성되어있다. 본 연구에서는 냉간 압연 및 고온열화가 carbide의 크기, 분율 그리고 상 변화에 미치는 영향을 평가하였다. 냉간 압연은 50%까지 수행하였으며, 50% 냉간 압연한 시편을 $1050^{\circ}C$에서 1시간 동안 재결정을 수행하였다. 이로 인해 미세한 결정립과 carbide을 가지는 시편을 확보할 수 있었으며, as-received 시편 보다 균일하게 carbide을 분산 시킬 수 있었다. 또한 재결정 후 $950^{\circ}C$에서 고온열화에 의한 carbide의 변화를 평가함으로써, 냉간 압연 및 고온열화에 의한 carbide의 크기, 분율 그리고 상 변화에 미치는 영향을 평가할 수 있었다. Carbide의 분율을 평가하기 위하여 BSE image을 관찰하였으며, Image analyzer을 이용하여 계산되었다. 그리고 carbide의 성분 분석을 통한 $M_{23}C_6$와 $M_6C$의 상을 평가하기 위하여 EPMA 분석을 수행하였으며, carbide의 분산에 의한 균질도를 평가하기 위하여 비커스 경도를 측정하였다.

• Korean Journal of Food Science and Technology
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• v.36 no.2
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• pp.288-293
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• 2004

Differential scanning calorimetry (DSC) was used to study effects of sucrose and gluten on wheat starch glass transition, gelatinization, and retrogradation. Glass transition temperature ($T_{g}$) of wheat starch decreased as the ratio of sucrose or gluten to starch increased. Both peak temperature ($T_{G}$) and enthalpy values of gelatinization endotherm increased or decreased with increasing ratio of sucrose or gluten, respectively. Wheat starch gel with no sucrose and gluten recrystallized up to 4 weeks of storage at $4^{\circ}C$, whereas those with sucrose and gluten completed recrystallization within 1 week. Both wheat starch gels with no sucrose and gluten, and those with sucrose and gluten at storage temperature of $32^{\circ}C$ recrystallized up to 4 weeks, with wheat starch-sucrose-gluten (1 : 0.5 : 0.12) system, which had highest ratios of gluten and sucrose to starch, showing lowest recrystallization. Nucleation and propagation rates of starch gel recrystallization based on polymer crystallization principles can be converted into peak width (${\delta}T$) and peak temperature ($T_{R}$) of retrogradative endotherm by DSC, because higher nucleation rate at storage temperature of $4^{\circ}C$ close to $T_{g}$ showed higher ${\delta}T$, whereas higher propagation rate at $32^{\circ}C$ (close to $T_{G}$) had higher $T_{R}$.

• Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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• v.16 no.1
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• pp.49-58
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• 2018

For the immobilization of high-radioactive nuclides such as Cs and Sr by high-temperature thermal decomposition, this study was carried out to investigate the phase transformation with calcined temperature by using TGA (thermogravimetric analysis) and XRD (X-ray diffraction) in the Cs-adsorbed CHA (chabazite zeolite of K type)-Cs and CHA-PCFC (potassium cobalt ferrocyanide)-Cs zeolite system, and Sr-adsorbed 4A-Sr and BaA-Sr zeolite system, respectively. In the case of CHA-Cs zeolite system, the structure of CHA-Cs remained at up to $900^{\circ}C$ and recrystallized to pollucite ($CsAlSi_2O_6$) at $1,100^{\circ}C$ after undergoing amorphous phase at $1,000^{\circ}C$. However, the CHA-CFC-Cs zeolite system retained the CHA-PCFC-Cs structure up to $700^{\circ}C$, but its structure collapsed in $900{\sim}1,000^{\circ}C$, and then transformed to amorphous phase, and recrystallized to pollucite at $1,100^{\circ}C$. In the case of 4A-Sr zeolite system, on the other hand, the structure of 4A-Sr maintained up to $700^{\circ}C$ and its phase transformed to amorphous at $800^{\circ}C$, and recrystallized to Sr-feldspar ($SrAl_2Si_2O_8$, hexagonal) at $900^{\circ}C$ and to $SrAl_2Si_2O_8$ (triclinic) at $1,100^{\circ}C$. However, the BaA-Sr zeolite system structure began to break down at below $500^{\circ}C$, and then transformed to amorphous phase in $500{\sim}900^{\circ}C$ and recrystallized to Ba/Sr-feldspar (coexistence of $Ba_{0.9}Sr_{0.1}Al_2Si_2O_8$ and $Ba_{0.5}Sr_{0.5}Al_2Si_2O_8$) at $1,100^{\circ}C$. All of the above zeolite systems recrystallized to mineral phase through the dehydration/(decomposition) ${\rightarrow}$ amorphous ${\rightarrow}$ recrystallization with increasing temperature. Although further study of the volatility and leachability of Cs and Sr in the high-temperature thermal decomposition process is required, Cs and Sr adsorbed in each zeolite system are mineralized as pollucite, Sr-feldspar and Ba/Sr-feldspar. Therefore, Cs and Sr seen to be able to completely immobilize in the calcining wasteform/(solidified wasteform).

• Proceedings of the Korean Magnestics Society Conference
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• 1991.05a
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• pp.71-72
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• 1991

• Transactions of Materials Processing
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• v.11 no.1
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• pp.3-13
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• 2002

• Proceedings of the Materials Research Society of Korea Conference
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• 2001.05a
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• pp.148-148
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• 2001

• 한국지구물리탐사학회:학술대회논문집
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• 2009.10a
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• pp.43-43
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• 2009