• The Korean Journal of Pesticide Science
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• v.8 no.1
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• pp.30-37
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• 2004

This study estimated the correlation between surface area/weight ratios and pesticide residues in two varieties of tomato, mini tomato and tomato. The ratios of surface area/weight of mini tomato and tomato were $2.15cm^2g^{-1}$ and $1.00cm^2g^{-1}$ respectively. Pesticide residues were measured with four kinds of pesticide, chlorothalonil WP, chlorothalonil SC, oxadixyl WP, thiophanate-methyl WP. Ie residue amount of mini tomato was $1.4\sim2.4$ times higher than those in tomato regardless of the application date and frequency. The ratios of surface area/weight on tomato varieties played a key role for determining pesticide residue.

• Journal of Navigation and Port Research
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• v.26 no.4
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• pp.435-440
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• 2002

The quantitative assessment of the effect of the residual stress on fracture behavior was executed by some experiment and numerical analysis. First of all, artificial residual stresses were imposed on CT(Compact Tension) specimens by local heating using gas torch, and an appropriate distribution of residual stresses was obtained by thermal elastic-plastic FE analysis. To certify the result of the FE analysis, an experimental measurement was performed in accordance with ASTM standard. Fracture toughness test was executed on the several types of specimens. The first type was the specimen without residual stresses, and the others had different peak value of compressive residual stress at crack front via controlling the heat flux. All the test results were presented on th J resistance(JR) curves and discussed to verify the effect of compressive residual stresses on fracture behavior.

• YAKHAK HOEJI
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• v.37 no.1
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• pp.54-65
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• 1993

A method for the determination of 16 residual pesticides in crude deugs was examined. Crude drug was extracted with acetonitrile/water solution and the extract was partitioned between hexane/CH$_{2}$Cl$_{2}$ and NaCl saturated water. The organic layer was passed through cleanup column and subjected to the GC/ECD or GC/NPD analysis. Essential oil components in crude drug interfere with the analysis, and sulfuric acid treatment was adapted to overcome this interference.

• Journal of the Institute of Electronics Engineers of Korea TC
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• v.47 no.8
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• pp.9-15
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• 2010

This paper presents an analysis of asynchronous multicarrier-code division multiple access (MC-CDMA) uplink systems over frequency-selective multipath fading channels when the frequency offsets (FOs) of all users are random variables and the frequency offset for the desired user is compensated. The effect of a residual frequency offset(RFO) on the average bit error rate (BER) is evaluated by the semi-analytical method, then the approximated BER performance is obtained as a closed-form expression. Moreover, the signal to noise ratio (SNR) loss caused by RFO is evaluated. Derived results show that the performance degradation due to RFO is negligible if the estimation error of RFO for the desired user is less than the normalized value of 0.1.

• Analytical Science and Technology
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• v.13 no.1
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• pp.34-40
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• 2000

The optimum conditions for the half-life time and residual analysis of the iminoactadine triacetate fungicide on soils were investigated by using the gas chromatography. Iminoctadine triacetate(IOTA) was extracted from soils with 2.0 M-NaOH/methanol and chloroform. The extracted IOTA was derivatized to pyrimidine hexafluroacetylacetone by the acetylation and analyzed with GC/ECD after elimination of moisture and impurities on the Sep-Pak column. From the standard addition experiments with 0.1 and 1.0 ppm, the average recoveries were ranged from 83.8 to 93.2 % and the detection limit was 0.005 ppm. The half-life time of iminoctadine triacetate in the silty clay was 30 days in the laboratory and 19.5 days in the field test whereas it was 27 days and 17.5 days for each in case of silty loam.

• Economic and Environmental Geology
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• v.44 no.1
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• pp.49-57
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• 2011

Water budget analysis in the groundwater system was conducted in order to understand water budget distributions in the ground water system in Geum-gang watershed. The annual amounts of precipitation, runoff, evapotranspiration, dam storage change and water supply over the sub-watershed in Geum-gang watershed were evaluated the residual groundwater from 2002 to 2006, based on the water budget considering inflow and outflow. Then we are able to expect residual groundwater of each sub-basin. According to the result of study, the year 2003 and 2006 were recorded the highest and the lowest precipitation value, respectively. Average run-off percentage against precipitation was 60.44%. Annual evapotranspiration in each of years didn't show the remarkable variations but the values were high in the lower reaches of the basin. The residual waters in Geum-gang basin were determined to be 133.36 in 2002, 77.64 in 2003, -19.40 in 2004, -82.25 in 2005 and -128.07 mm in 2006. The residual water in Geum-gang basin was high in the main and up stream such as Maepo. Also the residual water showed low distributions in Nonsan and Seokhwa.

• Proceedings of the Korean Institute of Navigation and Port Research Conference
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• 2012.06a
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• pp.15-17
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• 2012

파, 해저지반 및 해안 해양구조물과의 관계는 해안공학뿐만 아니라 지반공학 분야에서도 중요한 이슈중의 하나이며, 파랑에 의한 해저지반 내부의 압력 및 응력의 파악은 다양한 해안 해양 구조물의 기초 설계 및 해저 연안 지반의 불안정성 검토에 있어서 중요한 과제이다. 해저 지반의 불안정에 대한 문제 중, 파랑에 의한 해저지반의 액상화는 기존의 연구를 통하여, 두개의 메커니즘이 존재한다는 것이 밝혀졌으며, 이는 각각 파랑에 의해 해저지반 내부에 발생하는 과잉간극수압의 변동 특성 및 잔류 특성에 따른 것이다. 이 연구에서는 중복파에 의해 해저지반 내부에 에 발생하는 과잉간극수압에 대하여 수치해석을 하였으며, 발생하는 과잉간극 수압 중 잔류 과잉간극수압의 발생 특성과 실험 결과를 비교 분석하였다.

• Proceedings of the Korean Vacuum Society Conference
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• 2014.02a
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• pp.141.1-141.1
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• 2014

오일 증기의 제트를 분사하여 잔류가스를 배기하는 오일확산펌프는, 구조가 간단하여 고장이 적고 저렴하며 소음 및 전기노이즈가 적게 발생하는 많은 장점을 가지고 있다. 그러나 오일의 증기압에 의해 그 도달압력이 10-9 Torr 이상으로 제한되어, 액체질소로 냉각되는 배플형태의 저온 트랩을 사용하지 않는 한 10-10 Torr영역의 초고진공 배기용으로는 사용하지 못하는 것으로 알려져 있다. 유회전펌프로 뒷받침 배기(foreline pumping)하는 700l/s의 배기속도를 가진 오일확산펌프에 300 liter/sec의 컨덕턴스를 가진 액체질소 트랩을 부착하여 메탈 실링을 사용하는 초고진공 챔버를 배기하였다. 액체질소트랩에 액체질소를 투입하면 $1{\times}10-8Pa$이하의 초고진공이 얻어졌으나, 액체질소가 증발하여 트랩의 온도가 상온으로 상승하면 압력도 $1{\times}10-7Pa$ 이상으로 상승하였다. 50 liter/sec의 배기속도를 가진 터보분자펌프로 오일확산펌프를 뒷받침 배기하면 액체질소를 투입하지 않은 상태에서 $5{\times}10-9Pa$이하의 초고진공이 얻어졌으며, 액체질소를 투입하여도 압력은 거의 변화하지 않았다. 잔류가스분석장치로 얻은 잔류가스 성분 스펙트럼은 수소가 잔류가스의 대부분을 차지하는 것을 보여주었다.

• Journal of Food Hygiene and Safety
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• v.34 no.1
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• pp.30-39
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• 2019

An analytical method was developed for the determination of sedaxane in agricultural products using liquid chromatograph-tandem mass spectrometry (LC-MS/MS). The samples were extracted with acetonitrile and partitioned with dichloromethane to remove the interference, and then purified by using silica SPE cartridges to clean up. The analytes were quantified and confirmed by using LC-MS/MS in positive ion mode using multiple reaction monitoring (MRM). The matrix-matched calibration curves were linear over the calibration ranges ($0.001-0.25{\mu}g/mL$) into a blank extract with $r^2$>0.99. For validation, recovery tests were carried out at three different concentration levels (LOQ, 10LOQ, and 50LOQ, n=5) with five replicates performed at each level. The recoveries were ranged between 74.5 to 100.8% with relative standard deviations (RSDs) of less than 12.1% for all analytes. All values were consistent with the criteria ranges requested in the Codex guidelines (CAC/GL 40, 2003) and Food Safety Evaluation Department guidelines (2016). The proposed analytical method was accurate, effective and sensitive for sedaxane determination in agricultural commodities.

• Journal of Applied Biological Chemistry
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• v.65 no.1
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• pp.17-21
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• 2022

A new rapid and simple method for metalaxyl in Atractylodes macrocephala Koidzumi and Achyranthes japonica Nakai has been developed and validated. This study was conducted to develop a method for analyzing metalaxyl by a method based on QuEChERS using liquid chromatography coupled with tandem mass spectrometry (LC-MS/MS). Samples were extracted with acetonitrile and purified using amino-propyl (NH₂) Solid Phase Extraction cartridge. The method limit of quantitation (MLOQ) was 0.01 mg/kg. The linearity of matrix-matched calibration curve (r²) was ≥0.99 at the calibration range of 0.001-0.05 mg/kg. For recovery test, Atractylodes macrocephala Koidzumi or Achyranthes japonica Nakai was treated with standard solutions at MLOQ and 10MLOQ levels. Recovery rates were in the range of 88.1-109.1% with <5.5% coefficient of variation. This established analytical method was fully validated. Based on these results, it can contribute to improving the safety of residual pesticides in Atractylodes macrocephala Koidzumi and Achyranthes japonica Nakai.