• Title/Summary/Keyword: 자성입자

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Preparation of Magnetic Chitosan Microsphere Particles (나노 크기의 마그네타이트 입자를 이용한 자성 키토산 미소구체의 제조)

  • Ko, Sang-Gil;Cho, Jun-Hee;Ahn, Yang-Kyu;Song, Ki-Chang;Choi, Eun-Jung
    • Journal of the Korean Magnetics Society
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    • v.16 no.1
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    • pp.66-70
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    • 2006
  • Magnetite nanoparticles, which have been extensively used in many fields, were encapsulated with a natural polymer, chitosan, to improve their biocompatibility. We have synthesized magnetite $(Fe_3C_4)$ nanoparticles using chemical coprecipitation technique with sodium oleate as surfactant. Nanoparticle size can be varied from 1.2 to 7.4nm by controlling the sodium oleate concentration. Magnetite phase nanoparticles could be observed from X-ray diffraction. Magnetic colloid suspensions containing particles with sodium oleate and chitosan have been prepared. High magnetic property chitosan-microsphere particles were prepared from oleate-coated magnetite suspension using spray method. The surftce, and tile morphology of the magnetic chitosan microsphere particles were characterized using optical microscope and scanning electron microscope. Magnetic hysteresis measurement were performed using a superconducting quantum interference device (SQUID) magnetometer at room temperature to investigate the magnetic properties of the chitosan microspheres including magnetite nanoparticles. The SQUID measurements revealed superparamagnetism of nanoparticles.

평판형 자기장 발생기를 이용한 자성 나노 파우더 기열에 관한 연구

  • Yu, Jae-Hyeong;Lee, Jae-Seon;No, Jun-Hyeong;Jo, Tae-Hun;Yun, Myeong-Su;Park, Bong-Ju;Choe, Eun-Ha;Gwon, Gi-Cheong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2014.02a
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    • pp.434.1-434.1
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    • 2014
  • 최근 자성 나노 입자를 이용한 온열치료가 주목을 받고 있다. 자성을 띄는 나노 입자를 암 세포에 보내, 교류 자기장을 걸어주어 회전에 의한 마찰손실로 인한 열을 이용하여 암 조직만을 국소 가열하는 원리이다. 본 실험은 유도 자기장을 사용한 자성 나노 파우더의 가열을 목적으로 시행하였다. 나선형 코일위에 세라믹, 유리 등 절연체 원판 위에 자기장이 발생되도록 휴대용 평판형 자기장 발생장치를 제작하였다. 자기장 발생 장치는 평판형 나선형 코일에 특정 주파수를 가진 전원을 인가하여 자기장을 발생시킨다. 평판형 나선형 코일은 내경 40 mm, 외경 140 mm, 2 mm 동선으로 제작하였다. 제작한 자기장 발생장치를 자기장 측정 센서(Hall sensor 등)을 원판 위에 설치하여 거리별 자기장의 크기를 측정하였다. 자기장은 나선형 코일 위 원판 중심에서 최대로 발생되어 중심에서 멀어질수록 크기가 감소하였다. 자기장 발생장치 위에 자성 나노 파우더($Fe_3O_4$$CoFe_2O_4$)를 혼합한 용액 시료를 위치시키고 자기 쌍극자 모멘트와 자기장간의 상호작용을 유도한다. 이때 자성 나노 파우더별로 발생하는 열을 열전쌍(TC)이나 Optical fiber를 사용한 Thermometer로 측정하여 비교분석하였다.

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Development of Ultraprecision Finishing Technique using Bonded Magnetic Abrasives (결합된 자성연마입자를 이용한 초정밀 피니싱 기술 개발)

  • 윤종학;박성준;안병운
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.12 no.5
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    • pp.59-66
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    • 2003
  • This study suggests the new ultraprecision finishing techniques for micro die and mold parts using magnetic field-assisted polishing. Conventional magnetic abrasives have several disadvantages, which are missing of abrasive particle and inequal mixture between magnetic particle and abrasive particle. Therefore, bonded magnetic abrasive particles are fabricated by several method. For example, plasma melting and direct bonding. Carbonyl iron powder is used as magnetic particle there silicon carbide and alumina are abrasive particles. Developed magnetic abrasives are analyzed using SEM. Feasibility of magnetic abrasive and polishing performance of this magnetic abrasive particles also have been investigated. After polishing, surface roughness of workpiece is reduced from 85.4 ㎚ Ra to 9 ㎚ RA.

Mössbauer Studies of CoGa0.1Fe1.9O4 Nanoparticles (나노분말 CoGa0.1Fe1.9O4의 Mössbauer 분광학적 연구)

  • Lee, Seung-Wha
    • Journal of the Korean Magnetics Society
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    • v.16 no.2
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    • pp.144-148
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    • 2006
  • $CoGa_{0.1}Fe_{1.9}O_4$ nanoparticles have been prepared by a sol-gel method. The structural and magnetic properties have been investigated by XRD, SEM, VSM and $M\ddot{o}ssbauer$ spectroscopy. $CoGa_{0.1}Fe_{1.9}O_4$ powder that was annealed at $250^{\circ}C$ has spinel structure and behaved superparamagnetically. The estimated size of superparammagnetic $CoGa_{0.1}Fe_{1.9}O_4$ nanoparticle is around 10 nm. The hyperfine fields at 4.2 K f3r the A and B patterns were found to be 518 and 486 kOe, respectively. The blocking temperature $(T_B)$ of superparammagnetic $CoGa_{0.1}Fe_{1.9}O_4$ nanoparticle is about 250 K. The magnetic anisotropy constant of $CoGa_{0.1}Fe_{1.9}O_4$ nanoparticle was calculated to be $3.0X10^5\;ergs/cm^3$. $CoGa_{0.1}Fe_{1.9}O_4$ nanoparticle was annealed at $250^{\circ}C$ will be used to candidate for biomedicine applications as magnetic carriers.

Fabrication and Performance Evaluation of a Micro Separation Chip of Magnetic Beads Using Magnetophoretic Flow (자기영동을 이용한 자성입자 분리 마이크로 칩 제작 및 성능평가)

  • Go, Jeung-Sang
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.31 no.4
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    • pp.392-397
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    • 2007
  • We developed a microfluidic platform able to control the trap and release of magnetic beads used for separation of a specific biomolecules. The magnetic beads can be trapped and released conditionally by controlling the difference between the Stokes force induced by the fluid flow and magnetic force resulting from a permanent magnet. The permanent magnet of CoNiP alloy is electroplated. It is characterized to have the 1369 Oe of coercivity, 1762 Gauss of remanence, and 0.603MGOe of (BH)max. Through the experimental and numerical investigation, the magnetic beads are trapped under the flow velocity of 17 ${\mu}m/s$ and are released perfectly above the velocity of 174 ${\mu}m/s$.

Magnetic beads separation using a multi-layered microfluidic channel (다층구조의 미세유체채널을 이용한 자성입자 분리)

  • Lee, Hye-Lyn;Song, Suk-Heung;Jung, Hyo-Il
    • Proceedings of the KSME Conference
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    • 2008.11a
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    • pp.1685-1686
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    • 2008
  • This paper presents the design and experiment results of a multi-layered microsystem for magnetic bead applications. The magneto-microfluidic device is designed for capable of separating magnetic beads. In the presence of the magnetic field, magnetic beads are attracted and moved to high gradient magnetic fields. A multi-layered microfluidic channel consists of top and bottom layers in order to separate magnetic beads in the vertical direction. Our channel is easily integrated magnetic cell sorter, especially on-chip microelectromagnet or permanent magnet device. Fast separation of magnetic beads in top and bottom channels can be used in high throughput screening to monitor the efficiency of blood and drug compounds.

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Numerical Modeling for Behavior Prediction of the Magnetic Fluid Based on Finite Element Method (유한요소법을 이용한 자성유체의 거동예측을 위한 수치적 모델링)

  • Seo, Jae-Hyeong;Lee, Moo-Yeon;Seo, Lee-Soo
    • Journal of the Korean Magnetics Society
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    • v.23 no.1
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    • pp.31-35
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    • 2013
  • The objective of this study is numerically analyzed the behavior characteristics of the magnetic fluid in a closed rectangular container using finite element method (FEM). The governing equations are solved with magnetization and Maxwell equations for consideration of rotating effect of the magnetite particle. Then the discretized equations are solved with boundary conditions of the velocity and temperature. The developed model is validated with the results of Davis (1983) and Fusegi et al. (1991) has a good agreement within 5.5 % and 2.7 %, respectively.

Flow Visualization of Magnetic Particles under the external magnetic field in bubbly flow using Single Plane Illumination Microscopy - MicroPIV (Single Plane Illumination Microscopy - MicroPIV를 이용한 버블 유동에서 외부 자계 영향을 받는 자성입자 가시화)

  • Lee, Changje;Cho, Gyeong-rae;Lee, Sangyoup
    • Journal of the Korean Society of Visualization
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    • v.19 no.1
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    • pp.36-42
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    • 2021
  • This study measured the velocity of magnetic particles inside the power generation using external heat sources. Single Plane Illumination Microscopy (SPIM) was used to measure magnetic particles that are simultaneously affected by bubbly flow and magnetic field. It has the advantage of reducing errors due to particle superposition by illuminating the thin light sheet. The hydraulic diameter of the power generation is 3mm. Its surface is covered with a coil with a diameter of 0.3 mm. The average diameter of a magnetic particle is 200nm. The excitation and emission wavelengths are 530 and 650nm, respectively. In order to find out the flow characteristics, a total of four velocity fields were calculated in wide and narrow gap air bubbles, between the wall and the air bubble and just below the air bubble. Magnetic particles showed up to 8.59% velocity reduction in the wide gap between air bubbles due to external magnetic field.