• Transactions of the Korean Society of Mechanical Engineers
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• v.13 no.3
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• pp.472-478
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• 1989

Using the SMC(sheet moulding compound) composite material consisting of E-glass chopped strand mat and unsaturated polyester resin, three-point bending tests are carried out to evaluate the elasto-plastic fracture toughness by means of R curve. The crack extension is experimentally observed with the ink staining method. The point of stable crack growth is discussed in consideration of the load-load point displacement curve, the damage behavior of the notch vicinity, and the R-curves. The damage zone of the notch vicinity was composed of the initiation and growth of subcracks as well as those of the main crack. The point of stable crack growth can be defined as the inflection point in the R curves and its point also concurrs with the proportional limit on the load-load point displacement curve.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.23 no.5
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• pp.255-264
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• 2013

Cobalt aluminate ($CoAl_2O_4$) is a highly stable pigment with excellent resistance to light, weather, etc., which has resulted in widespread use as a ceramic pigment. Due to the unique optical characteristics, $CoAl_2O_4$ is generally used as a coloring agent to decorate porcelain products, glass, paints and plastics. Here, $CoAl_2O_4$ pigments were synthesized by polymerized complex method and solid state reaction. Then $CoAl_2O_4$ pigment were grinded using the attrition milling with 1 mm size zirconia ball for 3 hours. The attrition milling process was performed at the constant speed of 800 rpm and ball to powder weight ratio (BPR) was 100 : 1. The characteristics of synthesized pigment were analyzed by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), particle size analyser (PSA) and CIE $L^*a^*b^*$. The XRD patterns of $CoAl_2O_4$ show single phase spinel structure. The particle size of $CoAl_2O_4$ measured by FE-SEM, TEM and PSA analysis was in the range of 100~200 nm. The blue color of obtained $CoAl_2O_4$ pigments could be confirmed through CIE $L^*a^*b^*$ measurement.